CN106206474A - A kind of encapsulating structure improving Frit packaging machinery intensity and method for packing thereof - Google Patents

A kind of encapsulating structure improving Frit packaging machinery intensity and method for packing thereof Download PDF

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Publication number
CN106206474A
CN106206474A CN201610794325.0A CN201610794325A CN106206474A CN 106206474 A CN106206474 A CN 106206474A CN 201610794325 A CN201610794325 A CN 201610794325A CN 106206474 A CN106206474 A CN 106206474A
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China
Prior art keywords
frit
quantum
cover
inorganic
film layer
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CN201610794325.0A
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CN106206474B (en
Inventor
李春霞
李伟丽
甘帅燕
吴伟力
彭兆基
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Kunshan Govisionox Optoelectronics Co Ltd
Kunshan Guoxian Photoelectric Co Ltd
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Kunshan Guoxian Photoelectric Co Ltd
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Priority to CN201610794325.0A priority Critical patent/CN106206474B/en
Publication of CN106206474A publication Critical patent/CN106206474A/en
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L23/00Details of semiconductor or other solid state devices
    • H01L23/28Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection
    • H01L23/29Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection characterised by the material, e.g. carbon
    • H01L23/291Oxides or nitrides or carbides, e.g. ceramics, glass
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/50Assembly of semiconductor devices using processes or apparatus not provided for in a single one of the subgroups H01L21/06 - H01L21/326, e.g. sealing of a cap to a base of a container
    • H01L21/56Encapsulations, e.g. encapsulation layers, coatings
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L23/00Details of semiconductor or other solid state devices
    • H01L23/28Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection
    • H01L23/29Encapsulations, e.g. encapsulating layers, coatings, e.g. for protection characterised by the material, e.g. carbon
    • H01L23/298Semiconductor material, e.g. amorphous silicon

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Joining Of Glass To Other Materials (AREA)
  • Laser Beam Processing (AREA)

Abstract

The invention discloses a kind of encapsulating structure improving Frit packaging machinery intensity and method for packing thereof, substrate makes metallic diaphragm;Packaging area at cover-plate glass prepares Frit encapsulated layer and inorganic-quantum-dot nano thin-film layer;Cover-plate glass is docked with the packaging area of substrate;Irradiated the packaging area of cover-plate glass and substrate by light source, make frit seal between cover-plate glass and substrate;The present invention uses inorganic-quantum-dot nano thin-film layer to strengthen Frit package strength, melted Frit encapsulated layer penetrates into the gap of nano thin-film interlayer, form frit and nano thin-film layer composite strengthening system, increase heat seal strength, improve the adhesion of Frit encapsulated layer and cover-plate glass;Meanwhile, the even compact thin layer that inorganic-quantum-dot nano thin-film layer is formed can play cushion and the effect of release stress when cover-plate glass is squeezed;Quantum dot can also increase laser absorption, can use less laser welding Frit encapsulated layer, reduces the Thermal Stress of screen body.

Description

A kind of encapsulating structure improving Frit packaging machinery intensity and method for packing thereof
Technical field
The present invention relates to Display Technique field, specifically, relate to a kind of encapsulation knot improving Frit packaging machinery intensity Structure and method for packing thereof.
Background technology
Display screen uses Frit (frit) encapsulation and thin-film package two kinds at present.Frit is printed on lid by Frit encapsulation On glass sheet, use laser beam to move heated frit fusing and form air hermetic encapsulation, frit melted shape on the glass substrate Become one layer of seal.The defect using this packaged type is that frit is not enough with the adhesion of lid surface, it is impossible to provide foot Enough mechanical strengths;Simultaneously as the local insufficient strength of two pieces of glass contact, the most chipping when being squeezed and impact Etc. problem.
Chinese patent literature CN 103102075 discloses and a kind of uses frit to carry out the method and device sealed, should Frit includes that seal glass and filler, described filler include inorganic-quantum-dot material, is first disperseed in the carrier by frit, Obtain glass cement;Glass cement is deposited on the packaging area of first substrate;Glass cement on packaging area is preheated, obtains Obtain unorganic glass;By second substrate and first substrate pressing;Laser is used to irradiate encapsulation area of the pattern, so that unorganic glass melts Melt rear shape packaged glass, the region of the packaging area encirclement of described first substrate is sealed.Above-mentioned patent documentation is by nothing Machine quanta point material is entrained in frit the method carrying out being pre-mixed, and in encapsulation process, the frit to mixing carries out laser Irradiation makes its melted reaching encapsulate purpose, and the mass fraction of the inorganic-quantum-dot material in frit is only 0.1-10%, although The potting ability of encapsulating face can be strengthened, but when glass cover-plate is extruded by vertical mechanical, it is difficult to effectively release extruding should Power, easily causes extruding and ruptures.
Summary of the invention
Therefore, the present invention is to solve that display screen body cannot effectively discharge glass when by front extruding or impact Extrusion stress and impact stress, thus cause the frangible phenomenon that ruptures, the invention provides a kind of raising Frit packaging machinery strong The encapsulating structure of degree and method for packing thereof.
The technical scheme used is as follows:
On the one hand, the invention provides a kind of encapsulating structure improving Frit packaging machinery intensity, include substrate, gold successively Belonging to film layer, Frit encapsulated layer and cover-plate glass, described Frit encapsulated layer is positioned at the packaging area of described cover-plate glass, described Frit The side of encapsulated layer is additionally provided with inorganic-quantum-dot nano thin-film layer, and described inorganic-quantum-dot nano thin-film layer is positioned at described Frit envelope Between dress layer and described cover-plate glass, or described inorganic-quantum-dot nano thin-film layer is positioned at described Frit encapsulated layer and metal film Between Ceng.
On the other hand, present invention also offers a kind of method for packing improving Frit packaging machinery intensity, substrate is made Make metallic diaphragm;Packaging area at cover-plate glass prepares Frit encapsulated layer and inorganic-quantum-dot nano thin-film layer;By cover plate glass Glass docks with the packaging area of substrate;Irradiated the packaging area of cover-plate glass and substrate by light source, make cover-plate glass and substrate Between frit seal.
Cover-plate glass is prepared inorganic-quantum-dot nano thin-film layer, then prepares on inorganic-quantum-dot nano thin-film layer Frit encapsulated layer, docks the metallic diaphragm on substrate with Frit encapsulated layer, is irradiated by LASER Light Source and makes cover-plate glass and base Frit seal is reached between plate.
The thickness of prepared inorganic-quantum-dot nano thin-film layer is 100nm~1000nm.
Cover-plate glass is prepared Frit encapsulated layer, on Frit encapsulated layer, then prepares inorganic-quantum-dot nano thin-film Layer, the metallic diaphragm on substrate dock with inorganic-quantum-dot nano thin-film layer, by LASER Light Source irradiation make cover-plate glass and Frit seal is reached between substrate.
The thickness of prepared inorganic-quantum-dot nano thin-film layer is 500nm~2000nm.
The thickness of prepared Frit encapsulated layer is 4~6 μm.
The described method preparing inorganic-quantum-dot nano thin-film layer includes vapour deposition process, 3D impact system, inkjet printing One in method and spin-coating method.
The prepared columnar fiber in inorganic-quantum-dot nano thin-film layer is perpendicular to cover-plate glass.
Described inorganic-quantum-dot nano thin-film layer includes cadmium selenide, zinc sulfide, zinc selenide, Aska-Rid., cadmium telluride, oxidation At least one in zinc.
Technical solution of the present invention, has the advantage that
A. the present invention uses inorganic-quantum-dot nano thin-film layer to strengthen Frit package strength, inorganic-quantum-dot nano thin-film layer Being placed between cover-plate glass and substrate, inorganic-quantum-dot nano thin-film layer is similar to columnar fiber, plays enhancing again with cover-plate glass The effect closed.Melted Frit encapsulated layer penetrates into the gap of nano thin-film interlayer, forms Frit encapsulated layer and nano thin-film Layer composite strengthening system, increases heat seal strength, and the uneven surface of nano-particle provides a big adsorption area, improves Frit Encapsulated layer and the adhesion of cover-plate glass;Meanwhile, the even compact thin layer that inorganic-quantum-dot nano thin-film layer is formed can be Cushion and the effect of release stress is played when cover-plate glass is squeezed;Quantum dot can also increase laser absorption, can use Less laser welding Frit encapsulated layer, reduces the Thermal Stress of screen body.
B. the present invention will increase inorganic-quantum-dot nano thin-film layer between cover-plate glass and substrate, be received by inorganic-quantum-dot Rice thin layer strengthens the adhesion between cover plate and frit and heat seal strength, improves the machinery of sealant between cover-plate glass and substrate Intensity, inorganic-quantum-dot nano thin-film layer can play the effect of cushion, and can increase laser absorption, reduces laser merit Rate.
Accompanying drawing explanation
In order to be illustrated more clearly that the specific embodiment of the invention or technical scheme of the prior art, below will be to specifically In embodiment or description of the prior art, the required accompanying drawing used is briefly described, it should be apparent that, in describing below Accompanying drawing is some embodiments of the present invention, for those of ordinary skill in the art, before not paying creative work Put, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the structural representation of the first embodiment provided by the present invention;
Fig. 2 is the structural representation of the second embodiment provided by the present invention;
Fig. 3 is the inorganic-quantum-dot nano thin-film layer stress buffer schematic diagram when being extruded by cover-plate glass;
Fig. 4 is the Displacements Distribution figure that cover-plate glass moves down when by external world's extruding.
Description of reference numerals:
1-cover-plate glass;2-Frit encapsulated layer;3-inorganic-quantum-dot nano thin-film layer;4-metallic diaphragm;5-substrate.
Detailed description of the invention
Below in conjunction with accompanying drawing, technical scheme is clearly and completely described, it is clear that described enforcement Example is a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, ordinary skill The every other embodiment that personnel are obtained under not making creative work premise, broadly falls into the scope of protection of the invention.
A kind of encapsulating structure improving Frit packaging machinery intensity provided by the present invention, as illustrated in fig. 1 and 2, wraps successively Including substrate 5, metallic diaphragm 4, Frit encapsulated layer 2 and cover-plate glass 1, Frit encapsulated layer 2 is positioned at the packaging area of cover-plate glass 1, The side of Frit encapsulated layer 2 is additionally provided with inorganic-quantum-dot nano thin-film layer 3, and inorganic-quantum-dot nano thin-film layer 3 is positioned at Frit envelope Between dress layer 2 and cover-plate glass 1, or inorganic-quantum-dot nano thin-film layer 3 is between Frit encapsulated layer 2 and metallic diaphragm 4.
Being wherein the first version provided by the present invention in Fig. 1, inorganic-quantum-dot nano thin-film layer 3 therein is positioned at Between Frit encapsulated layer 2 and cover-plate glass 1.
And Fig. 2 is the second version provided by the present invention, inorganic-quantum-dot nano thin-film layer 3 therein is positioned at Between Frit encapsulated layer 2 and metallic diaphragm 4.
Here substrate is 0LED substrate, can be chip provide electrically connect, protect, support, dispel the heat, the effect such as assembling, with Realize many pinizations, reduce encapsulating products volume, improve electrical property and the mesh of thermal diffusivity, VHD or multi-chip module 's.
Below above two encapsulating structure is described in detail.
Embodiment 1
As it is shown in figure 1, make metallic diaphragm 4 on the substrate 5, cover-plate glass 1 is prepared inorganic-quantum-dot nano thin-film Layer 3, then prepares Frit encapsulated layer 2, by the metallic diaphragm 4 on substrate 5 and cover plate glass on inorganic-quantum-dot nano thin-film layer 3 Frit encapsulated layer 2 on glass 1 docks, and is irradiated by light source and makes to reach frit seal between cover-plate glass 1 and substrate 5.The most logical Cross the packaging area of laser welding method seal cover board glass 1 and substrate 5.
The thickness of wherein prepared inorganic-quantum-dot nano thin-film layer 3 is 100nm~1000nm, prepared Frit envelope The thickness of dress layer 2 is 4~6 μm;Preferably inorganic-quantum-dot nano thin-film layer 3 thickness is 800nm, preferred Frit encapsulated layer 2 Thickness is 5 μm.
The method preparing inorganic-quantum-dot nano thin-film layer employed in it includes vapour deposition process, 3D impact system, spray One in ink impact system and spin-coating method.
The present invention is when preparing inorganic-quantum-dot nano thin-film layer 3, and its columnar fiber presents and is perpendicular to cover-plate glass 1 and sets Put.
Inorganic-quantum-dot nano thin-film layer 3 therein includes cadmium selenide, zinc sulfide, zinc selenide, Aska-Rid., cadmium telluride, oxygen Change at least one in zinc.
The present invention uses inorganic-quantum-dot nano thin-film layer 3 for nanorod structure to strengthen Frit package strength, inorganic amount Son point nano thin-film layer 3 is similar to columnar fiber, plays with Frit encapsulated layer 2 and strengthens compound effect.Melted Frit encapsulated layer 2 Penetrate into the gap of nano thin-film interlayer, form Frit encapsulated layer 2 and the composite strengthening of inorganic-quantum-dot nano thin-film layer 3 System, increases heat seal strength;Owing to the uneven surface of nano-particle provides a big adsorption area, improve Frit encapsulated layer 2 with the adhesion of cover-plate glass 1;Meanwhile, the even compact thin layer that inorganic-quantum-dot nano thin-film layer 3 is formed can be at glass Cushion and the effect of release stress is played when being squeezed;Inorganic-quantum-dot can also increase laser absorption, can use less Laser welding Frit encapsulated layer 2, reduces the Thermal Stress of screen body.
Embodiment 2
As in figure 2 it is shown, as different from Example 1: make metallic diaphragm 4 on the substrate 5, on cover-plate glass 1 first Preparation Frit encapsulated layer 2, then prepares inorganic-quantum-dot nano thin-film layer 3 on Frit encapsulated layer 2, then by the gold on substrate 5 Belong to film layer 4 to dock with the inorganic-quantum-dot nano thin-film layer 3 on cover-plate glass 1, irradiated by light source and make cover-plate glass 1 and substrate Reach frit seal between 5, prepare structure as shown in Figure 2.Preferably by laser welding method seal cover board glass 1 and substrate 5 Packaging area.
The thickness of prepared inorganic-quantum-dot nano thin-film layer 3 is 500nm~2000nm, prepared Frit encapsulated layer The thickness of 2 is 4~6 μm, and preferred inorganic-quantum-dot nano thin-film layer 3 thickness is 1000nm, preferred Frit encapsulated layer 2 thickness It is 5 μm.
In above-mentioned two embodiments, between glass cover-plate 1 and substrate 5, increase inorganic-quantum-dot nano thin-film layer 3, by inorganic Quantum dot nano thin layer 3 strengthens adhesion and the heat seal strength of cover-plate glass 1 and Frit encapsulated layer 2, improve cover-plate glass 1 with The mechanical strength of 5 sealants of substrate, inorganic-quantum-dot nano thin-film layer 3 can play the effect of cushion, and can increase Laser absorption, reduces laser power.
Fig. 3 represents the inorganic-quantum-dot nano thin-film layer stress buffer schematic diagram when being extruded by glass cover-plate.From It can be seen that the inorganic-quantum-dot nano thin-film layer between cover-plate glass and substrate defines even compact thin film in figure Layer, plays cushion and the effect of release stress when cover-plate glass is squeezed.
Fig. 4 represent cover-plate glass by the external world extruding time, the Displacements Distribution situation moved down.It will be seen that In one stage (between 0~0.1), the displacement of cover-plate glass keeps the least state, is similar to 0, represents that inorganic-quantum-dot is received The extrusion stress of rice thin layer buffering release cap glass sheet;Second stage (> 0.1), the displacement of cover-plate glass sharply increases, Representing that stress has exceeded the release limit of inorganic-quantum-dot nano thin-film layer, quantum dot has been pressed into inside glass, and glass ruptures.
Without inorganic-quantum-dot nano thin-film layer, extrusion stress discharges nowhere, is equivalent to second stage in Fig. 4, glass Glass directly contacts, and is easily broken.
Obviously, above-described embodiment is only for clearly demonstrating example, and not restriction to embodiment.Right For those of ordinary skill in the field, can also make on the basis of the above description other multi-form change or Variation.Here without also cannot all of embodiment be given exhaustive.And the obvious change thus extended out or Change among still in the protection domain of the invention.

Claims (10)

1. improve an encapsulating structure for Frit packaging machinery intensity, include substrate, metallic diaphragm, Frit encapsulated layer and lid successively Glass sheet, described Frit encapsulated layer is positioned at the packaging area of described cover-plate glass, it is characterised in that the one of described Frit encapsulated layer Side is additionally provided with inorganic-quantum-dot nano thin-film layer, and described inorganic-quantum-dot nano thin-film layer is positioned at described Frit encapsulated layer with described Cover-plate glass between, or described inorganic-quantum-dot nano thin-film layer is between described Frit encapsulated layer and metallic diaphragm.
2. the method for packing improving Frit packaging machinery intensity, it is characterised in that make metallic diaphragm on substrate;At lid The packaging area of glass sheet prepares Frit encapsulated layer and inorganic-quantum-dot nano thin-film layer;Encapsulation region by cover-plate glass Yu substrate Territory is docked;Irradiated the packaging area of cover-plate glass and substrate by light source, make frit seal between cover-plate glass and substrate.
Method for packing the most according to claim 2, it is characterised in that prepare inorganic-quantum-dot nanometer thin on cover-plate glass Film layer, then prepares Frit encapsulated layer on inorganic-quantum-dot nano thin-film layer, is encapsulated with Frit by the metallic diaphragm on substrate Layer docking, is irradiated by LASER Light Source and makes to reach between cover-plate glass and substrate frit seal.
Method for packing the most according to claim 3, it is characterised in that the thickness of prepared inorganic-quantum-dot nano thin-film layer Degree is 100nm~1000nm.
Method for packing the most according to claim 2, it is characterised in that prepare Frit encapsulated layer on cover-plate glass, then Frit encapsulated layer is prepared inorganic-quantum-dot nano thin-film layer, by the metallic diaphragm on substrate and inorganic-quantum-dot nano thin-film Layer docking, is irradiated by LASER Light Source and makes to reach between cover-plate glass and substrate frit seal.
Method for packing the most according to claim 5, it is characterised in that the thickness of prepared inorganic-quantum-dot nano thin-film layer Degree is 500nm~2000nm.
Method for packing the most according to claim 2, it is characterised in that the thickness of prepared Frit encapsulated layer is 4~6 μ m。
Method for packing the most according to claim 7, it is characterised in that described inorganic-quantum-dot nano thin-film layer of preparing Method includes the one in vapour deposition process, 3D impact system, ink-jet printing process and spin-coating method.
Method for packing the most according to claim 8, it is characterised in that in prepared inorganic-quantum-dot nano thin-film layer Columnar fiber is perpendicular to cover-plate glass.
Method for packing the most according to claim 9, it is characterised in that described inorganic-quantum-dot nano thin-film layer includes At least one in cadmium selenide, zinc sulfide, zinc selenide, Aska-Rid., cadmium telluride, zinc oxide.
CN201610794325.0A 2016-08-31 2016-08-31 packaging structure for improving Frit packaging mechanical strength and packaging method thereof Active CN106206474B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114675439A (en) * 2022-03-30 2022-06-28 广州华星光电半导体显示技术有限公司 Display panel, preparation method thereof and display device

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TW201105601A (en) * 2009-06-30 2011-02-16 Guardian Industries Frit or solder glass compound including beads, and assemblies incorporating the same
TW201133434A (en) * 2010-03-31 2011-10-01 Au Optronics Corp Display panel package structure and fabricating method thereof
CN103258971A (en) * 2013-04-27 2013-08-21 上海和辉光电有限公司 Encapsulation method and device of display element
CN104409663A (en) * 2014-11-12 2015-03-11 京东方科技集团股份有限公司 Encapsulating method, encapsulating structure and display device
TW201521194A (en) * 2013-11-28 2015-06-01 Innolux Corp Organic light emitting diode display panel and method for manufacturing the same
CN105810796A (en) * 2016-04-21 2016-07-27 深圳市华星光电技术有限公司 Quantum-dot material glass plate and fabrication method thereof

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Publication number Priority date Publication date Assignee Title
CN101179113A (en) * 2006-11-07 2008-05-14 康宁股份有限公司 Hermetic seal for light emitting display device, method, and apparatus
TW201105601A (en) * 2009-06-30 2011-02-16 Guardian Industries Frit or solder glass compound including beads, and assemblies incorporating the same
TW201133434A (en) * 2010-03-31 2011-10-01 Au Optronics Corp Display panel package structure and fabricating method thereof
CN103258971A (en) * 2013-04-27 2013-08-21 上海和辉光电有限公司 Encapsulation method and device of display element
TW201521194A (en) * 2013-11-28 2015-06-01 Innolux Corp Organic light emitting diode display panel and method for manufacturing the same
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CN105810796A (en) * 2016-04-21 2016-07-27 深圳市华星光电技术有限公司 Quantum-dot material glass plate and fabrication method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114675439A (en) * 2022-03-30 2022-06-28 广州华星光电半导体显示技术有限公司 Display panel, preparation method thereof and display device
CN114675439B (en) * 2022-03-30 2023-11-28 广州华星光电半导体显示技术有限公司 Display panel, preparation method thereof and display device

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Denomination of invention: A packaging structure and method for improving the mechanical strength of frit packaging

Effective date of registration: 20201221

Granted publication date: 20191213

Pledgee: Xin Xin Finance Leasing Co.,Ltd.

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