CN106196899A - A kind of solid defoaming agent and preparation method thereof - Google Patents
A kind of solid defoaming agent and preparation method thereof Download PDFInfo
- Publication number
- CN106196899A CN106196899A CN201610498405.1A CN201610498405A CN106196899A CN 106196899 A CN106196899 A CN 106196899A CN 201610498405 A CN201610498405 A CN 201610498405A CN 106196899 A CN106196899 A CN 106196899A
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- CN
- China
- Prior art keywords
- parts
- defoaming agent
- waterglass
- dimethicone
- coke
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F26—DRYING
- F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
- F26B5/00—Drying solid materials or objects by processes not involving the application of heat
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- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
The invention discloses a kind of solid defoaming agent, it is made up of according to the raw material of weight portion following: 2 10 parts of coke, potassium iodide 3 13 parts, 2 10 parts of tetrabutyl phosphonium bromide phosphorus, fatty acid amide 17 parts, amido silicon oil 28 parts, trifluoroacetic acid 2 10 parts, epoxychloropropane 4 12 parts, waterglass 2 12 parts, dimethicone 3 13 parts.The present invention has easy to make, the advantage such as soaking effect good and antifoam performance is superior.
Description
Technical field
The present invention relates to a kind of defoamer, particularly relate to a kind of solid defoaming agent and preparation method thereof.
Background technology
At present, along with the development of science and technology, every field is all in fast development, and defoamer can be made in some goods
For compounding ingredient, absorb these goods moisture that filler used and foaming agent are brought in process of production, thus reach dry
Purpose, but existing defoamer selects the problem such as unreasonable because of its material, can not play the mesh preferably absorbing moisture
, bring the biggest problem to the processing of people.
Summary of the invention
In order to overcome the defect of above-mentioned prior art, it is an object of the invention to provide a kind of solid defoaming agent and preparation side thereof
Method.
The present invention takes techniques below scheme to realize: a kind of solid defoaming agent, by following former according to weight portion
Material composition: coke 2-10 part, potassium iodide 3-13 part, tetrabutyl phosphonium bromide phosphorus 2-10 part, fatty acid amide 1-7 part, amido silicon oil 2-8
Part, trifluoroacetic acid 2-10 part, epoxychloropropane 4-12 part, waterglass 2-12 part, dimethicone 3-13 part.
Above-mentioned a kind of solid defoaming agent, is made up of according to the raw material of weight portion following: coke 2-8 part, potassium iodide 3-11
Part, tetrabutyl phosphonium bromide phosphorus 2-8 part, fatty acid amide 1-5 part, amido silicon oil 2-6 part, trifluoroacetic acid 2-8 part, epoxychloropropane 4-
10 parts, waterglass 2-10 part, dimethicone 3-11 part.
Above-mentioned a kind of solid defoaming agent, is made up of according to the raw material of weight portion following: 6 parts of coke, potassium iodide 8 parts, and four
Butyl phosphonium bromide 6 parts, fatty acid amide 4 parts, amido silicon oil 5 parts, trifluoroacetic acid 6 parts, epoxychloropropane 8 parts, waterglass 7 parts,
Dimethicone 8 parts.
The preparation method of above-mentioned a kind of solid defoaming agent, comprises the steps of:
(1) the material number in claim 3 is chosen, by coke, potassium iodide, tetrabutyl phosphonium bromide phosphorus, fatty acid amide and amino
Silicone oil uses agitating device to mix, and mixing time is 20min, obtains mixture A；
(2) trifluoroacetic acid, epoxychloropropane, waterglass and dimethicone being carried out heat treated, heat time heating time is 30min,
Then being stirred by the material after heating, mixing time is 15min, obtains mixture B；
(3) mixture A and mixture B is carried out mixed processing, then mixed material is put in exsiccator and dry, obtain
Finished product.
The method have the advantages that in sum the present invention have easy to make, soaking effect good and defoaming
The advantages such as energy is superior, have preferable stability, and the most volatile, facilitate the use of staff.
Detailed description of the invention
A kind of solid defoaming agent, is made up of according to the raw material of weight portion following: coke 2-10 part, potassium iodide 3-13 part, four
Butyl phosphonium bromide 2-10 part, fatty acid amide 1-7 part, amido silicon oil 2-8 part, trifluoroacetic acid 2-10 part, epoxychloropropane 4-12
Part, waterglass 2-12 part, dimethicone 3-13 part.
Above-mentioned a kind of solid defoaming agent, is made up of according to the raw material of weight portion following: coke 2-8 part, potassium iodide 3-11
Part, tetrabutyl phosphonium bromide phosphorus 2-8 part, fatty acid amide 1-5 part, amido silicon oil 2-6 part, trifluoroacetic acid 2-8 part, epoxychloropropane 4-
10 parts, waterglass 2-10 part, dimethicone 3-11 part.
Above-mentioned a kind of solid defoaming agent, is made up of according to the raw material of weight portion following: 6 parts of coke, potassium iodide 8 parts, and four
Butyl phosphonium bromide 6 parts, fatty acid amide 4 parts, amido silicon oil 5 parts, trifluoroacetic acid 6 parts, epoxychloropropane 8 parts, waterglass 7 parts,
Dimethicone 8 parts.
The preparation method of above-mentioned a kind of solid defoaming agent, comprises the steps of:
(1) the material number in claim 3 is chosen, by coke, potassium iodide, tetrabutyl phosphonium bromide phosphorus, fatty acid amide and amino
Silicone oil uses agitating device to mix, and mixing time is 20min, obtains mixture A；
(2) trifluoroacetic acid, epoxychloropropane, waterglass and dimethicone being carried out heat treated, heat time heating time is 30min,
Then being stirred by the material after heating, mixing time is 15min, obtains mixture B；
(3) mixture A and mixture B is carried out mixed processing, then mixed material is put in exsiccator and dry, obtain
Finished product.
The present invention has easy to make, the advantage such as soaking effect good and antifoam performance is superior, has preferable stability,
And the most volatile, facilitate the use of staff.
The above is embodiments of the invention, therefore all according to the structure described in the present patent application scope, feature and principle institute
The equivalence change done or modification, in the range of being all included in present patent application.
Claims (4)
1. a solid defoaming agent, it is characterised in that be made up of according to the raw material of weight portion following: coke 2-10 part, potassium iodide
3-13 part, tetrabutyl phosphonium bromide phosphorus 2-10 part, fatty acid amide 1-7 part, amido silicon oil 2-8 part, trifluoroacetic acid 2-10 part, epoxy chlorine
Propane 4-12 part, waterglass 2-12 part, dimethicone 3-13 part.
A kind of solid defoaming agent the most according to claim 1, it is characterised in that by the following raw material group according to weight portion
Become: coke 2-8 part, potassium iodide 3-11 part, tetrabutyl phosphonium bromide phosphorus 2-8 part, fatty acid amide 1-5 part, amido silicon oil 2-6 part, three
Fluorine propanoic acid 2-8 part, epoxychloropropane 4-10 part, waterglass 2-10 part, dimethicone 3-11 part.
A kind of solid defoaming agent the most according to claim 1, it is characterised in that by the following raw material group according to weight portion
Become: 6 parts of coke, potassium iodide 8 parts, 6 parts of tetrabutyl phosphonium bromide phosphorus, fatty acid amide 4 parts, amido silicon oil 5 parts, trifluoroacetic acid 6 parts, ring
Oxygen chloropropane 8 parts, waterglass 7 parts, dimethicone 8 parts.
4. according to the preparation method of a kind of solid defoaming agent described in claim 1-3, it is characterised in that by following steps group
Become:
(1) the material number in claim 3 is chosen, by coke, potassium iodide, tetrabutyl phosphonium bromide phosphorus, fatty acid amide and amino
Silicone oil uses agitating device to mix, and mixing time is 20min, obtains mixture A；
(2) trifluoroacetic acid, epoxychloropropane, waterglass and dimethicone being carried out heat treated, heat time heating time is 30min,
Then being stirred by the material after heating, mixing time is 15min, obtains mixture B；
(3) mixture A and mixture B is carried out mixed processing, then mixed material is put in exsiccator and dry, obtain
Finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610498405.1A CN106196899A (en) | 2016-06-30 | 2016-06-30 | A kind of solid defoaming agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610498405.1A CN106196899A (en) | 2016-06-30 | 2016-06-30 | A kind of solid defoaming agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106196899A true CN106196899A (en) | 2016-12-07 |
Family
ID=57462829
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610498405.1A Pending CN106196899A (en) | 2016-06-30 | 2016-06-30 | A kind of solid defoaming agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106196899A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108221472A (en) * | 2017-12-14 | 2018-06-29 | 定远县权达新能源科技有限公司 | A kind of paper pulp asepsis environment-protecting antifoaming agent |
Citations (10)
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|---|---|---|---|---|
| CN101991975A (en) * | 2010-12-13 | 2011-03-30 | 南京四新科技应用研究所有限公司 | Mineral oil defoaming agent and preparation method thereof |
| CN101991976A (en) * | 2010-12-13 | 2011-03-30 | 南京四新科技应用研究所有限公司 | Solid defoaming agent and preparation method |
| CN102234697A (en) * | 2011-06-27 | 2011-11-09 | 河南通宇冶材集团有限公司 | Slagging defoamer for iron smelting and preparation method thereof |
| CN103127748A (en) * | 2012-12-27 | 2013-06-05 | 南通市海顺化工有限公司 | Antifoaming agent |
| CN103550961A (en) * | 2013-11-20 | 2014-02-05 | 南宁春城助剂有限责任公司 | Blocky solid defoaming agent and preparation method |
| CN103833606A (en) * | 2012-11-25 | 2014-06-04 | 韩聪平 | Foaming agent preparation process based on stirring time control |
| CN104479439A (en) * | 2014-12-08 | 2015-04-01 | 南京四新科技应用研究所有限公司 | Mineral oil defoaming agent |
| CN104740902A (en) * | 2015-03-12 | 2015-07-01 | 唐孟菲 | Defoaming agent |
| CN105289050A (en) * | 2015-11-13 | 2016-02-03 | 宣城市聚源精细化工有限公司 | High-efficiency antifoaming agent |
| CN105502544A (en) * | 2015-12-16 | 2016-04-20 | 江苏盖亚环境工程有限公司 | Defoaming agent for boiler water treatment and preparation method thereof |
-
2016
- 2016-06-30 CN CN201610498405.1A patent/CN106196899A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101991975A (en) * | 2010-12-13 | 2011-03-30 | 南京四新科技应用研究所有限公司 | Mineral oil defoaming agent and preparation method thereof |
| CN101991976A (en) * | 2010-12-13 | 2011-03-30 | 南京四新科技应用研究所有限公司 | Solid defoaming agent and preparation method |
| CN102234697A (en) * | 2011-06-27 | 2011-11-09 | 河南通宇冶材集团有限公司 | Slagging defoamer for iron smelting and preparation method thereof |
| CN103833606A (en) * | 2012-11-25 | 2014-06-04 | 韩聪平 | Foaming agent preparation process based on stirring time control |
| CN103127748A (en) * | 2012-12-27 | 2013-06-05 | 南通市海顺化工有限公司 | Antifoaming agent |
| CN103550961A (en) * | 2013-11-20 | 2014-02-05 | 南宁春城助剂有限责任公司 | Blocky solid defoaming agent and preparation method |
| CN104479439A (en) * | 2014-12-08 | 2015-04-01 | 南京四新科技应用研究所有限公司 | Mineral oil defoaming agent |
| CN104740902A (en) * | 2015-03-12 | 2015-07-01 | 唐孟菲 | Defoaming agent |
| CN105289050A (en) * | 2015-11-13 | 2016-02-03 | 宣城市聚源精细化工有限公司 | High-efficiency antifoaming agent |
| CN105502544A (en) * | 2015-12-16 | 2016-04-20 | 江苏盖亚环境工程有限公司 | Defoaming agent for boiler water treatment and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108221472A (en) * | 2017-12-14 | 2018-06-29 | 定远县权达新能源科技有限公司 | A kind of paper pulp asepsis environment-protecting antifoaming agent |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161207 |