CN106198129A - A kind of example reaction generates gas collector - Google Patents
A kind of example reaction generates gas collector Download PDFInfo
- Publication number
- CN106198129A CN106198129A CN201610538752.2A CN201610538752A CN106198129A CN 106198129 A CN106198129 A CN 106198129A CN 201610538752 A CN201610538752 A CN 201610538752A CN 106198129 A CN106198129 A CN 106198129A
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- CN
- China
- Prior art keywords
- catcher
- collecting pipe
- sample
- tube
- telescoping tube
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/24—Suction devices
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The present invention relates to gas collector, especially a kind of example reaction generates gas collector, including solution tank, groove lid, catcher, telescoping tube, fixing groove, ultrasound wave pot, rubber sealing boot, support, exhaust tube, sample hanged hook, flexible knob, wherein catcher collecting pipe part indicates scale, can measure the volume collecting gas, ultrasound wave pot can make catcher gather up inwall bubbles attached by sonic oscillation.It is an advantage of the invention that integrated gas collector, make collection and confinement of gases realize quantization, standardization and precision.
Description
Technical field
The present invention relates to gas collector, especially a kind of reacting gas collection device.
Background technology
Collection and confinement of gases relates in chemistry subject research field more, but quantifies device and rarely have report always.Conventional combination
The gas collector of formula cannot ensure its reliability and sealing, collects gas and is difficult to quantify.During collection and confinement of gases also
It is frequently present of the problems such as bubble inwall attachment, affects the accuracy of collection and confinement of gases, and operate with process very complicated, unfavorable
Expansion in experiment.
Summary of the invention
It is an object of the invention to realize collection and confinement of gases quantify, strengthen collection and confinement of gases operation integration, and the process of collection
High-speeding, improve the accuracy of collection and confinement of gases process and reliability simultaneously.
For achieving the above object, the technical scheme is that a kind of example reaction of employing generates gas collector, bag
Include solution tank 1, groove lid 2, catcher 3, telescoping tube 4, fixing groove 5, ultrasound wave pot 6, rubber sealing boot 7, support 8, exhaust tube 9,
Sample hanged hook 10, flexible knob 11；Described catcher 3 includes collecting pipe and collecting hood two parts, wherein collecting pipe part mark
Show scale；Described exhaust tube 9 capacity is at least above the capacity of catcher 3 collecting pipe；Described sample hanged hook 10 is gluing in collection
Device 3 collecting hood inwall；Described ultrasound wave pot 6 connects with solution tank 1 air tight communication；Described telescoping tube 4 and solution tank 1 air tight communication
Connect；It is tightly connected by rubber tube between described telescoping tube 4 and exhaust tube 9；Described groove lid 2 is logical spills catcher 3, is placed on solution
On groove 1.
Described telescoping tube 4 uses polytetrafluoroethylmaterial material, and requires that scalable each joint sealing joint is good.
The maximum height of described telescoping tube 4 is less than the top scale of catcher 3 collecting pipe part, and minimum altitude does not surpasses
Cross the height of catcher 3 collecting hood part.
Described sample hangs 10 hooks and uses polytetrafluoroethylmaterial material to make.
A kind of example reaction gas collection method, Main process steps is as follows: the first step, adds solution, sample in solution tank 1
Product are suspended on sample hanged hook 10, and catcher 3 buckles in solution, are placed in fixing groove 5；Second step, telescoping tube 4 is elongated to receive
Storage 3 collecting pipe top, exhaust tube 9 bleeds, and in catcher 3, solution rises at collecting pipe top scale；3rd step, shrinks
Telescoping tube 4, mobile collectors 3 is placed in collection gas in ultrasound wave pot 6, and time mobile, catcher 3 collecting hood mouth is in below liquid level；
4th step, during reading, opens ultrasound wave pot 6, supersound process complete after reading.
The beneficial effects of the present invention is: realize collection and confinement of gases and quantify；Realize the integration of collection and confinement of gases process；Effectively process
Bubble inwall attachment issue during collection and confinement of gases.
Accompanying drawing explanation
Fig. 1, Fig. 2, Fig. 3 are the schematic diagrams of the present invention, and wherein Fig. 2 represents the example reaction preparatory stage, and Fig. 3 represents that sample is anti-
The collection and confinement of gases stage should be generated.
In figure: solution tank 1, groove lid 2, catcher 3, telescoping tube 4, fixing groove 5, ultrasound wave pot 6, rubber sealing boot 7, support
8, exhaust tube 9, sample hanged hook 10, flexible knob 11.
Fig. 4 is the schematic diagram of catcher of the present invention.
Detailed description of the invention
In conjunction with Fig. 1, Fig. 2, Fig. 3, Fig. 4, the specific embodiment of the invention is further described: provide according to the present invention
Technical scheme, a kind of reacting gas collection device, including solution tank 1, groove lid 2, catcher 3, telescoping tube 4, fixing groove 5, ultrasonic
Ripple pot 6, rubber sealing boot 7, support 8, exhaust tube 9, sample hanged hook 10, flexible knob 11；Described catcher 3 includes collecting pipe
With collecting hood two parts, wherein collecting pipe part indicates scale；Described exhaust tube 9 capacity is at least above catcher 3 collecting pipe
Capacity；Described sample hanged hook 10 is gluing in catcher 3 collecting hood inwall；Described ultrasound wave pot 6 and solution tank 1 air tight communication phase
Connect；Described telescoping tube 4 connects with solution tank 1 air tight communication；It is tightly connected by rubber tube between described telescoping tube 4 and exhaust tube 9；
Described groove lid 2 is logical spills catcher 3, is placed on solution tank 1.
Described telescoping tube 4 uses polytetrafluoroethylmaterial material, and requires that scalable each joint sealing joint is good.
The maximum height of described telescoping tube 4 is less than the top scale of catcher 3 collecting pipe part, and minimum altitude does not surpasses
Cross the height of catcher 3 collecting hood part.
Described sample hangs 10 hooks and uses polytetrafluoroethylmaterial material to make.
A kind of example reaction gas collection method, Main process steps is as follows: the first step, adds solution, sample in solution tank 1
Product are suspended on sample hanged hook 10, and catcher 3 buckles in solution, are placed in fixing groove 5；Second step, telescoping tube 4 is elongated to receive
Storage 3 collecting pipe top, exhaust tube 9 bleeds, and in catcher 3, solution rises at collecting pipe top scale；3rd step, shrinks
Telescoping tube 4, mobile collectors 3 is placed in collection gas in ultrasound wave pot 6, and time mobile, catcher 3 collecting hood mouth is in below liquid level；
4th step, during reading, opens ultrasound wave pot 6, supersound process complete after reading.
The work process of the present invention is: at example reaction preparatory stage (Fig. 2), and sample is first suspended on sample hanged hook 10
Go up (schematic diagram that Fig. 1, Fig. 2, Fig. 3, Fig. 4 all do not indicate sample), then catcher 3 is put into fixing groove 5, to solution tank
Reaction solution is added in 1.Telescoping tube 4 is made to stretch to the highest sign scale of catcher 3 collecting pipe by flexible knob 11.Now
Bled by exhaust tube 9, make solution solution under the effect of pressure difference in catcher 3 increase, arrive catcher 3 collecting pipe
Top scale.Enter example reaction and generate collection and confinement of gases stage, the flexible knob 11 of regulation, make telescoping tube 4 retract original height shape
State.Take away groove lid 2, mobile gas catcher 3, put into ultrasound wave pot 6, moving process keeps catcher 3 collecting hood bottom begin
Eventually below the liquid level of solution in solution tank 1.After catcher 3 places, build groove lid 2 by position, hole, start collection and confinement of gases process.
When needing the scale registration reading catcher 3 collecting pipe, need to first open ultrasound wave pot, (interval mode of oscillation, shakes sonic oscillation
Swing total time less than 60 seconds), during concussion, hand steered good catcher 3, prevents inclination from skewing, and starts reading after having vibrated.
The beneficial effects of the present invention is: realize collection and confinement of gases and quantify, it is achieved the integration of collection and confinement of gases process, effectively process
Bubble inwall attachment issue during collection and confinement of gases.
Particular embodiments described above, has been carried out the purpose of the present invention, technical scheme and beneficial effect the most in detail
Describe in detail bright, be it should be understood that the specific embodiment that the foregoing is only the present invention, be not limited to invention, all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. done, should be included in the protection of the present invention
In the range of.
Claims (5)
1. a specimen reaction generates gas collector, it is characterised in that: include solution tank, groove lid, catcher, telescoping tube,
Fixing groove, ultrasound wave pot, rubber sealing boot, support, exhaust tube, sample hanged hook, flexible knob；Described catcher includes collecting
Pipe and collecting hood two parts, wherein collecting pipe part indicates scale；Described exhaust tube capacity is at least above catcher collecting pipe
Capacity；Described sample hanged hook is gluing in catcher collecting hood inwall；Described ultrasound wave pot connects with solution tank air tight communication；Institute
State telescoping tube to connect with solution tank air tight communication；It is tightly connected by rubber tube between described telescoping tube and exhaust tube；Described groove lid
Lead to and spill catcher, be placed on solution tank.
A kind of example reaction the most according to claim 1 generates gas collector, it is characterised in that: telescoping tube uses poly-
Tetrafluoroethene material, and require that scalable each joint sealing joint is good.
A kind of example reaction the most according to claim 1 generates gas collector, it is characterised in that: telescoping tube the highest
Highly less than the top scale of catcher collecting pipe, minimum altitude is less than the height of catcher collecting hood.
A kind of example reaction the most according to claim 1 generates gas collector, it is characterised in that: sample hanged hook is adopted
Make with polytetrafluoroethylmaterial material.
5. an example reaction gas collection method, uses a kind of example reaction described in claim 1 to generate collection and confinement of gases dress
Put, it is characterised in that: adding solution in the first step, solution tank, sample is suspended on sample hanged hook, and catcher buckles into solution
In, it is placed in fixing groove；Second step, telescopic tube is to catcher collecting pipe top, and exhaust tube is bled, in catcher on solution
It is raised at collecting pipe top scale；3rd step, shrinks telescoping tube, and mobile collectors collects gas in being placed in ultrasound wave pot, moves
Time dynamic, catcher collecting hood mouth is in below liquid level；4th step, during reading, opens ultrasound wave pot, supersound process complete after reading.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610538752.2A CN106198129A (en) | 2016-07-11 | 2016-07-11 | A kind of example reaction generates gas collector |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610538752.2A CN106198129A (en) | 2016-07-11 | 2016-07-11 | A kind of example reaction generates gas collector |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106198129A true CN106198129A (en) | 2016-12-07 |
Family
ID=57472908
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610538752.2A Pending CN106198129A (en) | 2016-07-11 | 2016-07-11 | A kind of example reaction generates gas collector |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106198129A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101968477A (en) * | 2010-08-27 | 2011-02-09 | 华南理工大学 | Medical integrated magnesium alloy biodegradability gas-collection measurement device |
| CN103623611A (en) * | 2013-11-20 | 2014-03-12 | 国家环境分析测试中心 | Ultrasonic-assisted anti-blocking solid-phase extraction device |
-
2016
- 2016-07-11 CN CN201610538752.2A patent/CN106198129A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101968477A (en) * | 2010-08-27 | 2011-02-09 | 华南理工大学 | Medical integrated magnesium alloy biodegradability gas-collection measurement device |
| CN103623611A (en) * | 2013-11-20 | 2014-03-12 | 国家环境分析测试中心 | Ultrasonic-assisted anti-blocking solid-phase extraction device |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161207 |
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| WD01 | Invention patent application deemed withdrawn after publication |