Quiet pressure release reactor
Technical field
The present invention relates to a kind of reactor, it is quiet pressure release reactor.
Background technology
Entecavir is in the preparation process of reactor, and the intermediate product of generation needs to be filled with noble gas as protection,
This noble gas many employings nitrogen, owing to the intermediate product in reactor can produce other certain gases, therefore when converting
Need to control well reactor internal gas pressure when being filled with nitrogen, anti-impervious liquid.
Want to be released by the gas of overvoltage in time simultaneously, it is ensured that intrinsic pressure suitably, be difficult to ensure that intrinsic pressure owing to manually carrying out pressure release
It is stable at a numerical value, and low during height time intrinsic pressure, and the preparation for Entecavir affects relatively big, and there is certain danger
Property.
Owing to, in pressure leak process, high velocity air, when through small holes or gap, can make air produce friction and vibrate, thus
Produce noise.
Summary of the invention
The goal of the invention of the present invention is to solve high velocity air in the problem producing noise through small holes or gap, it is provided that
Quiet pressure release reactor, increases the air-tightness of whole pressure relief device, it is to avoid gas spills from gap by tight mechanism, and generation is made an uproar
Sound.
In order to realize foregoing invention purpose, present invention employs techniques below scheme: quiet pressure release reactor, including kettle
And pressure relief device, described pressure relief device includes pressure release barrel, valve casing, spool and the elastic component for valve core reset;Pressure release barrel
Bottom is provided with the gas channel that connect internal with kettle, and pressure release barrel open top is arranged, and valve casing is sheathed and is fixed on pressure release cylinder
Pars intramuralis, forms the gap that supply stream passes through between pressure release barrel and valve casing, pressure release barrel is provided with silencing mechanism, described quiet machine
Structure includes tight mechanism and the multiple steam vents flowed out for air-flow, and described steam vent is along pressure release barrel sidewall circumference annular array;
Described tight mechanism includes sealing ring, tapered ring-type of described sealing ring, sealing ring between pressure release barrel and valve casing, valve
Shell lower end compresses sealing ring, and in a tubular form, valve casing lower end and the sealing ring place of compressing are provided with and sealing ring taper fit in valve casing lower end
Seal chamfering;Being provided with the cavity volume moved for spool reciprocal telescopic inside valve casing, elastic component and spool are respectively positioned in cavity volume, described appearance
Chamber sidewall is provided with the valve opening connected with gap, is additionally provided with the position limiting structure preventing spool from deviating from described cavity volume.
Preferably, the bottom of described sealing ring is additionally provided with horizontal washer, and the thickness of described horizontal washer is thick more than sealing ring
Degree.
Preferably, being provided with the closure gasket groove being embedded for sealing ring in described pressure release barrel, described sealing ring is embedded at sealing
In annular groove, closure gasket groove is tapered ring-type.
Preferably, described sealing ring and horizontal washer are all embedded in closure gasket groove.
Preferably, described pressure release barrel top is additionally provided with the close annular groove in top, and the close annular groove in described top is positioned at pressure release barrel inwall, institute
State and be additionally provided with on valve casing for fixing top Mi Quan in the fixing bulge loop pushed up in close annular groove.
Preferably, described valve casing outer wall is threaded connection with the inwall of pressure release barrel.
Preferably, described steam vent arranges and along pressure release barrel axle center array in the form of a ring in pressure release barrel sidewall.
Preferably, described position limiting structure is bulge loop, and described bulge loop is fixed on the inner wall surface of valve casing.
Compared with prior art, have employed the quiet pressure release reactor of technique scheme, have the advantages that
One, using the quiet pressure release reactor of the present invention, the spool in pressure relief device can be by air pressure jack-up, when spool quilt
During high pressure jack-up, valve opening is opened, and is connected with gap by the gas channel in valve casing, gap so that by the gas that releases from aerofluxus
Shed in hole.
Owing to spool can be controlled by elastic component, and it is to use elastic component to be controlled, therefore when intrinsic pressure slightly larger
When elastic pressure, valve opening can be opened, and quickly reactor internal high pressure is carried out pressure release, when intrinsic pressure less than elastic pressure
Time, spool sets back and is closed by valve opening, reaching the effect of pressure control voltage stabilizing.
Two, secondly by setting up multiple thickly dotted steam vent on pressure release barrel 3, the gas velocity at steam vent is reduced
Degree, eliminates fricative phenomenon, reduces noise, makes production environment the quietest.
Three, tight mechanism is for sealing the joint gap between pressure release barrel and valve casing, reduces the noise that gas leakage produces.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention quiet pressure release reactor embodiment;
Fig. 2 is the structural representation of pressure relief device in the present invention;
Fig. 3 is the sectional view (valve opening closed mode) of pressure relief device in the present invention;
Fig. 4 is the sectional view (valve opening opening) of pressure relief device in the present invention;
Fig. 5 is the sectional view of valve casing in the present invention;
Fig. 6 is the sectional view of pressure release barrel in the present invention;
Fig. 7 is the structural representation of sealing ring in the present invention;
Fig. 8 is the sectional view of sealing ring in the present invention.
Reference: 1, valve casing;10, valve opening;11, groove;110, gathering sill;12, external screw thread;13, bulge loop;2, spool;
20, lead;3, pressure release barrel;30, gap;31, steam vent;32, female thread;41, top Mi Quan;42, sealing ring;420, level
Packing ring.
Detailed description of the invention
Below in conjunction with the accompanying drawings the present invention is described further.
As Fig. 1 is to pressure release reactor quiet shown in 8, and including kettle and pressure relief device A, pressure relief device A includes pressure release barrel
3, valve casing 1, spool 2 and the elastic component resetted for spool 2;
Being provided with the gas channel that connect internal with kettle bottom pressure release barrel 3, pressure release barrel 3 open top is arranged, valve casing 1
Sheathed and to be fixed on pressure release barrel 3 internal, form the gap 30 that supply stream passes through, pressure release barrel between pressure release barrel 3 and valve casing 1
3 are provided with the multiple steam vents 31 flowed out for air-flow, and steam vent 31 is along pressure release barrel 3 sidewall circumference annular array.
Spool in pressure relief device can be by air pressure jack-up, and when spool is by high pressure jack-up, valve opening is opened, by valve casing
Gas channel is connected with gap, gap and then shed in steam vent by the gas released.
Owing to spool can be controlled by elastic component, and it is to use elastic component to be controlled, therefore when intrinsic pressure slightly larger
When elastic pressure, valve opening can be opened, and quickly reactor internal high pressure is carried out pressure release, when intrinsic pressure less than elastic pressure
Time, spool sets back and is closed by valve opening, reaching the effect of pressure control voltage stabilizing.
Steam vent 31 arranges and along pressure release barrel 3 axle center array in the form of a ring in pressure release barrel 3 sidewall.Owing to high velocity air exists
When small holes or gap, air can be made to produce friction and vibrate, thus produce noise.Therefore, the present embodiment is by pressure release
Set up multiple thickly dotted steam vent on barrel 3, eliminate fricative phenomenon, reduce noise, make production environment the quietest.
Valve casing 1 outer wall is threaded connection with the inwall of pressure release barrel 3.Pressure release barrel 3 inwall is provided with female thread, valve casing 1
Outer wall is provided with external screw thread, and external screw thread engages with female thread.By screwed tight, valve casing 1 is rigidly secured to pressure release barrel 3
In.
Tight mechanism includes sealing ring 42, and tapered ring-type of sealing ring 42, sealing ring 42 is positioned at pressure release barrel 3 and valve casing
Between 1, valve casing 1 lower end compresses sealing ring 42, and in a tubular form, valve casing 1 lower end and the sealing ring place of compressing are provided with and seal in valve casing 1 lower end
The sealing chamfering 15 of circle taper fit.
The effect of tight mechanism is to increase the air-tightness of pressure relief device, makes all of air-flow all arrange in pressure release steam vent
Go out, it is to avoid air-flow produces noise through gap.The tapering of sealing ring 42 coordinates with sealing chamfering 15, can increase the face of sealing
Long-pending, improve sealing, and so that the horizontal and vertical equal sealing that can obtain strengthens.
The bottom of sealing ring 42 is additionally provided with horizontal washer 420, and the thickness of horizontal washer 420 is more than sealing ring 42 thickness, water
Plain washer is one-body molded with sealing ring.Due to valve casing be threaded into tighten time, downward pressure is relatively big, sets up level pad successively
Circle 420 can effectively compress bottom valve casing, and the valve casing effect of tightening is played preferably utilization, the thickness of horizontal washer 420
Thicker, it is to deal with compressing when valve casing is tightened, it is therefore desirable to thicker thickness is used for deformable seal.
Being provided with the closure gasket groove 34 being embedded for sealing ring in pressure release barrel 3, sealing ring 42 and horizontal washer 420 are all embedded at
In closure gasket groove 34, closure gasket groove 34 is tapered ring-type.
The effect of closure gasket groove 34 is when sealing ring 42 and horizontal washer 420 are by valve casing crimp, it is possible to completely
Full live whole closure gasket groove 34, the area making contact is bigger, effectively improves sealing property.Secondly, closure gasket groove 34 can
So that sealing ring and horizontal washer are played good fixation, during preventing valve casing from turning, sealing ring and horizontal washer run
Partially.
Pressure release barrel 3 top is additionally provided with the close annular groove 33 in top, is embedded with the close circle 41 in top, pushes up close annular groove 33 in pushing up close annular groove 33
In pressure release barrel 3 inwall, valve casing 1 is additionally provided with for the fixing top Mi Quan fixing bulge loop 14 in pushing up close annular groove.
In the present embodiment, there is the place in gap except bottom in valve casing and pressure release barrel, also top, therefore top is still
Sealing structure set up by needs.
Setting up the close annular groove 33 in top on the sidewall of pressure release barrel, place and push up close circle 41 in pushing up close annular groove 33, pushing up close circle 41 is
Usual endless sealing ring, when valve casing is tightened, the fixing bulge loop 14 of valve casing outer wall can hold out against pushing up close circle 33, prevents top
Close circle 33 comes off or offsets.
Valve casing 1 is internal is provided with the cavity volume 11 moved for spool 2 reciprocal telescopic, and spring and spool 2 are respectively positioned in cavity volume 11, hold
Chamber 11 sidewall is provided with the valve opening 10 connected with gap 30, and cavity volume 11 inner wall surface is additionally provided with bulge loop 13.The effect of bulge loop 13 is,
Spool, when by spring fight back in situ, can play a spacing effect, prevents spool from deviating from cavity volume, causes control valve to lose
Effect.
Spool 2 includes lead 20, and lead 20 is located at the top of spool 2, and spool 2 assumes a " convex " shape, and sets in cavity volume 11
Having the gathering sill 110 embedded for lead 20, return unit is spring, and lead 20 sidewall is located at by spring housing.
Lead 20 has two functions: first, is for keeping the spool direction when sliding, it is ensured that spool can edge
The axis direction of valve casing slides, and prevents skew, it is to avoid dislocation;Secondly, sheathed for spring, plays a limit to spring
Position effect, prevents spring from use offseting.
Due to pressure release barrel 3 with valve casing 1 when docking, still there is gap, many places, therefore pressure release barrel 3 and valve casing 1 it
Between be additionally provided with prevent gas leakage top sealing ring 41 and bottom sealing ring 42.At two, the effect of sealing ring is, it is possible to coordinates and lets out
Pressure cylinder wall 3 and valve casing 1 tighten effect, pressing sealing ring card jail tightly down in gap by valve casing 1, improve tightness,
Avoid air-flow to overflow in gap, noise occurs.
It is above the preferred embodiment of the present invention, former without departing from the present invention for the person of ordinary skill of the art
On the premise of reason, it is also possible to make some modification and improvement, these also should be regarded as protection scope of the present invention.