CN106178912A - Double pH spray desulfurizing tower biphase rectification drainage sets - Google Patents
Double pH spray desulfurizing tower biphase rectification drainage sets Download PDFInfo
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- CN106178912A CN106178912A CN201610563548.6A CN201610563548A CN106178912A CN 106178912 A CN106178912 A CN 106178912A CN 201610563548 A CN201610563548 A CN 201610563548A CN 106178912 A CN106178912 A CN 106178912A
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- ring
- desulfurizing tower
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- alms bowl
- spray
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/501—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound
- B01D53/504—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound characterised by a specific device
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/40—Alkaline earth metal or magnesium compounds
- B01D2251/404—Alkaline earth metal or magnesium compounds of calcium
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- Biomedical Technology (AREA)
- Environmental & Geological Engineering (AREA)
- Analytical Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treating Waste Gases (AREA)
Abstract
The present invention develops a kind of double pH spray desulfurizing tower biphase rectification drainage sets of design, is mainly used in sulfur removal technology the drain of double pH spray desulfurizing tower cleaning mixture, and rises the rectification of flue gas in desulfurizing tower.This device is arranged in desulfurizing tower between double pH spray equipments, including wall stream draining ring and alms bowl type drip tray;Wall stream draining ring is combined by upper and lower distribution arc ring and vibration separatory ring, upper and lower distribution arc ring shape is suitable and opposing setting, and outwardly, two rings are respectively arranged with one end and are arranged on the inwall of desulfurizing tower concave surface, two ring other end outer rims offset connection, and inwardly connect described vibration separatory ring;Alms bowl type drip tray is arranged on the underface of inner wall of tower stream draining ring, alms bowl type drip tray open topped, and bottom is connected to high pH slurry pool through serosity pipeline.This device is mainly used in low ph value washing liquid, high ph-values washing liquid is separated recovery, has structure unique, and current-sharing is effective, it is high to wash effective liquid-gas ratio, desulfuration efficiency is high, the little feature of absorption tower resistance.
Description
Technical field:
The present invention provides a kind of multi-function double-way rectification hydrops pH value partitioning device, is specially a kind of double pH spray desulfurizing tower two-way
Rectification drainage set, belongs to resource environment flue gases purification field.
Background technology:
Along with thermal power plant's atmosphere pollution controls to enter the minimum discharge stage, thermoelectricity SO 2 from fume concentration of emission controls requirement
From the 200mg/m of standard GB/T 13223-20113Near 35mg/m3Below.At present, the conventional limestone Gypsum Fibrosum of application takes off
Sulfur technique uses the single pH value of single column spray to control, and desulfuration efficiency is generally 95%, relies on simple amplification conservative design, difficult
To meet new emission control requirement, and there is construction and run uneconomical, the problems such as adaptability for working condition is poor.
According to the further investigation of desulphurization mechanism and analysis, when in desulfurizing tower slurry pH value control low interval time, can carry
High liquid phase reactor speed, accelerates the dissolving of absorbent limestone, promotes the oxidation of by-product Gypsum Fibrosum and crystallization, after being beneficial to washing
The stable curing of sulfur dioxide and salt-forming conversions, promote desulfurization.Serosity can be improved to flue gas when pH value controls in high interval
The washing absorption speed of middle sulfur dioxide.Traditional single column list pH value controls to look for a relative compromise between height pH
Span of control, it is impossible to thoroughly solve this contradiction.At present, domestic use single column double circulation desulphurization tower use conical bottom collect bowl with
Serosity deflector, blocking-up shock effect that flue gas is through-flow is obvious, and flow transition is the most smooth and easy, distributing homogeneity is poor, causes flue gas to lead to
Flow resistance is big, and air and gas system energy consumption is significantly increased.It is thus desirable to exploitation one can be taken into account by high and low pH value zonal control simultaneously,
Homogenizing flow field is to reduce the technology and equipment of flue gas flow passage resistance, it is achieved desulfurization low energy consumption puies forward effect further, adapts to new environmental protection
Emission request.
Summary of the invention:
The present invention develops a kind of combination unit designing uniqueness, is mainly used in sulfur removal technology double pH spray desulfurizing tower cleaning mixture
The rectification of flue gas is risen in drain, and desulfurizing tower.
The concrete technical scheme of the present invention is as follows:
A kind of double pH spray desulfurizing tower biphase rectification drainage set, the high and low pH spray equipment that this device is arranged in desulfurizing tower
Between, including wall stream draining ring and alms bowl type drip tray;
Described wall stream draining ring is combined by upper and lower distribution arc ring and vibration separatory ring, upper and lower distribution arc ring shape quite and
Being symmetrical arranged dorsad, outwardly, two ring outer rims are separately mounted on desulfurizing tower inwall concave surface, and two ring outer rims offset and connect, and
The inner ring of inner edge connects described vibration separatory ring;
Described alms bowl type drip tray is arranged on the underface of wall stream draining ring, and is arranged in desulfurizing tower by bracing frame, and alms bowl type amasss
Liquid dish open topped, bottom is connected to high pH slurry pool through serosity pipeline.
The design further of the present invention is:
Port radius little compared with 0.618R 0.1~0.5m in upper and lower distribution arc ring radially projecting, outer port radius is suitable with desulfurizing tower,
The radian of upper and lower distribution arc ring is 1 °~30 °, and arc radius is 0.3 R~0.6R;Alms bowl type drip tray is suitable for reading with wall stream draining ring
The spacing of upper and lower distribution arc ring junction be 0.382R ± 0.5m;In alms bowl type drip tray bore compared with the 0.618 big 0.1m of R~
0.5m;The outer bore of vibration separatory ring is suitable with bore in upper and lower distribution arc ring, and interior bore is little by 0.1 compared with the bore of alms bowl type drip tray
~1.5m;Wherein R is desulfurizing tower radius.
Carry tapered below vibration separatory hoop desulfurizing tower, be 1 °~30 ° of angles with horizontal direction;Thickness be 0.02~
0.3mm;Width is 5~300mm.
It is located by connecting via limiting plate between upper and lower distribution arc ring;Alms bowl type drip tray surface uses airflow design;Vibration
Separatory ring inner ring is dentation.
Upper and lower distribution arc ring and alms bowl type drip tray use corrosion and wear resistant alloy, glass steel material or use carbon steel lining plating
Antiseptic wearable coat.
In order to realize the serosity vibration dispersion of wall stream draining ring, vibration separatory ring uses elastic alloy or nonmetal corrosion resistant resistance to
Wear down sheet material;As thin metallic titanium alloy, two-phase alloys steel, PC, PET, PFA etc. have certain elastic material and make.
The present invention has the advantages that compared to existing technology
1, double pH spray desulfurizing tower biphase rectification drainage sets of present invention design, for by high ph-values washing liquid and low ph value washing liquid
Separately reclaim control, by absorption tower wall stream serosity sub-distribution again, adsorption tower smoke is the most mixed, there is structure unique, current-sharing effect
Well, the features such as effective liquid-gas ratio is high, desulfuration efficiency is high, absorption tower resistance is little are washed.
2, double pH subregions are arranged, and absorption tower is divided into SO2High pH scrubbing section and low pH scrubbing section, this device can realize same
The function of the high and low pH value subregion regulation and control of lower cigarette wind flow passage resistance is compared in absorption tower.
3, research checking shows, for SO2Low pH scrubbing section, a large amount of SO of washing absorption2While, regulated and controled by low ph value,
Can promote that absorbent limestone the most thoroughly dissolves, improve the speed that absorbent dissolves and participates in chemical reaction, and be more conducive to
The oxidation of by-product Gypsum Fibrosum and crystallization;For SO2High pH scrubbing section, is regulated and controled by high ph-values, realizes SO further2Put forward effect;Phase
PH more single than conventional single column spray controls the double pH of technology and controls to realize higher desulfuration efficiency under the conditions of lower liquid-gas ratio,
Desulfuration efficiency is up to more than 99%, improves absorbent utilization rate close to 100%.
4, simultaneously, the employing of the present invention will be greatly improved the absorption tower adaptation to initial conditions (coal, absorbent, operating mode)
Property, improve while desulfuration efficiency, homogenizing absorption tower flow field, reduce flue gas flow passage resistance.
5, alms bowl type drip tray makes the serosity being in contact with it collision produce similar with unique Streamline Design of wall stream draining ring
The effect of " Folium Nelumbinis " effect, is gathered into rapidly liquid pearl and is rolled off surface, and in flue gas, condensation vapor gathering also provides dynamic for its surface
State self-cleaning, solves the serosity pickup scale problems of prior art, it is achieved that the self-cleaning function of this structure.
6, the Optimal Structure Designing of alms bowl type drip tray and wall stream draining ring makes the blocking effect of absorption tower section affect more
Low, current-sharing and concentration field effect of optimization are more preferable, and flow passage resistance is less.
Accompanying drawing illustrates:
Fig. 1 is the structural representation of the present invention.
Fig. 2 is the partial enlarged drawing of wall stream draining ring.
Fig. 1, in 2: 1-desulfurizing tower;2-height pH spray equipment;21-agitator;22-height pH slurry pool;23-oxidation spray gun;
24-height pH circulating pump;3-low pH scrubbing section;31-agitator;32-low pH slurry pool;33-oxidation spray gun;34-low pH circulating pump;
4-wall stream draining ring;Arc ring is distributed on 41-;Arc ring is distributed under 42-;43-limiting plate;44-vibrates separatory ring;5-alms bowl type hydrops
Dish;51-height pH serosity draws pipeline;52-bracing frame;6-one-level demister;Bis-grades of demisters of 7-.
Fig. 3 is existing single column double circulation desulphurization tower circular cone.
In Fig. 3: 1-desulfurizing tower;2-height pH spray equipment;21-agitator;22-height pH slurry pool;23-oxidation spray gun;24-
High pH circulating pump;3-low pH scrubbing section;31-agitator;32-low pH slurry pool;33-oxidation spray gun;34-low pH circulating pump;4-
Tower wall guide ring;5-conical trays;51-height pH serosity draws pipeline;52-supporting steel frame;6-one-level demister;7-bis-grades removes
Day with fog.
Detailed description of the invention:
The invention will be further elaborated below in conjunction with the accompanying drawings:
Embodiment one:
The concrete structure of the double pH spray desulfurizing tower biphase rectification drainage set of single column is as follows:
The double pH desulphurization system of single column of the present invention: include the high pH spray equipment 2 that is arranged in desulfurizing tower 1 and low pH spray equipment 3,
Connecting line and high pH serosity suspension oxidation device, low pH serosity suspension oxidation device, high pH slurry pool 22 and low pH slurry pool 32.
High pH spray equipment 2 and low pH spray equipment 3 are equipped with Multi-layer sprinkling head;High and low pH serosity suspension oxidation device bag
Include agitator, oxidation spray gun, filter screen and container etc..
Double pH desulphurization system features are to be washed by flue gas subregion, and the first order being arranged in lower floor is low pH scrubbing section, pH control
Scope 4-5.4 processed;The second level being arranged in upper strata is high pH scrubbing section, pH span of control 5.4-6.5.
As it is shown in figure 1, the high and low pH that the double pH spray desulfurizing tower biphase rectification drainage set of the present invention is arranged in desulfurizing tower
Between spray equipment, including wall stream draining ring and alms bowl type drip tray.
As in figure 2 it is shown, wall stream draining ring 4 by upper distribution arc ring 41, lower distribution arc ring 41 and vibration separatory ring 44 combine and
Becoming, upper and lower distribution arc ring shape quite and is dorsad symmetrical arranged, and outwardly, two ring outer rims are separately mounted to desulfurizing tower inwall to concave surface
On, two ring outer rims offset and connect, and the inner ring in inner edge connects described vibration separatory ring 44;Warp between upper and lower distribution arc ring
It is located by connecting by limiting plate 43.
Alms bowl type drip tray 5 is arranged on the underface of wall stream draining ring 4, and is arranged in desulfurizing tower 1 by bracing frame 52, alms bowl
Type drip tray 5 open topped, bottom is drawn pipeline 51 through high pH serosity and is connected paramount pH slurry pool 22, alms bowl type drip tray 5 surface
Use airflow design.
Port radius little compared with 0.618R 0.1~0.5m in upper and lower distribution arc ring radially projecting, outer port radius is fitted mutually with desulfurizing tower
Joining, the radian of upper and lower distribution arc ring is 1 °~30 °, and arc radius is 0.3 R~0.6R;Alms bowl type drip tray 5 is suitable for reading draws with wall stream
The spacing of the upper and lower distribution arc ring junction of stream ring 4 is 0.382R ± 0.5m;In alms bowl type drip tray 5, bore is big compared with 0.618 R
0.1m~0.5m;The vibration outer bore of separatory ring 44 is suitable with bore in upper and lower distribution arc ring, and interior bore is compared with alms bowl type drip tray 5
Bore little 0.1~1.5m;Wherein R is desulfurizing tower radius.
Vibration separatory ring 44 carries tapered below desulfurizing tower, is 1 °~30 ° of angles with horizontal direction;Thickness be 0.02~
0.3mm;Width be 5~300mm(these width be the bus of taper), vibration separatory ring 44 inner ring be dentation, be used for tearing drop.
Upper and lower distribution arc ring and alms bowl type drip tray 5 use corrosion and wear resistant alloy, glass steel material or use carbon steel lining plating
Antiseptic wearable coat.
The concrete function of the double pH spray desulfurizing tower biphase rectification drainage set each several part of the present invention is as follows:
1, wall stream draining ring deflects from absorbing tower wall for the serosity that upper strata sprays wall built-up, imports to alms bowl type drip tray, simultaneously
It is assigned to wall built-up liquid film vibrate on separatory ring, is again torn to cut by vibration separatory ring split by vibrating the serosity confluxed by wall built-up
It is dispersed into drop for flue gas washing, to improve the effective liquid-gas ratio of desulfurization.
2, vibration separatory ring is to be connected to the inner side that upper and lower two arc rings engage junctions to open the alloy thin layer of strip tooth mouth,
Inner generation under the impact of air-flow and spray droplet is shaken, and the serosity under along wall stream is torn into scattered drop.Vibration
The material of separatory ring can use alloy, carbon steel cover antiseptic wearable coat, can also use anticorrosive anti-wear non-metallic material (as
Fiberglass), vibration source is that the impact of air-flow, liquid stream or whereabouts serosity causes.Unique streamline construction design of wall stream draining ring makes
The serosity that must be in contact with it collision produces the effect of similar " Folium Nelumbinis " effect, is gathered into rapidly liquid pearl and is rolled off surface, and evaporates water
Vapour condenses to assemble and also provides self-cleaning function for its surface, solves the serosity pickup scale problems of prior art, it is achieved that
The self-cleaning function of this structure.
3, alms bowl type drip tray: in alms bowl body streamline construction, open topped, for collecting the serosity that high pH scrubbing section gets off,
Bottom connects serosity pipeline, the high pH serosity collected is derived the high pH stock tank outside absorption tower, thus low pH starches with in absorption tower
Being effectively isolated of pond, it is achieved double pH value control partition function.The Streamline Design of alms bowl type drip tray is conducive to cigarette from below to up
Gas rounding off and shunting, reduce the resistance that flue gas is through-flow to greatest extent.Airflow design any surface finish simultaneously, has " Folium Nelumbinis " to imitate
The function answered, the slurry droplet that flue gas carries collides its surface and is gathered into rapidly liquid pearl and tumbles, do not stains, and also can profit
Flue gas carried may the serosity that adheres to of collision and fine grained be carried out with the condensing drip of saturated wet flue gas curding out, real
Existing self-cleaning function.
4, the volume of alms bowl type drip tray is upper strata sprayed slurry 0~100S residence time volumes, arranges height bottom drip tray
PH serosity draws pipeline, and caliber needs to mate with drip tray volume to avoid drip tray serosity overflow.
5, using the present invention, the Optimal Structure Designing of alms bowl type drip tray and wall stream draining ring makes the obstruct of absorption tower section
Effects is lower, and current-sharing and concentration field effect of optimization are more preferable, and flow passage resistance is less.
Test case one:
Certain processes exhaust gas volumn 50,000 m3/ h desulfurization test device, absorption tower spray number of plies configuration is identical, has carried out following several situations
Test compare;
Situation one: void tower, 3 layers of spray, single pH value controls;
Situation two: use double pH spray desulfurizing tower biphase rectification drainage sets of embodiment two, it is achieved pH value subregion, above device
High pH spray equipment arranges one layer, and lower section low pH spray equipment arranges two-layer.
Situation three: use existing tradition single column double circulation desulphurization tower circular cone shown in Fig. 3 (to use conical trays, tower wall
Guide ring is plank frame), remaining experimental condition is similar with situation 2.
Experimental test result such as following table:
Ratio Relatively | Inlet flue gas Amount, m3/h | Entrance SO2Dense Degree, mg/m3 | Absorption tower Resistance, Pa | Spray is opened Open the number of plies | Desulfurization Effect Rate, % | PH value | Outlet SO2Dense Degree, mg/m3 | Section flow field Speed is inclined Difference, % |
Feelings Shape One | 41122 | 2500 | 556 | 3 | 95.12 | 4.91 | 122.00 | 18.7 |
Feelings Shape Two | 41078 | 2651 | 692 | 3 | 99.03 | Low pH4.61, High pH5.81 | 25.71 | 3.56 |
Feelings Shape Three | 40975 | 2623 | 835 | 3 | 98.23 | Low pH4.59, High pH5.85 | 46.43 | 7.91 |
As seen from the above table, the rectification drainage set of present invention design have that desulfuration efficiency is high, absorption tower resistance is little, improve flow field,
Reduce the feature overcoming cigarette wind flow passage resistance energy consumption.
Claims (9)
1. double pH spray desulfurizing tower biphase rectification drainage sets, the high and low pH spray dress that this device is arranged in desulfurizing tower
Between putting, it is characterised in that: include wall stream draining ring and alms bowl type drip tray;
Described wall stream draining ring is combined by upper and lower distribution arc ring and vibration separatory ring, upper and lower distribution arc ring shape quite and
Being symmetrical arranged dorsad, outwardly, two ring outer rims are separately mounted on desulfurizing tower inwall concave surface, and two ring outer rims offset and connect, and
The inner ring of inner edge connects described vibration separatory ring;
Described alms bowl type drip tray is arranged on the underface of wall stream draining ring, and is arranged in desulfurizing tower by bracing frame, and alms bowl type amasss
Liquid dish open topped, bottom is connected to high pH slurry pool through serosity pipeline.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: upper and lower distribution arc
Port radius little compared with 0.618R 0.1~0.5m in ring radially projecting, outer port radius is suitable with desulfurizing tower, upper and lower distribution arc ring
Radian is 1 °~30 °, and arc radius is 0.3 R~0.6R;The alms bowl type drip tray upper and lower distribution arc ring with wall stream draining ring suitable for reading
The spacing of junction is 0.382R ± 0.5m;In alms bowl type drip tray, bore is compared with 0.618 big 0.1m~0.5m of R;Outside vibration separatory ring
Bore is suitable with bore in upper and lower distribution arc ring, and interior bore is compared with the bore little 0.1~1.5m of alms bowl type drip tray;Wherein R is desulfurization
Tower radius.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: vibration separatory hoop
Carry tapered below desulfurizing tower, be 1 °~30 ° with horizontal direction;Thickness is 0.02~0.3mm;Width is 5~300mm.
4. according to the arbitrary described pair of pH spray desulfurizing tower biphase rectification drainage set of claim 1-3, it is characterised in that: upper and lower
It is located by connecting via limiting plate between distribution arc ring.
5. according to the arbitrary described pair of pH spray desulfurizing tower biphase rectification drainage set of claim 1-3, it is characterised in that: alms bowl type amasss
Liquid panel surface uses airflow design.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: in vibration separatory ring
Circle is in dentation.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: upper and lower distribution arc
Ring and alms bowl type drip tray use corrosion and wear resistant alloy, glass steel material or use carbon steel lining plating antiseptic wearable coat.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: vibration separatory ring is adopted
By elastic alloy or nonmetal anticorrosive anti-wear thin slice material.
The most double pH spray desulfurizing tower biphase rectification drainage sets, it is characterised in that: vibration separatory ring is adopted
Make with thin metallic titanium alloy, two-phase alloys steel, PC, PET or PFA material.
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CN201610563548.6A CN106178912B (en) | 2016-07-15 | 2016-07-15 | Double pH spray desulfurizing towers biphase rectification drainage sets |
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CN201610563548.6A CN106178912B (en) | 2016-07-15 | 2016-07-15 | Double pH spray desulfurizing towers biphase rectification drainage sets |
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CN106178912B CN106178912B (en) | 2018-06-26 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106731591A (en) * | 2017-01-23 | 2017-05-31 | 浙江菲达环保科技股份有限公司 | Two stage cycle subregion desulfurizing tower |
CN114042374A (en) * | 2021-11-16 | 2022-02-15 | 临西县军华机械配件有限公司 | Prevent alkali lye spray column of wall flow |
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JPH09299744A (en) * | 1996-05-09 | 1997-11-25 | Babcock Hitachi Kk | Wet process flue gas desulfurziation equipment with acoustic wave generator and method thereof |
CN103041689A (en) * | 2013-01-04 | 2013-04-17 | 张国栋 | Liquid distribution device for absorption tower |
CN203816500U (en) * | 2014-05-15 | 2014-09-10 | 武汉凯迪电力环保有限公司 | Desulfurization tower with efficient dust removal performance |
CN206215029U (en) * | 2016-07-15 | 2017-06-06 | 国电环境保护研究院 | Double pH spray desulfurizing towers biphase rectification drainage sets |
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2016
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JPH09299744A (en) * | 1996-05-09 | 1997-11-25 | Babcock Hitachi Kk | Wet process flue gas desulfurziation equipment with acoustic wave generator and method thereof |
CN103041689A (en) * | 2013-01-04 | 2013-04-17 | 张国栋 | Liquid distribution device for absorption tower |
CN203816500U (en) * | 2014-05-15 | 2014-09-10 | 武汉凯迪电力环保有限公司 | Desulfurization tower with efficient dust removal performance |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106731591A (en) * | 2017-01-23 | 2017-05-31 | 浙江菲达环保科技股份有限公司 | Two stage cycle subregion desulfurizing tower |
CN114042374A (en) * | 2021-11-16 | 2022-02-15 | 临西县军华机械配件有限公司 | Prevent alkali lye spray column of wall flow |
CN114042374B (en) * | 2021-11-16 | 2023-11-07 | 临西县军华机械配件有限公司 | Alkali liquor spray tower capable of preventing wall flow |
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Address after: 210031 Qixia, Jiangsu Province, Wonderland Road, No. 10, Patentee after: National Electric Environmental Protection Research Institute Co., Ltd. Address before: 210031 Qixia, Jiangsu Province, Wonderland Road, No. 10, Patentee before: State Power Environmental Protection Research Institute |
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