CN106168002A - A kind of preparation method of fiber paper base mulch film - Google Patents

A kind of preparation method of fiber paper base mulch film Download PDF

Info

Publication number
CN106168002A
CN106168002A CN201610550123.1A CN201610550123A CN106168002A CN 106168002 A CN106168002 A CN 106168002A CN 201610550123 A CN201610550123 A CN 201610550123A CN 106168002 A CN106168002 A CN 106168002A
Authority
CN
China
Prior art keywords
staple fibre
mulch film
fiber
viscose staple
paper base
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610550123.1A
Other languages
Chinese (zh)
Other versions
CN106168002B (en
Inventor
张晓丽
王浩
杜兆芳
刘陶
周凯瑞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Agricultural University AHAU
Original Assignee
Anhui Agricultural University AHAU
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Agricultural University AHAU filed Critical Anhui Agricultural University AHAU
Priority to CN201610550123.1A priority Critical patent/CN106168002B/en
Publication of CN106168002A publication Critical patent/CN106168002A/en
Application granted granted Critical
Publication of CN106168002B publication Critical patent/CN106168002B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21FPAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F13/00Making discontinuous sheets of paper, pulpboard or cardboard, or of wet web, for fibreboard production
    • D21F13/02Making hand-made paper
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/02Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D5/00Purification of the pulp suspension by mechanical means; Apparatus therefor
    • D21D5/02Straining or screening the pulp
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/12Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/02Synthetic cellulose fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00Coated paper; Coating material
    • D21H19/10Coatings without pigments
    • D21H19/14Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
    • D21H19/18Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising waxes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00Coated paper; Coating material
    • D21H19/10Coatings without pigments
    • D21H19/14Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
    • D21H19/20Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/06Paper forming aids
    • D21H21/08Dispersing agents for fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H23/00Processes or apparatus for adding material to the pulp or to the paper
    • D21H23/02Processes or apparatus for adding material to the pulp or to the paper characterised by the manner in which substances are added
    • D21H23/22Addition to the formed paper
    • D21H23/70Multistep processes; Apparatus for adding one or several substances in portions or in various ways to the paper, not covered by another single group of this main group
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H25/00After-treatment of paper not provided for in groups D21H17/00 - D21H23/00
    • D21H25/04Physical treatment, e.g. heating, irradiating
    • D21H25/06Physical treatment, e.g. heating, irradiating of impregnated or coated paper

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Protection Of Plants (AREA)

Abstract

The invention discloses the preparation method of a kind of fiber paper base mulch film, the mixture of ramee or viscose staple fibre or Boehmeria and viscose staple fibre is sheared and carries out pretreatment;Then use chinlon net filtration, filter off serosity, washing, 80 DEG C of drying;Mixture to ramee or viscose staple fibre or Boehmeria and viscose staple fibre adds water and makes fiber dispersion system;Add dispersant, penetrating agent JFC, and stirring, pulling an oar until forming finely dispersed fiber slurry;Pour into fiber slurry chinlon net handshcet former is copied and make handsheet, handsheet is dried to obtain paper mulch sheet semi-finished product;By PVA solution brush on the surface of the mulch film semi-finished product obtained, make its impregnation bubble removing the most side by side by pressure roller extruding, again mulch film semi-finished product are being filled the submergence of liquid paraffin after drying, carrying out an immersing and rolling process;Then carry out preliminary drying and bake;Fiber paper base mulch film prepared by the method has the advantage such as environmental protection, relatively low, the high insulating effect of price, is suitable for large-scale promotion.

Description

A kind of preparation method of fiber paper base mulch film
Technical field
The present invention relates to agricultural installations Material Field, the preparation method of a kind of fiber paper base mulch film.
Background technology
The extensively application of plastic film, to improving crop yield, quality, solves extremely frigid zones and shifts to an earlier date nursery, plantation, with And plantation anti-season vegetable, melon and fruit etc. play very important effect, the use advantage of agricultural film is a lot, but its molecular structure ten Divide stable, be difficult to biodegradation or light degradation voluntarily under natural environment, not only pollute environment and also make farm output and quality Being affected, the recycling of mulch film cost of wasting time and energy is the highest, and general mulch film can exist more than 2 hundred to three hundred in soil Year is non-degradable.In recent years, starch addition type Biodegradable mulch, photodegradation film, Plant fiber ground have the most been developed Film, liquid-state mulch film etc..The primary raw material that wherein starch addition type Biodegradable mulch and photodegradation film use remains plastics And chemical fibre, it is impossible to eradicate " white pollution " problem completely;Plant fiber mulch is primarily referred to as paper mulch sheet;Mainly use paper maker Skill makes paper mulch film, and it is a kind of environment-friendly type mulch film that can be degradable in soil.There is wind resistance rain ability, easily in paper mulch film Broken, the problem such as inapplicable machinery plastic film mulch.Japan develops the paper mulch sheet of different purposes, and such as fiber net type paper mulch film, it is With Plant fiber as primary raw material, it simply being placed into the soil after using, the antibacterial in soil just can be decomposed.
Organic fertilizer type paper mulch film is to be mixed with natural organic phosphatic fertiliser and natural antimicrobial substance in common paper mulch film, is suitable for In extensive range, can be to add containing chitosan and fiber in paper mulch film with the use of biochemical type paper mulch film with variety classes crop The compositions such as element, can promote the breeding of the soil bacteria favourable to crop growth, otherwise, the propagation to virus disease has control With natural control effect, but owing to paper mulch sheet price is the most expensive, use less.New Zealand Murray Cmick shank company grinds Make the Eco.Cover paper mulch film developed in 2,004 2006 years successively in 21, New Zealand, the U.S., European Union, Canada, Germany etc. Country is patented.Paper ground film strength and service life different because of the thickness of film, the degradable time 6 24 months it Between, can need to change properties of product according to production, the primary raw material of this paper mulch film is waste paper, can 100% be biodegradable, cover Lid can reduce moisture evaporation 75%, effectively suppresses weeds, reduces soil erosion, increases soil fertility, promotes plant growing.Additionally The waste liquids such as black liquid are modified by degradable liquid-state mulch film with brown coal, weathered coal or peat, by lignin, cellulose and Polysaccharide forms macromolecule under the effect of cross-linking agent, then mixes system with various additives, siliceous fertilizer trace element, pesticide and herbicide Taking acquisition, the insulation soil moisture conservation effect of this kind of mulch film is poor.
According to statistics, more than 50 ten thousand tons of the discarded natural fiber such as cotton that China produces every year, fiber crops, viscose glue, silkworm silk, and increase year by year Adding, these garbages not only endanger environment, and cause the biggest wasting of resources.As these discarded natural fibers are made agriculture Film, uses about the 10% of total amount by alternative macromolecule agricultural film.The non-woven agricultural film of textile fabric relative to other kinds of can Degradative plastic film, the huge superiority of non-woven mulch film is that its biodegradability, and catabolite can also increase The fertilizer matter of soil, meets the requirement of " ecological agriculture ".But the technology of plant fiber mulch is the most immature, combination property There is also many shortcomings, also have with a certain distance from practical;Therefore need to design a kind of environmental protection, price relatively low, high insulating effect Fiber paper base mulch film.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of fiber paper base mulch film, to solve above-mentioned background technology carries The problem gone out.
For achieving the above object, the present invention provides following technical scheme: the preparation method of a kind of fiber paper base mulch film, step As follows:
Step one, the mixture of ramee or viscose staple fibre or Boehmeria and viscose staple fibre is sheared into
Row pretreatment;
Step 2, mixed by through the ramee of step one pretreatment or viscose staple fibre or Boehmeria and viscose staple fibre Compound chinlon net filtration, filters off serosity, and washing, 80 DEG C of drying are stand-by;
The mixture of step 3, the ramee obtained to step 2 or viscose staple fibre or Boehmeria and viscose staple fibre adds Water makes fiber dispersion system;
Step 4, fiber dispersion system in step 3 add dispersant, penetrating agent JFC, and stir, pull an oar until shape Become finely dispersed fiber slurry;
Step 5, pour into the fiber slurry in step 4 chinlon net handshcet former is copied and make handsheet, handsheet is done Dry obtain paper mulch sheet semi-finished product;
Step 6, the surface of the mulch film semi-finished product obtained in step 5 by PVA solution brush, make it soak by pressure roller extruding Glue bubble removing, in an oven drying forming the most side by side;
Step 7, by step 6 prepare paper mulch sheet semi-finished product be totally submerged in the maceration tank fill liquid paraffin, Laboratory mangle carries out an immersing and rolling process;
Step 8, the paper mulch sheet semi-finished product processed through step 7 are put in an oven, carry out preliminary drying and bake.
Preferably, by the ramee in described step one or viscose staple fibre or Boehmeria and the mixture of viscose staple fibre Cut into the segment of 3mm-8mm.
Preferably, the pretreatment in described step one is by the ramee sheared or viscose staple fibre or Boehmeria and to glue The mixture dedusting remove impurity of glue chopped fiber, then shredding mixing is warming up to 100 DEG C in thermostat water bath, and 30min, bath raio are boiled in boiling For 60:1, in the solution of thermostat water bath, the mass fraction of NaOH is 3%, and the mass fraction of penetrating agent JFC is 1%-1.5%, H2O2Mass fraction be 6%.
Preferably, the chinlon network planning lattice in described step 2 are 40 × 40cm2, 200 mesh, Gram Mass 30g/m2-40g/ m2
Preferably, in the fiber dispersion system that described step 3 prepares, the mass percent concentration of ramee is 10%, Bath raio is 400:1.
Preferably, the penetrating agent JFC consumption in described step 4 is ramee or viscose staple fibre or Boehmeria and viscose glue The 15%-20% of the quality of the mixture of chopped fiber, in fiber slurry, the mass fraction of dispersant is 1%.
Preferably, the dry in the sun environment of described step 5 is room temperature 18 DEG C-25 DEG C, relative humidity 30%-60%, and chinlon net is 200 mesh.
Preferably, in the PVA solution in described step 6, the mass fraction of PVA controls is 3%, and oven temperature controls 50 ℃。
Preferably, in described step 7, the time of submergence is 1min-3min.
Preferably, the preliminary drying control temperature in described step 8 is at 40 DEG C-50 DEG C, with the speed of 5 DEG C/min after preliminary drying 30min Degree is warming up to 110 DEG C, bakes 3min.
Compared with prior art, the invention has the beneficial effects as follows: utilize the textile mills such as discarded Boehmeria and short rayon fiber to give up Abandoning raw material, abundant raw material, it is possible to decrease cost, the cost producing paper mulch sheet is only the half of dry non-woven cloth, product appearance Performance is close to plastic film, and compactness is high, and light transmission is preferable, and Gram Mass is up to 30g/m2-40g/m2, film thickness is 0.2mm- 0.4mm;Impregnated by preferred promoter, adjuvant and paraffin, preliminary drying and bake etc. after operation processes, the fracture of fiber paper base mulch film is strong Power can reach 39N-70N, elongation at break up to 3.8%-4.6%, it is seen that light light transmittance reaches 50%-75%, and breathability reaches 2500mm/s-4000mm/s, the degradable time be less than 90 days, greatly reduce " white pollution ", hydrone can not pass through substantially Face penetrates into, and water repellency is preferable, and covering with ground sheeting effect is close with plastic film.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be clearly and completely described below, it is clear that described enforcement Example is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this area is common The every other embodiment that technical staff is obtained under not making creative work premise, broadly falls into the model of present invention protection Enclose.
Embodiment 1.
Step is as follows:
Step one, the segment that ramee cuts into 3-5mm carry out pretreatment, and pretreatment is that the Boehmeria that will have sheared is fine Dimension dedusting remove impurity, shredding mixes, is then warming up to 100 DEG C in thermostat water bath, and 30min is boiled in boiling, and bath raio is 60:1, thermostatted water In the solution of bath, the mass fraction of NaOH is 3%, and the mass fraction of penetrating agent JFC is 1%, H2O2Mass fraction be 6%; The short fine abundance of discarded Boehmeria, is the first-selection manufacturing non-woven material in textile fabric, is possible not only in soil the most certainly So degraded, and do not injure soil, crops yield and quality is also had no adverse effects;Ramee intensity is big, can be to a certain extent Increase the dry and wet intensity of goods;Ramee has hydrophilic simultaneously, can fully swollen and fibrillating in pulping process;
Step 2, by the chinlon net filtration of the ramee through step one pretreatment, chinlon network planning lattice are 40 × 40cm2、 200 mesh, Gram Mass 30g/m2, filtering off serosity, washing, 80 DEG C of drying are stand-by;
Step 3, the ramee obtaining step 2 add water and make fiber dispersion system, prepared fiber dispersion system The mass percent concentration of middle ramee is 10%, and bath raio is 400:1;
Step 4, fiber dispersion system in step 3 add dispersant, penetrating agent JFC so that chopped fiber is in water It is dispersed into ultimate fibre shape, is beneficial to making beating uniformly;Penetrating agent JFC consumption is the 15% of the quality of ramee, divides in fiber slurry The mass fraction of powder is 1%, and stirring, pulling an oar until forming finely dispersed fiber slurry;
Step 5, pour into the fiber slurry in step 4 chinlon net handshcet former is copied and make handsheet, handsheet is dried in the air Shining 24h or oven drying at low temperature, dry in the sun environment is room temperature 18 DEG C, relative humidity 30%, and chinlon net is 200 mesh, obtains paper mulch sheet half Finished product;
Step 6, the surface of the mulch film semi-finished product obtained in step 5 by PVA solution brush, make it soak by pressure roller extruding Glue bubble removing, in an oven drying forming the most side by side, in PVA solution, the mass fraction of PVA controls is 3%, oven temperature control System is at 50 DEG C;
Step 7, by step 6 prepare paper mulch sheet semi-finished product be totally submerged in the maceration tank fill liquid paraffin 1min, makes liquid paraffin be fully infiltrated in mulch film semi-finished product, carries out an immersing and rolling process, be remarkably improved system on laboratory mangle The water repellency of product and light transmission;
Step 8, the paper mulch sheet semi-finished product processed through step 7 are put in an oven, carry out preliminary drying and make it the most viscous Closing, then high temperature bakes sizing, preliminary drying control temperature, at 40 DEG C, is warming up to 110 DEG C with the speed of 5 DEG C/min after preliminary drying 30min, roasting Drying 3min to shape, both having prepared surface density is 35+5g/m2Fiber paper base mulch film;
Embodiment 2.
Step is as follows:
Step one, the segment that viscose staple fibre cuts into 5-8mm carry out pretreatment, and pretreatment is the viscose glue that will have sheared Chopped fiber dedusting remove impurity, shredding mixing (1:1), in thermostat water bath, then it is warming up to 100 DEG C, 30min is boiled in boiling, and bath raio is 60:1, in the solution of thermostat water bath, the mass fraction of NaOH is 3%, and the mass fraction of penetrating agent JFC is 1.5%, H2O2Matter Amount mark is 6%;Viscose staple fibre abundance, is the first-selection manufacturing non-woven material in textile fabric, is possible not only at soil Complete natural degradation in earth, and do not injure soil, crops yield and quality is also had no adverse effects;
Step 2, by the short rayon fiber Wesy chinlon net filtration through step one pretreatment, chinlon network planning lattice are 40 × 40cm2, 200 mesh, Gram Mass 40g/m2, filtering off serosity, washing, 80 DEG C of drying are stand-by;
Step 3, the viscose staple fibre obtaining step 2 add water and make fiber dispersion system, prepared fiber dispersion In system, the mass percent concentration of ramee is 10%, and bath raio is 400:1;
Step 4, fiber dispersion system in step 3 add dispersant, penetrating agent JFC so that chopped fiber is in water It is dispersed into ultimate fibre shape, is beneficial to making beating uniformly;Penetrating agent JFC consumption is the 20% of the quality of viscose staple fibre, in fiber slurry The mass fraction of dispersant is 1%, and stirring, pulling an oar until forming finely dispersed fiber slurry;
Step 5, pour into the fiber slurry in step 4 chinlon net handshcet former is copied and make handsheet, handsheet is dried in the air Shining 24h or oven drying at low temperature, dry in the sun environment is room temperature 25 DEG C, relative humidity 60%, and chinlon net is 200 mesh, obtains paper mulch sheet half Finished product;
Step 6, the surface of the mulch film semi-finished product obtained in step 5 by PVA solution brush, make it soak by pressure roller extruding Glue bubble removing, in an oven drying forming the most side by side, in PVA solution, the mass fraction of PVA controls is 3%, oven temperature control System is at 50 DEG C;
Step 7, by step 6 prepare paper mulch sheet semi-finished product be totally submerged in the maceration tank fill liquid paraffin 3min, makes liquid paraffin be fully infiltrated in mulch film semi-finished product, carries out an immersing and rolling process, be remarkably improved system on laboratory mangle The water repellency of product and light transmission;
Step 8, the paper mulch sheet semi-finished product processed through step 7 are put in an oven, carry out preliminary drying and make it the most viscous Closing, then high temperature bakes sizing, preliminary drying control temperature, at 50 DEG C, is warming up to 110 DEG C, bakes 3min and shape after preliminary drying 30min, Both having prepared surface density is 35+5g/m2Fiber paper base mulch film.
The main performance of fiber paper base mulch film such as following table:
According to the fiber mulch film that above method prepares there is good mechanical property and ventilating water seepage, thickness 0.308cm, Air penetrability 3352mm/s, bending resistance length 87g cm, it is seen that light light transmittance is up to 77.8%, ultimate strength 64N, hydroscopicity 5.93%, the degraded degradation rate of 44 days of placing into the soil reaches more than 90%, basically reaches the requirement of strength of common agricultural mulching, degraded Cycle substantially meets the covering demand of the whole trophophase of common crops, is a kind of agricultural mulching with bigger market potential;Cause This this fiber paper base mulch film has the advantage such as environmental protection, relatively low, the high insulating effect of price, is suitable for large-scale promotion.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, permissible Understand and these embodiments can be carried out multiple change without departing from the principles and spirit of the present invention, revise, replace And modification, the scope of the present invention be defined by the appended.

Claims (10)

1. the preparation method of a fiber paper base mulch film, it is characterised in that step is as follows:
Step one, the mixture of ramee or viscose staple fibre or Boehmeria and viscose staple fibre is sheared carry out pretreatment;
Step 2, will use through the mixture of the ramee of step one pretreatment or viscose staple fibre or Boehmeria and viscose staple fibre Chinlon net filtration, filters off serosity, and washing, 80 DEG C of drying are stand-by;
Step 3, the ramee obtained to step 2 or the mixture system of adding water of viscose staple fibre or Boehmeria and viscose staple fibre Become fiber dispersion;
Step 4, fiber dispersion system in step 3 add dispersant, penetrating agent JFC, and stir, pull an oar until being formed and dividing Dissipate uniform fiber slurry;
Step 5, pour into the fiber slurry in step 4 chinlon net handshcet former is copied and make handsheet, handsheet is dried To paper mulch sheet semi-finished product;
Step 6, the surface of the paper mulch sheet semi-finished product obtained in step 5 by PVA solution brush, make it soak by pressure roller extruding Glue bubble removing, in an oven drying forming the most side by side;
Step 7, by step 6 prepare paper mulch sheet semi-finished product be totally submerged in the maceration tank fill liquid paraffin, little An immersing and rolling process is carried out on padding machine;
Step 8, the paper mulch sheet semi-finished product processed through step 7 are put in an oven, carry out preliminary drying and bake.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: by described step one Ramee or the mixture of viscose staple fibre or Boehmeria and viscose staple fibre cut into the segment of 3mm-8mm.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: in described step one Pretreatment is by the mixture dedusting remove impurity of the ramee sheared or viscose staple fibre or Boehmeria and viscose staple fibre, shredding Then mixing is placed in thermostat water bath, is warming up to 100 DEG C, and 30min is boiled in boiling, and bath raio is 60:1, in the solution of thermostat water bath The mass fraction of NaOH is 3%, and the mass fraction of penetrating agent JFC is 1%-1.5%, H2O2Mass fraction be 6%.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: in described step 2 Chinlon network planning lattice are 40 × 40cm2, 200 mesh, Gram Mass 30g/m2-40g/m2
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: described step 3 prepares Fiber dispersion system in the mass percent concentration of ramee be 10%, bath raio is 400:1.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: in described step 4 Penetrating agent JFC consumption is the 15%-of the quality of the mixture of ramee or viscose staple fibre or Boehmeria and viscose staple fibre 20%, in fiber slurry, the mass fraction of dispersant is 1%.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: doing of described step 5 Dry dry in the sun environment is room temperature 18 DEG C-25 DEG C, relative humidity 30%-60%, and chinlon net is 200 mesh.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: in described step 6 In PVA solution, the mass fraction of PVA controls is 3%, and oven temperature controls at 50 DEG C.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: will in described step 7 The time that paper mulch sheet semi-finished product are totally submerged is 1min-3min.
The preparation method of a kind of fiber paper base mulch film the most according to claim 1, it is characterised in that: in described step 8 Preliminary drying control temperature at 40 DEG C-50 DEG C, be warming up to 110 DEG C with the speed of 5 DEG C/min after preliminary drying 30min, bake 3min.
CN201610550123.1A 2016-07-13 2016-07-13 A kind of preparation method of fiber paper base mulch Active CN106168002B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610550123.1A CN106168002B (en) 2016-07-13 2016-07-13 A kind of preparation method of fiber paper base mulch

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610550123.1A CN106168002B (en) 2016-07-13 2016-07-13 A kind of preparation method of fiber paper base mulch

Publications (2)

Publication Number Publication Date
CN106168002A true CN106168002A (en) 2016-11-30
CN106168002B CN106168002B (en) 2018-06-15

Family

ID=58065227

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610550123.1A Active CN106168002B (en) 2016-07-13 2016-07-13 A kind of preparation method of fiber paper base mulch

Country Status (1)

Country Link
CN (1) CN106168002B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776661A (en) * 2019-10-25 2020-02-11 东华大学 Method for preparing waterproof environment-friendly bast fiber film by using carboxymethyl cellulose as film forming agent
CN111749041A (en) * 2020-07-16 2020-10-09 东北农业大学 Secondary fiber-based insect-resistant full-degradable mulching film for cigarettes and manufacturing method thereof
CN114892444A (en) * 2022-05-07 2022-08-12 南京林业大学 Paper-based mulching film and preparation method and application thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4306441C1 (en) * 1993-03-02 1994-04-28 Wibmer & Co Kg Biodegradable moulded bodies for use as plant pots - consist of natural plant or animal fibres impregnated with potato pulp in which the potato pulp particles are smaller than 350 microns
CN1217351A (en) * 1998-09-23 1999-05-26 湖北省轻工业科学研究设计院 Farm plant fiber mulch and producing method therefor
CN1559176A (en) * 2004-03-03 2005-01-05 中国农业科学院麻类研究所 Environmental protection type base fibre film, and its mfg. process
CN101629398A (en) * 2009-06-08 2010-01-20 江南大学 Naturally degradative cotton linter plastic film and manufacture process thereof
CN103243480A (en) * 2013-05-10 2013-08-14 安徽农业大学 Method for manufacturing non-woven seedling-growing culture medium by using rice straw fibers and ramie fibers
CN105178094A (en) * 2015-06-17 2015-12-23 华南理工大学 Agricultural degradable thermal-insulation mulch film manufacturing method

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4306441C1 (en) * 1993-03-02 1994-04-28 Wibmer & Co Kg Biodegradable moulded bodies for use as plant pots - consist of natural plant or animal fibres impregnated with potato pulp in which the potato pulp particles are smaller than 350 microns
CN1217351A (en) * 1998-09-23 1999-05-26 湖北省轻工业科学研究设计院 Farm plant fiber mulch and producing method therefor
CN1559176A (en) * 2004-03-03 2005-01-05 中国农业科学院麻类研究所 Environmental protection type base fibre film, and its mfg. process
CN101629398A (en) * 2009-06-08 2010-01-20 江南大学 Naturally degradative cotton linter plastic film and manufacture process thereof
CN103243480A (en) * 2013-05-10 2013-08-14 安徽农业大学 Method for manufacturing non-woven seedling-growing culture medium by using rice straw fibers and ramie fibers
CN105178094A (en) * 2015-06-17 2015-12-23 华南理工大学 Agricultural degradable thermal-insulation mulch film manufacturing method

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张晓丽 等: ""木屑/粘胶纤维湿法非织造地膜的研制"", 《纺织学报》 *
张燕杰 等: ""完全降解纸基棉质地膜的制备及性能研究"", 《产业用纺织品》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110776661A (en) * 2019-10-25 2020-02-11 东华大学 Method for preparing waterproof environment-friendly bast fiber film by using carboxymethyl cellulose as film forming agent
CN111749041A (en) * 2020-07-16 2020-10-09 东北农业大学 Secondary fiber-based insect-resistant full-degradable mulching film for cigarettes and manufacturing method thereof
CN114892444A (en) * 2022-05-07 2022-08-12 南京林业大学 Paper-based mulching film and preparation method and application thereof

Also Published As

Publication number Publication date
CN106168002B (en) 2018-06-15

Similar Documents

Publication Publication Date Title
FI125943B (en) Substrate structures based on moss moss and a method for making them
CN106168002B (en) A kind of preparation method of fiber paper base mulch
CN101629398A (en) Naturally degradative cotton linter plastic film and manufacture process thereof
CN106718414A (en) A kind of degradable high-performance string synthesis agricultural mulching and preparation method thereof
CN102943414A (en) High-water repellency high-photopermeability biodegradable cotton agricultural thin film
CN102613040A (en) Soybean stalk fiber mulch
CN107687109A (en) A kind of agricultural paper mulch film of environment-friendly degradable and its manufacture method
CN105753599A (en) Total-alga biological mulching film and method for preparing same
CN102517798B (en) Mulching film and preparation method thereof
CN108396559A (en) A kind of bagasse base film and preparation method thereof
CN111040210A (en) Method for producing mulching film by using crop straws and mulching film
CN101509210B (en) Paper-pulp
CN102283057B (en) Method for manufacturing slurry-processed multifunction organic environmental-protection flaky mulching film
CN112442922A (en) Method for producing degradable mulching film paper by using bamboo pulp
CN102283056B (en) Method for manufacturing paper making-process multifunction organic environmental-protection flaky mulching film
CN107955985B (en) Preparation method of bamboo charcoal fiber
CN110409055A (en) In the method for straw preparation tubular type non-woven fabrics
CN106544787A (en) A kind of production technology of the non-woven new material with degradation function
CN107523080B (en) Ground surface covering and preparation method thereof
Chokboribal et al. Tapioca starch/PVA plastic films with water hyacinth powder: Enhanced stability in direct contact with moisture
CN106995939A (en) The method that Jujun grasses fibrillation is produced using chemical method
CN102246654B (en) Seedling raising and planting method for apocynum venetum
Li et al. Preparation and research of environment-friendly degradable paper mulching film of cotton stalk fiber
CN110760087A (en) Wind-resistant cold-resistant decomposable agricultural mulching film suitable for cotton field plain and preparation method thereof
CN110591260A (en) Spraying type degradable mulching film material special for dry land and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant