CN106217586B - A kind of use for laboratory powder granule centrifugal forming device - Google Patents

A kind of use for laboratory powder granule centrifugal forming device Download PDF

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Publication number
CN106217586B
CN106217586B CN201610825781.7A CN201610825781A CN106217586B CN 106217586 B CN106217586 B CN 106217586B CN 201610825781 A CN201610825781 A CN 201610825781A CN 106217586 B CN106217586 B CN 106217586B
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CN
China
Prior art keywords
centrifugation
powder
pedestal
molding
powder granule
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201610825781.7A
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Chinese (zh)
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CN106217586A (en
Inventor
邸永江
贾碧
邱杨
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Chongqing University of Science and Technology
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Chongqing University of Science and Technology
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Priority to CN201610825781.7A priority Critical patent/CN106217586B/en
Publication of CN106217586A publication Critical patent/CN106217586A/en
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Publication of CN106217586B publication Critical patent/CN106217586B/en
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Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B1/00Producing shaped prefabricated articles from the material
    • B28B1/26Producing shaped prefabricated articles from the material by slip-casting, i.e. by casting a suspension or dispersion of the material in a liquid-absorbent or porous mould, the liquid being allowed to soak into or pass through the walls of the mould; Moulds therefor ; specially for manufacturing articles starting from a ceramic slip; Moulds therefor
    • B28B1/28Producing shaped prefabricated articles from the material by slip-casting, i.e. by casting a suspension or dispersion of the material in a liquid-absorbent or porous mould, the liquid being allowed to soak into or pass through the walls of the mould; Moulds therefor ; specially for manufacturing articles starting from a ceramic slip; Moulds therefor involving rotation of the mould about a centrifugal axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B13/00Feeding the unshaped material to moulds or apparatus for producing shaped articles; Discharging shaped articles from such moulds or apparatus
    • B28B13/04Discharging the shaped articles
    • B28B13/06Removing the shaped articles from moulds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28BSHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B3/00Producing shaped articles from the material by using presses; Presses specially adapted therefor
    • B28B3/02Producing shaped articles from the material by using presses; Presses specially adapted therefor wherein a ram exerts pressure on the material in a moulding space; Ram heads of special form

Abstract

The present invention is for when preparing new material powder by liquid phase method, tradition molding is big to the demand of powder, more, powder shape is lost and property is easy the disadvantages of changing, a kind of use for laboratory powder granule centrifugal forming device is invented, centrifuge tube including bottom of which has holes, it is centrifuged side wall, molding cylinder, shaping base, centrifugation pedestal, contoured squeeze board, demoulding pedestal, powder granule is first preforming in being centrifuged preforming system, then the compression moulding in press-moulding die system.The present invention is suitble to laboratory to use when preparing the molding of a small amount of powder granule, the defect that several grams or less powder granule can be formed, while powder reuniting, powder structure and property being avoided to change, and can be reduced experimental procedure, and convenient formation is quick.

Description

A kind of use for laboratory powder granule centrifugal forming device
Technical field
Being used the present invention relates to a kind of centrifugal forming device and its application method more particularly to a kind of suitable laboratory, Molding centrifugal forming device is carried out after preparing a small amount of powder granule by liquid phase method.
Background technique
It is all much to first pass through the liquid phase method such as precipitation method, hydro-thermal method, water when laboratory carries out new material research or exploitation The methods of solution prepares new material powder, needs further to separate powder with liquid later, dries, is levigate, molding, heat Processing or sintering, block materials are made and study its performance.But the new material powder granule prepared when generally testing Amount it is fewer, such as powder quality only has tens grams, several grams or less, and the amount ratio for the powder that common forming method needs More, whole process loss is larger, and is easy to reunite after drying, then the powder after drying is changed to the shape of powder when levigate And property, thus affect the performance of material.General centrifugal formation method is mainly used in the centrifugation of the products such as hollow cement Molding, and the powder of the components such as ceramics, metal are made suspended nitride centrifugal forming again, huge construction and are first made outstanding The method that laitance material carries out centrifugal forming again is not suitable for the centrifugal forming of a small amount of powder when new material experiment.Based on small-sized centrifugation The powder granule and liquid phase separation that machine prepares liquid phase method, and pressed again using centrifugal forming device by powder granule is preforming Type is made, can be convenient the heat treatment for efficiently carrying out new material and performance test experiment.
Summary of the invention
When the present invention is for powder is prepared using liquid phase method in the exploitation of existing new material research, the amount of the powder of preparation compared with Less, when then being separated with liquid by powder, dry, is levigate, forming, being heat-treated or sintering into block materials and studying its performance, powder The disadvantages of demand of body is big, more, powder the shape of loss and property are easy change proposes a kind of to prepare liquid phase method After original powder cleaning, first carry out being centrifuged preforming, the re-compacted device at block materials.Technical scheme is as follows:
A kind of use for laboratory powder granule centrifugal forming device, the centrifuge tube including bottom of which has holes are centrifuged side wall, shaping column Body, shaping base, centrifugation pedestal, contoured squeeze board and demoulding pedestal, it is characterised in that:Centrifugation side wall and molding cylinder are entrenched in one It rises, centrifugation lower sidewall is entrenched togather with shaping base, and centrifugation lower sidewall is that scalariform is hollow;Being centrifuged pedestal is cylinder Hollow shape, is centrifuged pedestal and shaping base is entrenched togather;Molding cylinder is hollow cylindrical, the top of molding cylinder and molding Pressure head lower part coincide, and the lower part of molding cylinder and the top of shaping base coincide;Demoulding the middle of the base is hollow spill, for compacting It is detached from the slave molding cylinder of shaping base and molding sample after molding and space is provided.
The use for laboratory powder granule centrifugal forming device, it is characterised in that:It is centrifuged side wall and is centrifuged the material of pedestal Matter be loose porous polymer material, molding cylinder, contoured squeeze board, shaping base and demould pedestal material be stainless steel or Mould steel.
The use for laboratory powder granule centrifugal forming device, it is characterised in that:The centrifuge tube of bottom of which has holes, centrifugation side The preforming system of centrifugation that wall, molding cylinder, shaping base, centrifugation pedestal and contoured squeeze board are constituted;Molding cylinder, contoured squeeze board Press-moulding die system is constituted with shaping base;Powder granule be put into the preforming system of centrifugation be centrifuged it is preforming;It takes out Molding cylinder, shaping base and preformed powder granule, form powder particle in press-moulding die system, most Press-moulding die system is placed on demoulding pedestal afterwards and applies appropriate pressure, the sample of forming is taken out.
The present invention has following beneficial effect:
(1) powder granule centrifugal forming device be very suitable to laboratory using liquid phase method prepare a small amount of powder granule form when It uses, several grams or less powder granule can be formed into flakiness or cylindric material.
(2) present apparatus a small amount of liquid in top in centrifugal forming can be absorbed by porous centrifugation side wall, the liquid of lower part Body can flow to centrifugation pedestal by the gap between molding cylinder and shaping base, absorb or pass through centrifugation by centrifugation pedestal The circular hole of pedestal is discharged.
(3) present apparatus can be changed to avoid powder reuniting caused by traditional molding method for preparing, powder with structure and property The defect of change, and can be reduced experimental procedure, forming process is convenient and efficient.
Detailed description of the invention
Attached drawing 1 is the structural schematic diagram of use for laboratory powder granule centrifugal forming device;
Figure label:The centrifuge tube of 1- bottom of which has holes;2- is centrifuged side wall;3- molding cylinder;4- shaping base;5- is centrifuged bottom Seat;6- contoured squeeze board;7- demoulds pedestal;8- powder granule.
Specific embodiment
The invention proposes a kind of use for laboratory powder granule centrifugal forming devices, below by Detailed description of the invention and specifically real Applying example, the present invention will be further described.
Use for laboratory powder granule centrifugal forming device as shown in Figure 1, centrifugation side wall 2, the material for being centrifuged pedestal 5 are micro- Hole rubber, the material of molding cylinder 3, shaping base 4 and demoulding pedestal 7 are mould steel.Will centrifugation pedestal 5, shaping base 4, at Type cylinder 3, centrifugation side wall 2 are sequentially placed into the centrifuge tube 1 of bottom of which has holes, by 2-3 grams it is cleaned, pass through coprecipitation preparation YAG powder out is put into togerther in the centrifugation side wall 2 of centrifugal forming device together with liquid, then centrifugal forming is filled It is placed on centrifuge and carries out centrifugally operated, absorb the clear liquid on YAG powder top later, pass through centrifuge tube 1 and centrifugation The hole of pedestal 5 takes out molding cylinder 3, shaping base 4, then contoured squeeze board 6 is pressed into molding cylinder 3, will be by shaping column The press-moulding die system that body, shaping base, contoured squeeze board are constituted is placed on compression moulding on moulding press, finally will compacting Forming die system is placed on demoulding pedestal 7, and applying certain pressure makes the powder and shaping column of shaping base 4 and forming Body 3 separates, and the laminar sample of forming can carry out subsequent ceramic post sintering experiment.

Claims (3)

1. a kind of use for laboratory powder granule centrifugal forming device, centrifuge tube, centrifugation side wall, shaping column including bottom of which has holes Body, shaping base, centrifugation pedestal, contoured squeeze board and demoulding pedestal, it is characterised in that:Centrifugation side wall and molding cylinder are entrenched in one It rises, centrifugation lower sidewall is entrenched togather with shaping base, and centrifugation lower sidewall is that scalariform is hollow;Being centrifuged pedestal is cylinder Hollow shape, is centrifuged pedestal and shaping base is entrenched togather;Molding cylinder is hollow cylindrical, the top of molding cylinder and molding Pressure head lower part coincide, and the lower part of molding cylinder and the top of shaping base coincide;Demoulding the middle of the base is hollow spill, for compacting Shaping base and molding sample are detached from from molding cylinder and provide space after molding.
2. use for laboratory powder granule centrifugal forming device according to claim 1, it is characterised in that:Be centrifuged side wall and from The material of heart pedestal is loose porous polymer material, molding cylinder, contoured squeeze board, shaping base and the material for demoulding pedestal For stainless steel.
3. use for laboratory powder granule centrifugal forming device according to claim 1, it is characterised in that:Bottom of which has holes from The preforming system of centrifugation that heart pipe, centrifugation side wall, molding cylinder, shaping base, centrifugation pedestal and contoured squeeze board are constituted;Shaping column Body, contoured squeeze board and shaping base constitute press-moulding die system;Powder granule is put into the preforming system of centrifugation and is centrifuged It is preforming;Molding cylinder, shaping base and preformed powder granule are taken out, makes powder particle in press-moulding die system It is formed in system, finally press-moulding die system is placed on demoulding pedestal and applies appropriate pressure, the sample of forming is taken out.
CN201610825781.7A 2016-08-30 2016-08-30 A kind of use for laboratory powder granule centrifugal forming device Expired - Fee Related CN106217586B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610825781.7A CN106217586B (en) 2016-08-30 2016-08-30 A kind of use for laboratory powder granule centrifugal forming device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610825781.7A CN106217586B (en) 2016-08-30 2016-08-30 A kind of use for laboratory powder granule centrifugal forming device

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CN106217586B true CN106217586B (en) 2018-11-27

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2211181A (en) * 1987-10-19 1989-06-28 Fuji Tokushu Concrete Ind Concrete product with surface aggregate
KR20020044057A (en) * 2000-12-04 2002-06-14 무라타 야스타카 Powder feeding apparatus and powder forming apparatus
CN2811291Y (en) * 2005-08-12 2006-08-30 郑州磨料磨具磨削研究所 Centrifugal hot-pressed sintering device
KR20060109837A (en) * 2005-04-18 2006-10-23 칭 종 차이 Method for forming conductive concrete block containing graphite
CN204209086U (en) * 2014-11-05 2015-03-18 重庆孟池机械制造有限公司 Turbine centrifugal casting moulded barrel and outer wall cleaner
CN205148576U (en) * 2015-09-05 2016-04-13 周述文 Preparation equipment of ceramic tile back dovetail
CN206048449U (en) * 2016-08-30 2017-03-29 重庆科技学院 Use for laboratory powder granule centrifugal forming device

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2211181A (en) * 1987-10-19 1989-06-28 Fuji Tokushu Concrete Ind Concrete product with surface aggregate
KR20020044057A (en) * 2000-12-04 2002-06-14 무라타 야스타카 Powder feeding apparatus and powder forming apparatus
KR20060109837A (en) * 2005-04-18 2006-10-23 칭 종 차이 Method for forming conductive concrete block containing graphite
CN2811291Y (en) * 2005-08-12 2006-08-30 郑州磨料磨具磨削研究所 Centrifugal hot-pressed sintering device
CN204209086U (en) * 2014-11-05 2015-03-18 重庆孟池机械制造有限公司 Turbine centrifugal casting moulded barrel and outer wall cleaner
CN205148576U (en) * 2015-09-05 2016-04-13 周述文 Preparation equipment of ceramic tile back dovetail
CN206048449U (en) * 2016-08-30 2017-03-29 重庆科技学院 Use for laboratory powder granule centrifugal forming device

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