CN106178589B - A kind of efficient extraction equipment - Google Patents
A kind of efficient extraction equipment Download PDFInfo
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- CN106178589B CN106178589B CN201610701597.1A CN201610701597A CN106178589B CN 106178589 B CN106178589 B CN 106178589B CN 201610701597 A CN201610701597 A CN 201610701597A CN 106178589 B CN106178589 B CN 106178589B
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- tower body
- feeder
- pipeline
- tower
- visor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The present invention provides a kind of efficient extraction equipments, including extraction tower, agitating device and feeder；Extraction tower includes tower body, upper capping and lower capping, liquid distributing board is equipped between tower body and upper capping, several through-holes are evenly distributed on liquid distributing board, the discharge port of tower body is connected with visor by pipeline, the first block valve is equipped between visor and discharge port, the pipeline after visor is equipped with the second block valve；Agitating device is set to the intracorporal center of tower vertically；Feeder is connected by the feed inlet of pipeline and tower body.Efficient extraction equipment of the present invention, material and extractant are pre-mixed, by the stirring of stirring rod and the distribution of liquid distribution plates between the feed inlet and liquid distribution plates of tower body, increase the mixability between material, pass through the visor of the discharge port of tower body, material flows out situation after observable control extraction, improves production quality.
Description
Technical field
The invention belongs to field of chemical equipment, more particularly, to a kind of efficient extraction equipment.
Background technique
Liquid-liquid extraction is using the difference of solute solubility between immiscible or partial miscibility two kinds of liquid phases come real
The process of separation or the purification of existing liquid mixture.Material to be extracted and extractant are mixed, stood, after being layered completely, into
Row blowing.When blowing, due to there is no observation device, often upper layer is not extracted to complete material by experience merely and released
It releases, can not guarantee the quality of extraction.The mixability of material and extractant is also influence extraction quality one before extraction
A important influence factor, relatively adequately mixing, it is complete to be conducive to extraction.
Summary of the invention
In view of this, the present invention is directed to propose a kind of efficient extraction equipment, can increase mixability between extraction material, clearly
Boundary liquid level after clear observation extraction, improves extraction quality.
In order to achieve the above objectives, the technical scheme of the present invention is realized as follows:
A kind of efficient extraction equipment, comprising: extraction tower, agitating device and feeder；
The extraction tower, comprising:
Tower body；
Upper capping, the upper end with the tower body is by flanged joint, equipped with liquid point between the upper capping and tower body
Fabric swatch, the upper capping are equipped with the feed inlet of tower body；
Lower capping, for the lower end with the tower body by flanged joint, the lower capping bottom end is equipped with the discharge port of tower body,
The discharge port of the tower body is connected with visor by pipeline；
The agitating device is set to the intracorporal center of the tower vertically, and the agitating device includes agitating shaft and multilayer stirring
Bar, the agitating shaft upper end passes through liquid distributing board and upper capping is connected to the motor；
The feeder is connected by the feed inlet of pipeline and tower body.
Further, several through-holes are evenly distributed on the liquid distributing board.Material is uniform by liquid distributing board
Distribution, is flowed into tower body.
Further, the feeder includes solution mix tank, and solution mix tank upper end is equipped with the first feed liquor of feeder
Second inlet of mouth and feeder, lower end are equipped with the liquid outlet of feeder, and the liquid outlet of the feeder passes through pipeline and tower
The feed inlet of body connects, and the pipeline between the liquid outlet of feeder and the feed inlet of tower body is equipped with pump.Feeder by material and
Extractant is pre-mixed, and is conducive to improve mixed degree.
Further, the stirring rod vertical welding is on agitating shaft, and is located between upper capping and liquid distributing board
Agitating shaft is equipped with stirring rod.The liquid come in from the feed inlet of tower body, the stirring rod by rotation are broken into tiny drop.
Further, the first block valve, the pipeline after the visor are equipped between the visor and the discharge port of tower body
It is equipped with the second block valve.First block valve and the second block valve are used cooperatively, and prevent discharge port of the extra material from tower body
Middle outflow.
Compared with the existing technology, efficient extraction equipment of the present invention has the advantage that
Material and extractant are pre-mixed by efficient extraction equipment of the present invention, feeder, and liquid distribution plates are arranged
Liquid is allocated before entering tower body, stirring rod is set between the feed inlet and liquid distribution plates of tower body, after mixing
Liquid several droplets are broken by stirring rod, increase the degree of mixing, by the visor of the discharge port of tower body, avoid
To not extract complete upper materials discharges, and improves extraction quality.
Detailed description of the invention
The attached drawing for constituting a part of the invention is used to provide further understanding of the present invention, schematic reality of the invention
It applies example and its explanation is used to explain the present invention, do not constitute improper limitations of the present invention.In the accompanying drawings:
Fig. 1 is efficient extraction equipment simple structure schematic diagram described in the embodiment of the present invention.
Description of symbols:
1- tower body；It is covered on 2-；It is covered under 3-；4- liquid distributing board；5- feed inlet；6- discharge port；7- agitating shaft；8- is stirred
Mix bar；9- visor；10- circular hole；11- solution mix tank；The first inlet of 12-；The second inlet of 13-；14- liquid outlet；15-
One block valve；The second block valve of 16-.
Specific embodiment
It should be noted that in the absence of conflict, the feature in embodiment and embodiment in the present invention can phase
Mutually combination.
In the description of the present invention, it is to be understood that, term " center ", " longitudinal direction ", " transverse direction ", "upper", "lower",
The orientation or positional relationship of the instructions such as "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outside" is
It is based on the orientation or positional relationship shown in the drawings, is merely for convenience of description of the present invention and simplification of the description, rather than instruction or dark
Show that signified device or element must have a particular orientation, be constructed and operated in a specific orientation, therefore should not be understood as pair
Limitation of the invention.In addition, term " first ", " second " etc. are used for description purposes only, it is not understood to indicate or imply phase
To importance or implicitly indicate the quantity of indicated technical characteristic.The feature for defining " first ", " second " etc. as a result, can
To explicitly or implicitly include one or more of the features.In the description of the present invention, unless otherwise indicated, " multiple "
It is meant that two or more.
In the description of the present invention, it should be noted that unless otherwise clearly defined and limited, term " installation ", " phase
Even ", " connection " shall be understood in a broad sense, for example, it may be being fixedly connected, may be a detachable connection, or be integrally connected；It can
To be mechanical connection, it is also possible to be electrically connected；It can be directly connected, can also can be indirectly connected through an intermediary
Connection inside two elements.For the ordinary skill in the art, above-mentioned term can be understood by concrete condition
Concrete meaning in the present invention.
The present invention will be described in detail below with reference to the accompanying drawings and embodiments.
A kind of efficient extraction equipment, including extraction tower, agitating device and feeder；
The extraction tower includes tower body 1, upper capping 2 and lower capping 3, equipped with liquid point between the tower body 1 and upper capping 2
Fabric swatch 4, the upper capping 2 are equipped with the feed inlet 5 of tower body 1, and 3 bottom ends of the lower capping are equipped with the discharge port 6 of tower body 1, described
The discharge port 6 of tower body 1 is connected with visor 9 by pipeline；
The agitating device is set to the center in tower body 1 vertically, and the agitating device includes agitating shaft 7 and multilayer stirring rod
8,7 upper end of agitating shaft passes through liquid distributing board 4 and upper capping 2 is connected to the motor；
The feeder is connect by pipeline with the feed inlet 5 of tower body 1.
Several through-holes 10 are evenly distributed on aforesaid liquid distribution grid 4.
Above-mentioned feeder includes solution mix tank 11, and 11 upper end of solution mix tank is equipped with 12 He of the first inlet of feeder
Second inlet 13 of feeder, lower end are equipped with the liquid outlet 14 of feeder, the liquid outlet 14 of the feeder by pipeline with
The feed inlet 5 of tower body 1 connects, and the pipeline between the liquid outlet 14 of feeder and the feed inlet 5 of tower body 1 is equipped with pump.
Above-mentioned 8 vertical welding of stirring rod is in the agitating shaft on agitating shaft 7, and between upper capping 2 and liquid distributing board 4
7 are equipped with stirring rod 8.
It is equipped with the first block valve 15 between above-mentioned visor 9 and the discharge port 6 of tower body 1, is set on the pipeline after the visor 9
There is the second block valve 16.
As shown in Figure 1, when in use, material to be extracted and extractant to be passed through to 12 He of the first inlet of feeder respectively
Second inlet 13 of feeder is passed through solution mix tank 11 and is pre-mixed, and material after mixing is passed through tower by pumping later
The feed inlet 5 of body 1 inputs in tower body 1, starts the motor being connected with agitating shaft 7, and agitating shaft 7 and stirring rod 8 rotate, due to
Have one layer of stirring rod 8 between liquid distributing board 4 and upper capping 2, into the mixing of tower body 1 after the stirring rod that is rotated of material
8 are broken into droplet drops on liquid distributing board 4 later, after the mean allocation by liquid distributing board 4, flows into tower body 1
Inside, using stirring rod 8 rotation stir, after mixing material by mixing more thoroughly.Material is uniformly mixed after to be mixed
Afterwards, a period of time is stood, material is classified into upper layer and lower layer after the mixing in tower body 1, and has an apparent boundary liquid level.Then
The first block valve 15 and the second block valve 16 are opened, boundary liquid level is observed by visor 9, to observe boundary liquid level in visor 9
When, closing the second block valve 16 immediately prevents supernatant liquid from flowing out.If you need to extract again, can continue to feed.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (4)
1. a kind of efficient extraction equipment characterized by comprising extraction tower, agitating device and feeder；
The extraction tower, comprising:
Tower body (1)；And
Upper capping (2), the upper end with the tower body (1) are set between upper capping (2) and the tower body (1) by flanged joint
Have liquid distributing board (4), the upper capping (2) is equipped with the feed inlet (5) of tower body (1)；And
Lower capping (3), for the lower end with the tower body (1) by flanged joint, lower capping (3) bottom end is equipped with tower body (1)
Discharge port (6), the discharge port (6) of the tower body (1) is connected with visor (9) by pipeline；
The agitating device is set to the center in the tower body (1) vertically, and the agitating device includes that agitating shaft (7) and multilayer are stirred
It mixes bar (8), agitating shaft (7) upper end passes through liquid distributing board (4) and upper capping (2) is connected to the motor；
The feeder is connect by pipeline with the feed inlet (5) of tower body (1)；Stirring rod (8) vertical welding is in agitating shaft
(7) on, and the agitating shaft (7) being located between upper capping (2) and liquid distributing board (4) is equipped with stirring rod (8).
2. efficient extraction equipment according to claim 1, it is characterised in that: be uniformly distributed on the liquid distributing board (4)
There are several through-holes (10).
3. efficient extraction equipment according to claim 1, it is characterised in that: the feeder includes solution mix tank
(11), solution mix tank (11) upper end is equipped with the first inlet (12) of feeder and the second inlet (13) of feeder, under
End is equipped with the liquid outlet (14) of feeder, and the liquid outlet (14) of the feeder is connected by pipeline and the feed inlet (5) of tower body (1)
It connects, the pipeline between the liquid outlet (14) of feeder and the feed inlet (5) of tower body (1) is equipped with pump.
4. efficient extraction equipment according to claim 1, it is characterised in that: the discharge port of the visor (9) and tower body (1)
(6) the first block valve (15) are equipped between, the pipeline after the visor (9) is equipped with the second block valve (16).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610701597.1A CN106178589B (en) | 2016-08-19 | 2016-08-19 | A kind of efficient extraction equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610701597.1A CN106178589B (en) | 2016-08-19 | 2016-08-19 | A kind of efficient extraction equipment |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106178589A CN106178589A (en) | 2016-12-07 |
| CN106178589B true CN106178589B (en) | 2019-04-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610701597.1A Active CN106178589B (en) | 2016-08-19 | 2016-08-19 | A kind of efficient extraction equipment |
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| CN (1) | CN106178589B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034370B (en) * | 2017-04-06 | 2018-05-25 | 江苏永超磁性材料有限公司 | A kind of rare earth processing Extractant of Rare Earth Elements high-efficient disposition equipment |
| CN107008030A (en) * | 2017-04-18 | 2017-08-04 | 上海应用技术大学 | A kind of continuous extraction separator |
| CN111876595A (en) * | 2020-07-02 | 2020-11-03 | 安徽南都华铂新材料科技有限公司 | Extraction tank and extraction method for lithium battery recovery |
| CN112575183A (en) * | 2020-12-02 | 2021-03-30 | 江西斯源科技有限公司 | Intelligent flow control device for rare and noble metal extraction |
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| WO2009152906A2 (en) * | 2008-05-26 | 2009-12-23 | Merck Patent Gmbh | Use of ionic liquids with tetracyanoborate anions as a solvent for extraction of alcohols from aqueous solutions |
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| CN202446857U (en) * | 2011-12-23 | 2012-09-26 | 湖北新蓝天新材料股份有限公司 | Extracting tower applied to butanone oxime hydrochloride |
| CN102974128A (en) * | 2012-11-28 | 2013-03-20 | 中国科学院南京土壤研究所 | Centrifugal stirring extraction tower |
| CN103215057A (en) * | 2013-04-12 | 2013-07-24 | 枣庄矿业集团煤化工研究院有限公司 | Low-temperature extraction separation kettle of coal tar |
| CN204293906U (en) * | 2014-11-25 | 2015-04-29 | 河南科技学院 | A kind of Chinese herbal medicine effective ingredients extraction element |
| CN204723799U (en) * | 2015-07-03 | 2015-10-28 | 四川天福精细化工有限公司 | Desensitizer production extraction tower |
| CN205988585U (en) * | 2016-08-19 | 2017-03-01 | 天津市博爱制药有限公司 | A kind of extraction equipment |
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2016
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|---|---|---|---|---|
| CN2174245Y (en) * | 1993-12-11 | 1994-08-17 | 浙江大学 | Fast-acting continuous extracting device for tea polyphenols |
| CN1562995A (en) * | 2004-04-02 | 2005-01-12 | 胡绍海 | Left ofloxacin and Pidotimod compound preparation tech and its appts. |
| CN201070547Y (en) * | 2007-07-24 | 2008-06-11 | 中国科学院武汉植物园 | Thermoregulation type ultrasound wave and microwave coupling extracting device |
| WO2009152906A2 (en) * | 2008-05-26 | 2009-12-23 | Merck Patent Gmbh | Use of ionic liquids with tetracyanoborate anions as a solvent for extraction of alcohols from aqueous solutions |
| CN201509562U (en) * | 2009-10-24 | 2010-06-23 | 阜新维远食品科技有限公司 | Vegetable protein extracting tank |
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| CN102974128A (en) * | 2012-11-28 | 2013-03-20 | 中国科学院南京土壤研究所 | Centrifugal stirring extraction tower |
| CN103215057A (en) * | 2013-04-12 | 2013-07-24 | 枣庄矿业集团煤化工研究院有限公司 | Low-temperature extraction separation kettle of coal tar |
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| Publication number | Publication date |
|---|---|
| CN106178589A (en) | 2016-12-07 |
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Effective date of registration: 20191203 Address after: 300000 South Zone, Jinghai Economic Development Zone, Tianjin Patentee after: TIANJIN BOAI BIO-PHARMACEUTICAL CO., LTD. Address before: 300382 Tianjin city Xiqing District Jingwu town Ronghua Road No. 4 Patentee before: TIANJIN BOAI PHARMACEUTICAL CO., LTD. |