CN106178589A - A kind of efficiently extraction equipment - Google Patents

A kind of efficiently extraction equipment Download PDF

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Publication number
CN106178589A
CN106178589A CN201610701597.1A CN201610701597A CN106178589A CN 106178589 A CN106178589 A CN 106178589A CN 201610701597 A CN201610701597 A CN 201610701597A CN 106178589 A CN106178589 A CN 106178589A
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CN
China
Prior art keywords
tower body
feeder
pipeline
visor
upper cover
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610701597.1A
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Chinese (zh)
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CN106178589B (en
Inventor
夏雪城
黄友法
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN BOAI BIO-PHARMACEUTICAL CO., LTD.
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Tianjin Boai Pharmaceutical Co Ltd
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Priority to CN201610701597.1A priority Critical patent/CN106178589B/en
Publication of CN106178589A publication Critical patent/CN106178589A/en
Application granted granted Critical
Publication of CN106178589B publication Critical patent/CN106178589B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid

Abstract

The invention provides a kind of efficiently extraction equipment, including extraction tower, agitating device and feeder;Extraction tower includes tower body, upper cover and lower capping, liquid distributing board it is provided with between tower body and upper cover, some through holes it are evenly distributed with on liquid distributing board, the discharging opening of tower body is connected by pipeline visor, being provided with the first block valve between visor and discharging opening, the pipeline after visor is provided with the second block valve;The center in tower body is vertically located at by agitating device;Feeder is connected with the charging aperture of tower body by pipeline.Efficient extraction equipment of the present invention, material and extractant are pre-mixed, the stirring of puddler and the distribution of liquid distribution plates between the charging aperture and liquid distribution plates of tower body, add the mixability between material, visor by the discharging opening of tower body, after observable controls extraction, material flows out situation, improves production quality.

Description

A kind of efficiently extraction equipment
Technical field
The invention belongs to field of chemical equipment, especially relate to a kind of efficiently extraction equipment.
Background technology
Liquid-liquid extraction is to utilize solute difference of dissolubility between immiscible or two kinds of liquid phases of partial miscibility to come real The process separating or purifying of existing liquid mixture.Material to be extracted and extractant are mixed, stands, after layering completely, enter Row blowing.Blowing when, owing to there is no facilities for observation, by experience, often upper strata is not extracted material completely merely and release Release, it is ensured that the not quality of extraction.Before extraction, the mixability of material and extractant is also the one of impact extraction quality Individual important influence factor, more sufficiently mixes, and is conducive to extraction completely.
Summary of the invention
In view of this, it is contemplated that propose a kind of efficiently extraction equipment, mixability between extraction material can be increased, clearly Boundary liquid level after clear observation extraction, improves extraction quality.
For reaching above-mentioned purpose, the technical scheme is that and be achieved in that:
A kind of efficiently extraction equipment, including: extraction tower, agitating device and feeder;
Described extraction tower, including:
Tower body;
Upper cover, it passes through Flange joint with the upper end of described tower body, is provided with liquid and divides between described upper cover and tower body Fabric swatch, described upper cover is provided with the charging aperture of tower body;
Lower capping, its lower end with described tower body is by Flange joint, and described lower capping bottom is provided with the discharging opening of tower body, The discharging opening of described tower body is connected by pipeline visor;
The center in described tower body is vertically located at by described agitating device, and described agitating device includes shaft and multilamellar stirring Bar, described shaft upper end is connected with motor through liquid distributing board with upper cover;
Described feeder, is connected with the charging aperture of tower body by pipeline.
Further, described liquid distributing board is evenly distributed with some through holes.Material passes through liquid distributing board by uniformly Distribution, is flowed in tower body.
Further, described feeder includes that solution mix tank, solution mix tank upper end are provided with the first feed liquor of feeder Mouth and the second inlet of feeder, lower end is provided with the liquid outlet of feeder, and the liquid outlet of described feeder passes through pipeline and tower The charging aperture of body connects, and the pipeline between liquid outlet and the charging aperture of tower body of feeder is provided with pump.Feeder by material and Extractant is pre-mixed, and is conducive to improving the degree of mixing.
Further, described puddler vertical welding is on shaft, and between upper cover and liquid distributing board Shaft is provided with puddler.The liquid come in from the charging aperture of tower body, is broken into tiny drop through the puddler rotated.
Further, the first block valve, the pipeline after described visor it are provided with between described visor and the discharging opening of tower body It is provided with the second block valve.First block valve and the second block valve with the use of, prevent the unnecessary material discharging opening from tower body Middle outflow.
Relative to prior art, efficient extraction equipment of the present invention has the advantage that
Efficient extraction equipment of the present invention, material and extractant are pre-mixed, arrange liquid distribution plates by feeder Liquid was allocated before entering tower body, puddler is set between charging aperture and the liquid distribution plates of tower body, after mixing Liquid be broken into some droplets by puddler, add the degree of mixing, by the visor of the discharging opening of tower body, it is to avoid To not extract upper materials completely discharges, and improves extraction quality.
Accompanying drawing explanation
The accompanying drawing of the part constituting the present invention is used for providing a further understanding of the present invention, and the present invention's is schematic real Execute example and illustrate for explaining the present invention, being not intended that inappropriate limitation of the present invention.In the accompanying drawings:
Fig. 1 is the efficient extraction equipment simple structure schematic diagram described in the embodiment of the present invention.
Description of reference numerals:
1-tower body;2-upper cover;Cover under 3-;4-liquid distributing board;5-charging aperture;6-discharging opening;7-shaft;8-stirs Mix bar;9-visor;10-circular hole;11-solution mix tank;12-the first inlet;13-the second inlet;14-liquid outlet;15- One block valve;16-the second block valve.
Detailed description of the invention
It should be noted that in the case of not conflicting, the embodiment in the present invention and the feature in embodiment can phases Combination mutually.
In describing the invention, it is to be understood that term " " center ", " longitudinally ", " laterally ", " on ", D score, Orientation or the position relationship of the instruction such as "front", "rear", "left", "right", " vertically ", " level ", " top ", " end ", " interior ", " outward " are Based on orientation shown in the drawings or position relationship, it is for only for ease of the description present invention and simplifies description rather than instruction or dark The device or the element that show indication must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that right The restriction of the present invention.Additionally, term " first ", " second " etc. are only used for describing purpose, and it is not intended that indicate or hint phase To importance or the implicit quantity indicating indicated technical characteristic.Thus, the feature defining " first ", " second " etc. can To express or to implicitly include one or more this feature.In describing the invention, except as otherwise noted, " multiple " It is meant that two or more.
In describing the invention, it should be noted that unless otherwise clearly defined and limited, term " is installed ", " phase Even ", " connection " should be interpreted broadly, for example, it may be fixing connection, it is also possible to be to removably connect, or be integrally connected;Can To be mechanical connection, it is also possible to be electrical connection;Can be to be joined directly together, it is also possible to be indirectly connected to by intermediary, Ke Yishi The connection of two element internals.For the ordinary skill in the art, above-mentioned term can be understood by concrete condition Concrete meaning in the present invention.
Describe the present invention below with reference to the accompanying drawings and in conjunction with the embodiments in detail.
A kind of efficiently extraction equipment, including extraction tower, agitating device and feeder;
Described extraction tower includes tower body 1, upper cover 2 and lower capping 3, is provided with liquid and divides between described tower body 1 and upper cover 2 Fabric swatch 4, described upper cover 2 is provided with the charging aperture 5 of tower body 1, and described lower capping 3 bottom is provided with the discharging opening 6 of tower body 1, described The discharging opening 6 of tower body 1 is connected by pipeline visor 9;
The center in tower body 1 is vertically located at by described agitating device, and described agitating device includes shaft 7 and multilamellar puddler 8, described shaft 7 upper end is connected with motor through liquid distributing board 4 with upper cover 2;
Described feeder is connected with the charging aperture 5 of tower body 1 by pipeline.
Some through holes 10 it are evenly distributed with on aforesaid liquid distribution grid 4.
Above-mentioned feeder includes that solution mix tank 11, solution mix tank 11 upper end are provided with the first inlet 12 He of feeder Second inlet 13 of feeder, lower end is provided with the liquid outlet 14 of feeder, the liquid outlet of described feeder 14 by pipeline with The charging aperture 5 of tower body 1 connects, and the pipeline between liquid outlet 14 and the charging aperture 5 of tower body 1 of feeder is provided with pump.
Above-mentioned puddler 8 vertical welding is on shaft 7, and the shaft between upper cover 2 and liquid distributing board 4 7 are provided with puddler 8.
It is provided with the first block valve 15 between above-mentioned visor 9 and the discharging opening 6 of tower body 1, the pipeline after described visor 9 sets There is the second block valve 16.
As it is shown in figure 1, in use, material to be extracted and extractant are passed through respectively the first inlet 12 He of feeder Second inlet 13 of feeder is passed through solution mix tank 11 and is pre-mixed, and by pump, material after mixing is passed through tower afterwards The charging aperture 5 of body 1 inputs in tower body 1, starts the motor being connected with shaft 7, and shaft 7 and puddler 8 rotate, due to One layer of puddler 8 is had, the puddler that after entering the mixing of tower body 1, material is rotated between liquid distributing board 4 and upper cover 2 8 be broken into droplet after drop on liquid distributing board 4, after the mean allocation of liquid distributing board 4, flow into tower body 1 Inside, then the rotation stirring through puddler 8, after mixing, material is more thorough by mix.Rear material mix homogeneously to be mixed After, standing a period of time, after the mixing in tower body 1, material is classified into upper and lower two-layer, and has an obvious boundary liquid level.Then Open the first block valve 15 and the second block valve 16, observe boundary liquid level by visor 9, treat visor 9 is observed boundary liquid level Time, close the second block valve 16 immediately and prevent supernatant liquid from flowing out.As need to be again extracted, charging can be continued.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all essences in the present invention Within god and principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.

Claims (5)

1. an efficient extraction equipment, it is characterised in that including: extraction tower, agitating device and feeder;
Described extraction tower, including:
Tower body (1);And
Upper cover (2), it passes through Flange joint with the upper end of described tower body (1), sets between described upper cover (2) and tower body (1) Liquid distributing board (4), described upper cover (2) is had to be provided with the charging aperture (5) of tower body (1);And
Lower capping (3), its lower end with described tower body (1) is by Flange joint, and described lower capping (3) bottom is provided with tower body (1) Discharging opening (6), the discharging opening (6) of described tower body (1) by pipeline connect have visor (9);
The center in described tower body (1) is vertically located at by described agitating device, and described agitating device includes that shaft (7) and multilamellar are stirred Mixing bar (8), described shaft (7) upper end is connected with motor through liquid distributing board (4) with upper cover (2);
Described feeder, is connected with the charging aperture (5) of tower body (1) by pipeline.
Efficient extraction equipment the most according to claim 1, it is characterised in that: described liquid distributing board is uniformly distributed on (4) There are some through holes (10).
Efficient extraction equipment the most according to claim 1, it is characterised in that: described feeder includes solution mix tank (11), solution mix tank (11) upper end is provided with first inlet (12) of feeder and second inlet (13) of feeder, under End is provided with the liquid outlet (14) of feeder, and the liquid outlet (14) of described feeder is connected by the charging aperture (5) of pipeline with tower body (1) Connecing, the pipeline between liquid outlet (14) and the charging aperture (5) of tower body (1) of feeder is provided with pump.
Efficient extraction equipment the most according to claim 1, it is characterised in that: described puddler (8) vertical welding is in stirring On axle (7), and the shaft (7) being positioned between upper cover (2) and liquid distributing board (4) is provided with puddler (8).
Efficient extraction equipment the most according to claim 1, it is characterised in that: described visor (9) and the discharging opening of tower body (1) (6) being provided with the first block valve (15) between, the pipeline after described visor (9) is provided with the second block valve (16).
CN201610701597.1A 2016-08-19 2016-08-19 A kind of efficient extraction equipment Active CN106178589B (en)

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Application Number Priority Date Filing Date Title
CN201610701597.1A CN106178589B (en) 2016-08-19 2016-08-19 A kind of efficient extraction equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610701597.1A CN106178589B (en) 2016-08-19 2016-08-19 A kind of efficient extraction equipment

Publications (2)

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CN106178589A true CN106178589A (en) 2016-12-07
CN106178589B CN106178589B (en) 2019-04-16

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107008030A (en) * 2017-04-18 2017-08-04 上海应用技术大学 A kind of continuous extraction separator
CN107034370A (en) * 2017-04-06 2017-08-11 南昌浩牛科技有限公司 A kind of rare earth processing Extractant of Rare Earth Elements high-efficient disposition equipment
CN111876595A (en) * 2020-07-02 2020-11-03 安徽南都华铂新材料科技有限公司 Extraction tank and extraction method for lithium battery recovery
CN112575183A (en) * 2020-12-02 2021-03-30 江西斯源科技有限公司 Intelligent flow control device for rare and noble metal extraction

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2174245Y (en) * 1993-12-11 1994-08-17 浙江大学 Fast-acting continuous extracting device for tea polyphenols
CN1562995A (en) * 2004-04-02 2005-01-12 胡绍海 Left ofloxacin and Pidotimod compound preparation tech and its appts.
CN201070547Y (en) * 2007-07-24 2008-06-11 中国科学院武汉植物园 Thermoregulation type ultrasound wave and microwave coupling extracting device
WO2009152906A2 (en) * 2008-05-26 2009-12-23 Merck Patent Gmbh Use of ionic liquids with tetracyanoborate anions as a solvent for extraction of alcohols from aqueous solutions
CN201509562U (en) * 2009-10-24 2010-06-23 阜新维远食品科技有限公司 Vegetable protein extracting tank
CN202446857U (en) * 2011-12-23 2012-09-26 湖北新蓝天新材料股份有限公司 Extracting tower applied to butanone oxime hydrochloride
CN102974128A (en) * 2012-11-28 2013-03-20 中国科学院南京土壤研究所 Centrifugal stirring extraction tower
CN103215057A (en) * 2013-04-12 2013-07-24 枣庄矿业集团煤化工研究院有限公司 Low-temperature extraction separation kettle of coal tar
CN204293906U (en) * 2014-11-25 2015-04-29 河南科技学院 A kind of Chinese herbal medicine effective ingredients extraction element
CN204723799U (en) * 2015-07-03 2015-10-28 四川天福精细化工有限公司 Desensitizer production extraction tower
CN205988585U (en) * 2016-08-19 2017-03-01 天津市博爱制药有限公司 A kind of extraction equipment

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2174245Y (en) * 1993-12-11 1994-08-17 浙江大学 Fast-acting continuous extracting device for tea polyphenols
CN1562995A (en) * 2004-04-02 2005-01-12 胡绍海 Left ofloxacin and Pidotimod compound preparation tech and its appts.
CN201070547Y (en) * 2007-07-24 2008-06-11 中国科学院武汉植物园 Thermoregulation type ultrasound wave and microwave coupling extracting device
WO2009152906A2 (en) * 2008-05-26 2009-12-23 Merck Patent Gmbh Use of ionic liquids with tetracyanoborate anions as a solvent for extraction of alcohols from aqueous solutions
CN201509562U (en) * 2009-10-24 2010-06-23 阜新维远食品科技有限公司 Vegetable protein extracting tank
CN202446857U (en) * 2011-12-23 2012-09-26 湖北新蓝天新材料股份有限公司 Extracting tower applied to butanone oxime hydrochloride
CN102974128A (en) * 2012-11-28 2013-03-20 中国科学院南京土壤研究所 Centrifugal stirring extraction tower
CN103215057A (en) * 2013-04-12 2013-07-24 枣庄矿业集团煤化工研究院有限公司 Low-temperature extraction separation kettle of coal tar
CN204293906U (en) * 2014-11-25 2015-04-29 河南科技学院 A kind of Chinese herbal medicine effective ingredients extraction element
CN204723799U (en) * 2015-07-03 2015-10-28 四川天福精细化工有限公司 Desensitizer production extraction tower
CN205988585U (en) * 2016-08-19 2017-03-01 天津市博爱制药有限公司 A kind of extraction equipment

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107034370A (en) * 2017-04-06 2017-08-11 南昌浩牛科技有限公司 A kind of rare earth processing Extractant of Rare Earth Elements high-efficient disposition equipment
CN107008030A (en) * 2017-04-18 2017-08-04 上海应用技术大学 A kind of continuous extraction separator
CN111876595A (en) * 2020-07-02 2020-11-03 安徽南都华铂新材料科技有限公司 Extraction tank and extraction method for lithium battery recovery
CN112575183A (en) * 2020-12-02 2021-03-30 江西斯源科技有限公司 Intelligent flow control device for rare and noble metal extraction

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Effective date of registration: 20191203

Address after: 300000 South Zone, Jinghai Economic Development Zone, Tianjin

Patentee after: TIANJIN BOAI BIO-PHARMACEUTICAL CO., LTD.

Address before: 300382 Tianjin city Xiqing District Jingwu town Ronghua Road No. 4

Patentee before: TIANJIN BOAI PHARMACEUTICAL CO., LTD.