CN106213764A - The cleaning external member of a kind of shunting/Splitless injecting samples mouth and using method thereof - Google Patents
The cleaning external member of a kind of shunting/Splitless injecting samples mouth and using method thereof Download PDFInfo
- Publication number
- CN106213764A CN106213764A CN201610820626.6A CN201610820626A CN106213764A CN 106213764 A CN106213764 A CN 106213764A CN 201610820626 A CN201610820626 A CN 201610820626A CN 106213764 A CN106213764 A CN 106213764A
- Authority
- CN
- China
- Prior art keywords
- assembly
- shunting
- injecting samples
- splitless injecting
- samples mouth
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004140 cleaning Methods 0.000 title claims abstract description 16
- 238000000034 method Methods 0.000 title claims abstract description 11
- 229920000742 Cotton Polymers 0.000 claims abstract description 22
- 238000005406 washing Methods 0.000 claims abstract description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 20
- 239000002904 solvent Substances 0.000 claims description 12
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims description 4
- 239000010931 gold Substances 0.000 claims description 4
- 229910052737 gold Inorganic materials 0.000 claims description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 4
- 150000002576 ketones Chemical class 0.000 claims description 2
- 238000002347 injection Methods 0.000 abstract description 13
- 239000007924 injection Substances 0.000 abstract description 13
- 239000000356 contaminant Substances 0.000 abstract description 4
- 239000003960 organic solvent Substances 0.000 abstract description 4
- 238000007598 dipping method Methods 0.000 abstract description 3
- 238000010030 laminating Methods 0.000 abstract description 3
- 238000012423 maintenance Methods 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 11
- 238000005070 sampling Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000004454 trace mineral analysis Methods 0.000 description 2
- 206010019133 Hangover Diseases 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000002452 interceptive effect Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000001819 mass spectrum Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002324 mouth wash Substances 0.000 description 1
- 229940051866 mouthwash Drugs 0.000 description 1
- 239000000447 pesticide residue Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 238000004451 qualitative analysis Methods 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 239000000273 veterinary drug Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46B—BRUSHES
- A46B5/00—Brush bodies; Handles integral with brushware
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46D—MANUFACTURE OF BRUSHES
- A46D1/00—Bristles; Selection of materials for bristles
- A46D1/02—Bristles details
-
- B08B1/12—
-
- B08B1/143—
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/02—Cleaning by the force of jets or sprays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- A—HUMAN NECESSITIES
- A46—BRUSHWARE
- A46B—BRUSHES
- A46B2200/00—Brushes characterized by their functions, uses or applications
- A46B2200/40—Other application
Abstract
The invention belongs to instrument maintenance instrument and application, be specifically related to cleaning external member and the using method thereof of a kind of shunting/Splitless injecting samples mouth.Cleaning external member and include assembly I and assembly II, wherein there is a groove (7) in cylinder (5) end portion of assembly II, and this groove exists the upper age of a draught animal (6) and the lower age of a draught animal (8)；Using method include injection port accessory remove, use assembly I scrub and use inside assembly II wiping injection port weldment, drip washing and drying and other steps.Assembly I of the present invention can scrub the residual contaminants inside weldment by External Force Acting, after in assembly II, the groove part of cylinder fills the absorbent cotton dipping organic solvent, can under external force can high laminating degree by thorough for residual contaminants inside weldment wiped clean, simultaneously because there is the upper and lower age of a draught animal in groove, absorbent cotton does not comes off when moving up and down inside injection port weldment, clean external member have easy and simple to handle, clean remarkable advantage thoroughly.
Description
Technical field
The invention belongs to instrument maintenance instrument and application, be specifically related to the clear of a kind of shunting/Splitless injecting samples mouth
Wash external member and using method thereof.
Background technology
Gas chromatograph and the feature that gas chromatograph-mass spectrometer is high with its precision, qualitative, quantitative is effective are being eaten
Being used widely in multiple fields such as product, cosmetics, oil, is pesticide residues, residue of veterinary drug and other multiple Harmful chemicals
The important means of retention analysis.
The operation principle of gas chromatograph and gas chromatograph-mass spectrometer is typically to utilize detected object easily to vaporize
Feature, by detected object at shunting/Splitless injecting samples mouth rapid vaporization, the gaseous state measured target thing of formation is in carrier gas
Realize separating with interfering material through capillary tube or filling detached dowel under drive, arrive detector afterwards and be detected and by chromatograph
Workstation software is converted into recognizable chromatogram or mass spectrum, thus realizes the purpose of qualitative analysis and detection by quantitative.
Wherein, shunting/Splitless injecting samples mouth analyzes most important parts as gas chromatogram or gas chromatography combined with mass spectrometry
One of, in realizing trace analysis, play vital effect.According to statistics, the clean level of shunting/Splitless injecting samples mouth is
Affect gas chromatograph and gas chromatograph-mass spectrometer produces the key factor of qualitatively and quantitatively accuracy.When shunting/regardless of
When polluting occurs in stream injection port, would generally there is target peak disappearance, peak shape not in gas chromatograph and gas chromatograph-mass spectrometer
Symmetrical or hangover, the problems such as ghost peak or peak division, instrument quantitative bad stability occur.Have based on this, in application gas phase
When chromatograph and gas chromatograph-mass spectrometer carry out trace analysis, needs conscientiously clean, safeguard shunting/Splitless injecting samples mouth,
To obtain qualitative, quantitative effect accurately.
In the regular maintenance of shunting/Splitless injecting samples mouth, such as dottle pin, round section joint ring, bushing pipe, chromatographic column, reducing nut
All can dismantle Deng the related accessory at injection port position, intercept, change and clean.But the welding of shunting/Splitless injecting samples mouth
Part is owing to being welded on heating module, it is impossible to dismounting, it is difficult to clean, thus becomes shunting/Splitless injecting samples mouth and safeguard, clearly
The difficult point washed.
Currently, clean, safeguard shunting/Splitless injecting samples mouth method be typically with cotton swab dip organic solvent to shunting/
Wiping is carried out inside Splitless injecting samples mouth weldment.But owing to cotton swab absorbent cotton part is little compared with weldment internal diameter, absorbent cotton and weldering
Inside fitting, laminating degree is the highest, and cotton swab force-applied less, be prone to shortcomings such as fractureing, cause this kind of mode effectively to remove
The pollutant of residual inside shunting/Splitless injecting samples mouth weldment.
Summary of the invention
In order to solve currently to shunt/Splitless injecting samples mouth cleans the problem of difficulty, it is contemplated that in provide one shunting/
The cleaning external member of Splitless injecting samples mouth and using method thereof, to meeting the mesh quickly, thoroughly cleaning shunting/Splitless injecting samples mouth
Mark.
The present invention is achieved through the following technical solutions above-mentioned target.
The cleaning external member of a kind of shunting/Splitless injecting samples mouth, including assembly I and assembly II, wherein assembly I is by ring 1, gold
Belong to bar 2 and bristle 3 forms；Assembly II is made up of cylindrical handle 4 and cylinder 5, it is characterised in that cylinder 5 lower end of assembly II
There is a groove 7 in part, this groove exists the upper age of a draught animal 6 and the lower age of a draught animal 8.
Wherein,
Described assembly I is positioned at the bristle lengths of metallic rod 2 one side isometric and for 3mm to 4mm.
A diameter of 5mm to 6mm of the cylinder 5 of described assembly II.
The using method of the cleaning external member of a kind of shunting/Splitless injecting samples mouth comprises the following steps:
Step one, prepares: by the dottle pin of shunting/Splitless injecting samples mouth, round section joint ring, bushing pipe, chromatographic column, reducing nut etc.
Shunting/Splitless injecting samples mouth accessory is removed, and exposes shunting/Splitless injecting samples mouth；
Step 2, scrubs: place a beaker in the lower end of injection port, dips methanol with assembly I and scrubs shunting/no up and down
Inside split sampling mouth weldment, repeat 10 to 20 times；Afterwards, dip acetone solvent with assembly I and scrub shunting/do not shunt up and down
Inside injection port weldment, repeat 10 to 20 times；
Step 3, wiping: fill up the groove 7 of assembly II after absorbent cotton is dipped methanol, the cylinder 5 of assembly II is inserted point
Inside stream/Splitless injecting samples mouth weldment, repeat wiping 10 to 20 times up and down, discard absorbent cotton；Afterwards, absorbent cotton is dipped third
Fill up the groove 7 of assembly II after ketone, the cylinder 5 of assembly II is inserted inside shunting/Splitless injecting samples mouth weldment, repeat up and down
Wiping 10 to 20 times.
Step 4, drip washing and being dried: draw the acetone of 10mL to 20mL and normal hexane solvent washing injection port successively, treat point
The solvent of stream/Splitless injecting samples mouth evaporates into dry naturally.
It is an advantage of the current invention that:
(1) shunting of the present invention/Splitless injecting samples mouth clean external member have easy and simple to handle, clean the most notable
Advantage；
(2) assembly I bristle lengths of the present invention is slightly larger than shunting/Splitless injecting samples mouth weldment internal diameter, is dipping in
The residual contaminants inside weldment can be cleaned by External Force Acting after taking organic solvent；
(3) after in assembly II of the present invention, the groove part of cylinder fills the absorbent cotton dipping organic solvent, cotton
Loop diameter is slightly larger than shunting/Splitless injecting samples mouth internal diameter, under external force can high laminating degree by inside weldment through assembly I
The thorough wiped clean of residual contaminants after scrubbing, simultaneously because groove 7 exists the upper and lower age of a draught animal 6 and 8, absorbent cotton welds at injection port
Do not come off when moving up and down inside fitting.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of assembly I；
Fig. 2 is the schematic diagram of assembly II；
Fig. 3 is the schematic diagram that shunting/Splitless injecting samples mouth cleans external member.
Detailed description of the invention
For the openest rather than restriction present invention, below in conjunction with example, the present invention is described in further detail.
Embodiment 1
The cleaning external member of a kind of shunting/Splitless injecting samples mouth, including assembly I and assembly II, wherein assembly I is by ring 1, gold
Belong to bar 2 and bristle 3 forms；Assembly II is made up of cylindrical handle 4 and cylinder 5, it is characterised in that cylinder 5 lower end of assembly II
There is a groove 7 in part, this groove exists the upper age of a draught animal 6 and the lower age of a draught animal 8.
Wherein,
Described assembly I is positioned at the bristle lengths of metallic rod 2 one side isometric and for 3mm.
A diameter of 5mm of the cylinder 5 of described assembly II.
The using method of the cleaning external member of a kind of shunting/Splitless injecting samples mouth comprises the following steps:
Step one, prepares: by the dottle pin of shunting/Splitless injecting samples mouth, round section joint ring, bushing pipe, chromatographic column, reducing nut etc.
Shunting/Splitless injecting samples mouth accessory is removed, and exposes shunting/Splitless injecting samples mouth；
Step 2, scrubs: place a beaker in the lower end of injection port, dips methanol with assembly I and scrubs shunting/no up and down
Inside split sampling mouth weldment, repeat 10；Afterwards, dip acetone solvent with assembly I and scrub shunting/Splitless injecting samples mouth up and down
Inside weldment, repeat 10；
Step 3, wiping: fill up the groove 7 of assembly II after absorbent cotton is dipped methanol, the cylinder 5 of assembly II is inserted point
Inside stream/Splitless injecting samples mouth weldment, repeat wiping 10 up and down, discard absorbent cotton；Afterwards, fill out after absorbent cotton being dipped acetone
The groove 7 of full assembly II, inserts inside shunting/Splitless injecting samples mouth weldment by the cylinder 5 of assembly II, repeats wiping 10 up and down
Secondary.
Step 4, drip washing and being dried: draw acetone and the normal hexane solvent washing injection port of 10mL successively, to be shunted/no
The solvent of split sampling mouth evaporates into dry naturally.
Embodiment 2
The cleaning external member of a kind of shunting/Splitless injecting samples mouth, including assembly I and assembly II, wherein assembly I is by ring 1, gold
Belong to bar 2 and bristle 3 forms；Assembly II is made up of cylindrical handle 4 and cylinder 5, it is characterised in that cylinder 5 lower end of assembly II
There is a groove 7 in part, this groove exists the upper age of a draught animal 6 and the lower age of a draught animal 8.
Wherein,
Described assembly I is positioned at the bristle lengths of metallic rod 2 one side isometric and for 4mm.
A diameter of 6mm of the cylinder 5 of described assembly II.
The using method of the cleaning external member of a kind of shunting/Splitless injecting samples mouth comprises the following steps:
Step one, prepares: by the dottle pin of shunting/Splitless injecting samples mouth, round section joint ring, bushing pipe, chromatographic column, reducing nut etc.
Shunting/Splitless injecting samples mouth accessory is removed, and exposes shunting/Splitless injecting samples mouth；
Step 2, scrubs: place a beaker in the lower end of injection port, dips methanol with assembly I and scrubs shunting/no up and down
Inside split sampling mouth weldment, it is repeated 20 times；Afterwards, dip acetone solvent with assembly I and scrub shunting/Splitless injecting samples up and down
Inside mouth weldment, it is repeated 20 times；
Step 3, wiping: fill up the groove 7 of assembly II after absorbent cotton is dipped methanol, the cylinder 5 of assembly II is inserted point
Inside stream/Splitless injecting samples mouth weldment, repeat wiping 20 times up and down, discard absorbent cotton；Afterwards, after absorbent cotton being dipped acetone
Fill up the groove 7 of assembly II, the cylinder 5 of assembly II is inserted inside shunting/Splitless injecting samples mouth weldment, repeat wiping up and down
20 times.
Step 4, drip washing and being dried: draw acetone and the normal hexane solvent washing injection port of 20mL successively, to be shunted/no
The solvent of split sampling mouth evaporates into dry naturally.
Embodiment described above only have expressed embodiments of the present invention, and it describes more concrete and detailed, but can not
Therefore the restriction to the scope of the claims of the present invention it is interpreted as.It should be pointed out that, for the ordinary skill in the art,
Without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these belong to the protection model of the present invention
Enclosing, the protection domain of patent the most of the present invention should be as the criterion with claims.
Claims (4)
1. a cleaning external member for shunting/Splitless injecting samples mouth, including assembly I and assembly II, wherein assembly I is by ring (1), gold
Belong to bar (2) and bristle (3) composition；Assembly II is made up of cylindrical handle (4) and cylinder (5), it is characterised in that the circle of assembly II
There is a groove (7) in post (5) end portion, this groove exists the upper age of a draught animal (6) and the lower age of a draught animal (8).
The cleaning external member of a kind of shunting/Splitless injecting samples mouth the most as claimed in claim 1, it is characterised in that in described assembly I
It is positioned at the unilateral bristle lengths of metallic rod (2) isometric and for 3mm to 4mm.
The cleaning external member of a kind of shunting/Splitless injecting samples mouth the most as claimed in claim 1, it is characterised in that described assembly II
A diameter of 5mm to 6mm of cylinder (5).
4., according to claim 1, the using method of the cleaning external member of a kind of shunting/Splitless injecting samples mouth comprises the following steps:
Step one, prepares: by sample introductions such as the dottle pin of shunting/Splitless injecting samples mouth, round section joint ring, bushing pipe, chromatographic column, reducing nuts
Mouth accessory is removed, and exposes shunting/Splitless injecting samples mouth；
Step 2, scrubs: places a beaker in the lower end of shunting/Splitless injecting samples mouth, dips methanol with assembly I and scrub up and down
Inside shunting/Splitless injecting samples mouth weldment, repeat 10 to 20 times；Afterwards, dip acetone solvent with assembly I to scrub up and down point
Inside stream/Splitless injecting samples mouth weldment, repeat 10 to 20 times；
Step 3, wiping: fill up the groove (7) of assembly II after absorbent cotton is dipped methanol, the cylinder (5) of assembly II is inserted and divides
Inside stream/Splitless injecting samples mouth weldment, repeat wiping 10 to 20 times up and down, discard absorbent cotton；Afterwards, absorbent cotton is dipped third
Fill up the groove (7) of assembly II after ketone, the cylinder (5) of assembly II is inserted inside shunting/Splitless injecting samples mouth weldment, up and down
Repeat wiping 10 to 20 times.
Step 4, drip washing is with dry: draw acetone and the normal hexane solvent washing shunting/Splitless injecting samples of 10mL to 20mL successively
Mouthful, the solvent of to be shunted/Splitless injecting samples mouth evaporates into dry naturally.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610820626.6A CN106213764A (en) | 2016-09-13 | 2016-09-13 | The cleaning external member of a kind of shunting/Splitless injecting samples mouth and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610820626.6A CN106213764A (en) | 2016-09-13 | 2016-09-13 | The cleaning external member of a kind of shunting/Splitless injecting samples mouth and using method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106213764A true CN106213764A (en) | 2016-12-14 |
Family
ID=58074882
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610820626.6A Pending CN106213764A (en) | 2016-09-13 | 2016-09-13 | The cleaning external member of a kind of shunting/Splitless injecting samples mouth and using method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106213764A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002086362A (en) * | 2000-09-12 | 2002-03-26 | Masao Nishiki | Cup-shaped rotary brush and its manufacturing method |
| JP2010022694A (en) * | 2008-07-23 | 2010-02-04 | Kowa Co Ltd | Brush |
| CN201415196Y (en) * | 2009-06-11 | 2010-03-03 | 张思哲 | Wiper convenient for cleaning |
| CN202891014U (en) * | 2012-10-31 | 2013-04-24 | 广东明朗生活用品制造厂有限公司 | Open-close type toilet brush seat frame |
| CN104544927A (en) * | 2013-10-25 | 2015-04-29 | 大连民族学院 | Bottle brush for chemical experiment |
-
2016
- 2016-09-13 CN CN201610820626.6A patent/CN106213764A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002086362A (en) * | 2000-09-12 | 2002-03-26 | Masao Nishiki | Cup-shaped rotary brush and its manufacturing method |
| JP2010022694A (en) * | 2008-07-23 | 2010-02-04 | Kowa Co Ltd | Brush |
| CN201415196Y (en) * | 2009-06-11 | 2010-03-03 | 张思哲 | Wiper convenient for cleaning |
| CN202891014U (en) * | 2012-10-31 | 2013-04-24 | 广东明朗生活用品制造厂有限公司 | Open-close type toilet brush seat frame |
| CN104544927A (en) * | 2013-10-25 | 2015-04-29 | 大连民族学院 | Bottle brush for chemical experiment |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161214 |