CN106147992A - A kind of preparation method of fragrant vegetable seed oil - Google Patents
A kind of preparation method of fragrant vegetable seed oil Download PDFInfo
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- CN106147992A CN106147992A CN201610698906.4A CN201610698906A CN106147992A CN 106147992 A CN106147992 A CN 106147992A CN 201610698906 A CN201610698906 A CN 201610698906A CN 106147992 A CN106147992 A CN 106147992A
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- seed oil
- caraway seeds
- vegetable seed
- fragrant vegetable
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Fats And Perfumes (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses the preparation method of a kind of fragrant vegetable seed oil, including: (1) pulverizes；(2) enzymolysis；(3) extraction；(4) refine；(5) packaging.The preparation method of the fragrant vegetable seed oil that the present invention provides, preparation is simple, and whole process does not use any toxic reagent, safety and Health, environmental protection, and extraction ratio is up to 87.4%, improves income 32.2%；Caraway seeds slurry compound enzyme is carried out enzymolysis processing, destroys cellularity and macromole nutritional labeling, improve oil extraction rate；Caraway seeds powder extracts through twice reflow of alcohol, fully extracts oils and fats and flavor component, improves extraction ratio, aromatic flavor；After adding boiling water, insulation stands, and abundant degumming improves the quality scale of fragrant vegetable seed oil.
Description
Technical field
The invention mainly relates to edible oil processing technique field, particularly relate to the preparation method of a kind of fragrant vegetable seed oil.
Background technology
Caraway seeds, another name: coriander seed, pine palpus Semen Allii Tuberosi, Herba Coriandri seed, the namely fruit of Herba Coriandri, when Herba Coriandri length is white to outputing
After color little Hua, cross and shortly can bear fruit.Caraway seeds surface is fallow, and mature fruit is hard, and gas fragrance, with gentleness
Fragrance and Salvia japonica Thunb. and the mixing taste of Fructus Citri Limoniae, containing volatile oil, malic acid, potassium salt, organic acid calcium salt, fat, protein, many
Plant vitamin and nitrogen substance, there is various health-care, it is possible to protection the intestines and stomach, kill fish raw meat poison, control anal fistula proctoptosis, only tooth
Bitterly, solve alimentary toxicosis, promote wound healing, cardioprotection.
Research shows, fragrant vegetable seed oil aromatic flavor, and bactericidal effect is obvious, it is possible to enhancing immunity, and auxiliary treats chronic disease
Disease, but fragrant vegetable seed oil in the market is the most few, it is impossible to meet consumer demand, and currently there are no complete system
The literature method of standby fragrant vegetable seed oil, therefore caraway seeds is prepared as fragrant vegetable seed oil is that market is needed badly, increases the Herba Coriandri on market and produces
Product, hence it is evident that improve the added value of Herba Coriandri, improve the income of peasant household.
Summary of the invention
In order to make up the defect of prior art, it is an object of the invention to provide the preparation method of a kind of fragrant vegetable seed oil.
The preparation method of a kind of fragrant vegetable seed oil, specifically includes following steps:
(1) pulverize: select caraway seeds full, ripe, without disease pest, after carrying out selecting crude drugs with winnower, screening, be placed in clear water and clean, dewatering,
It is crushed to 80 ~ 100 mesh, obtains caraway seeds powder, in caraway seeds powder, add the distilled water of caraway seeds weight 1.6 ~ 1.8 times amount, stirring
Uniformly, caraway seeds slurry is obtained；
(2) enzymolysis: adding compound enzyme in caraway seeds slurry, mass concentration is 0.06 ~ 0.08%, after mix homogeneously, in 40 ~ 42
DEG C stirring enzymolysis 200 ~ 220 minutes, destroys cellularity, decomposes macromole nutritional labeling, promote oil extraction, big fire boil to
Water content is 25 ~ 30%, obtains enzymolysis caraway seeds powder；
(3) extraction: add the food that volume fraction is 82 ~ 84% of enzymolysis caraway seeds grain weight amount 2 ~ 3 times amount in enzymolysis caraway seeds powder
With alcoholic solution, after backflow extraction, obtain lixiviating solution and caraway seeds granulated slag, add in caraway seeds granulated slag caraway seeds granulated slag weight 2 ~
The volume fraction of 3 times amount is the edible alcohol solution of 86 ~ 88%, repeats backflow extraction, fully extracts oils and fats, merge all extractions
Liquid, is concentrated into constancy of volume in 46 ~ 48 DEG C of vacuum rotatings, obtains thick fragrant vegetable seed oil；
(4) refine: add the boiling water of thick fragrant vegetable seed oil weight 35 ~ 40% in thick fragrant vegetable seed oil, 40 ~ 42 revs/min of limits are stirred,
Limit heating keeps micro-boiling 10 ~ 15 minutes, insulation standing 90 ~ 100 minutes, carries out hyperfiltration through the filter membrane of 0.22 μm, removes glue
Body impurity, keeps oil body stable, removes precipitation, by supernatant in 52 ~ 54 DEG C of rotary evaporation in vacuo to without moisture, removes moisture,
Fragrant vegetable seed oil；
(5) packaging: packaging, in 7000 ~ 8000uW/c ultraviolet-sterilization 20 ~ 25 minutes, inspection, obtains finished product.
The compound enzyme of described step (2), is made up of the enzyme preparation of following weight ratio: cellulase: amylase: protease:
Pectase=23 ~ 25:15 ~ 17:12 ~ 14:9 ~ 11, enzyme activity is 2700 ~ 2900U/mg.
Fragrant vegetable seed oil prepared by the preparation method of described a kind of fragrant vegetable seed oil.
The invention have the advantage that the preparation method of a kind of fragrant vegetable seed oil that the present invention provides, preparation is simple, and whole process is not
Using any toxic reagent, safety and Health, environmental protection, extraction ratio is up to 87.4%, improves income 32.2%；By caraway seeds
Slurry compound enzyme carries out enzymolysis processing, destroys cellularity and macromole nutritional labeling, improves oil extraction rate；Caraway seeds powder
Extract through twice reflow of alcohol, fully extract oils and fats and flavor component, improve extraction ratio, aromatic flavor；It is incubated after adding boiling water
Stand, abundant degumming, improve the quality scale of fragrant vegetable seed oil, meet nutrition and the health demand of consumer.
Detailed description of the invention
With specific embodiment, the present invention is described below.
Embodiment 1
The preparation method of a kind of fragrant vegetable seed oil, specifically includes following steps:
(1) pulverize: select caraway seeds full, ripe, without disease pest, after carrying out selecting crude drugs with winnower, screening, be placed in clear water and clean, dewatering,
It is crushed to 80 mesh, obtains caraway seeds powder, in caraway seeds powder, add the distilled water of caraway seeds weight 1.6 times amount, stir, obtain fragrant
Semen Allii Tuberosi slurry；
(2) enzymolysis: adding compound enzyme in caraway seeds slurry, mass concentration is 0.06%, after mix homogeneously, stirs enzyme in 40 DEG C
Solve 200 minutes, destroy cellularity, decompose macromole nutritional labeling, promote oil extraction, big fire boil to water content be 25%,
Obtain enzymolysis caraway seeds powder；
(3) extraction: add the edible wine that volume fraction is 82% of enzymolysis caraway seeds grain weight amount 2 times amount in enzymolysis caraway seeds powder
Essence solution, after backflow extraction, obtains lixiviating solution and caraway seeds granulated slag, adds caraway seeds granulated slag weight 2 times amount in caraway seeds granulated slag
The edible alcohol solution that volume fraction is 86%, repeat backflow extraction, fully extract oils and fats, merge all lixiviating solution, in 46 DEG C
Vacuum rotating is concentrated into constancy of volume, obtains thick fragrant vegetable seed oil；
(4) refine: adding the boiling water of thick fragrant vegetable seed oil weight 35% in thick fragrant vegetable seed oil, 40 revs/min of limit stirrings, limit is heated
Keeping micro-boiling 10 minutes, insulation stands 90 minutes, carries out hyperfiltration through the filter membrane of 0.22 μm, removes colloidal impurity, keep oil
Body is stable, removes precipitation, by supernatant in 52 DEG C of rotary evaporation in vacuo to without moisture, removes moisture, obtains fragrant vegetable seed oil；
(5) packaging: packaging, in 7000uW/c ultraviolet-sterilization 20 minutes, inspection, obtains finished product.
The compound enzyme of described step (2), is made up of the enzyme preparation of following weight ratio: cellulase: amylase: protease:
Pectase=23:15:12:9, enzyme activity is 2700 ~ 2900U/mg.
Embodiment 2
The preparation method of a kind of fragrant vegetable seed oil, specifically includes following steps:
(1) pulverize: select caraway seeds full, ripe, without disease pest, after carrying out selecting crude drugs with winnower, screening, be placed in clear water and clean, dewatering,
It is crushed to 100 mesh, obtains caraway seeds powder, in caraway seeds powder, add the distilled water of caraway seeds weight 1.7 times amount, stir,
Caraway seeds slurry；
(2) enzymolysis: adding compound enzyme in caraway seeds slurry, mass concentration is 0.07%, after mix homogeneously, stirs enzyme in 41 DEG C
Solve 210 minutes, destroy cellularity, decompose macromole nutritional labeling, promote oil extraction, big fire boil to water content be 28%,
Obtain enzymolysis caraway seeds powder；
(3) extraction: add in enzymolysis caraway seeds powder the volume fraction of enzymolysis caraway seeds grain weight amount 2.5 times amount be 83% edible
Alcoholic solution, after backflow extraction, obtains lixiviating solution and caraway seeds granulated slag, adds caraway seeds granulated slag weight 2.5 in caraway seeds granulated slag
The volume fraction of times amount is the edible alcohol solution of 87%, repeats backflow extraction, fully extracts oils and fats, merge all lixiviating solution, in
47 DEG C of vacuum rotatings are concentrated into constancy of volume, obtain thick fragrant vegetable seed oil；
(4) refine: adding the boiling water of thick fragrant vegetable seed oil weight 38% in thick fragrant vegetable seed oil, 41 revs/min of limit stirrings, limit is heated
Keeping micro-boiling 13 minutes, insulation stands 95 minutes, carries out hyperfiltration through the filter membrane of 0.22 μm, removes colloidal impurity, keep oil
Body is stable, removes precipitation, by supernatant in 53 DEG C of rotary evaporation in vacuo to without moisture, removes moisture, obtains fragrant vegetable seed oil；
(5) packaging: packaging, in 8000uW/c ultraviolet-sterilization 23 minutes, inspection, obtains finished product.
The compound enzyme of described step (2), is made up of the enzyme preparation of following weight ratio: cellulase: amylase: protease:
Pectase=24:16:13:10, enzyme activity is 2700 ~ 2900U/mg.
Embodiment 3
The preparation method of a kind of fragrant vegetable seed oil, specifically includes following steps:
(1) pulverize: select caraway seeds full, ripe, without disease pest, after carrying out selecting crude drugs with winnower, screening, be placed in clear water and clean, dewatering,
It is crushed to 100 mesh, obtains caraway seeds powder, in caraway seeds powder, add the distilled water of caraway seeds weight 1.8 times amount, stir,
Caraway seeds slurry；
(2) enzymolysis: adding compound enzyme in caraway seeds slurry, mass concentration is 0.08%, after mix homogeneously, stirs enzyme in 42 DEG C
Solve 220 minutes, destroy cellularity, decompose macromole nutritional labeling, promote oil extraction, big fire boil to water content be 30%,
Obtain enzymolysis caraway seeds powder；
(3) extraction: add the edible wine that volume fraction is 84% of enzymolysis caraway seeds grain weight amount 3 times amount in enzymolysis caraway seeds powder
Essence solution, after backflow extraction, obtains lixiviating solution and caraway seeds granulated slag, adds caraway seeds granulated slag weight 3 times amount in caraway seeds granulated slag
The edible alcohol solution that volume fraction is 88%, repeat backflow extraction, fully extract oils and fats, merge all lixiviating solution, in 48 DEG C
Vacuum rotating is concentrated into constancy of volume, obtains thick fragrant vegetable seed oil；
(4) refine: adding the boiling water of thick fragrant vegetable seed oil weight 40% in thick fragrant vegetable seed oil, 42 revs/min of limit stirrings, limit is heated
Keeping micro-boiling 15 minutes, insulation stands 100 minutes, carries out hyperfiltration through the filter membrane of 0.22 μm, removes colloidal impurity, keep oil
Body is stable, removes precipitation, by supernatant in 54 DEG C of rotary evaporation in vacuo to without moisture, removes moisture, obtains fragrant vegetable seed oil；
(5) packaging: packaging, in 8000uW/c ultraviolet-sterilization 25 minutes, inspection, obtains finished product.
The compound enzyme of described step (2), is made up of the enzyme preparation of following weight ratio: cellulase: amylase: protease:
Pectase=25:17:14:11, enzyme activity is 2700 ~ 2900U/mg.
Comparative example
The preparation method of existing fragrant vegetable seed oil.
The mensuration of each index of embodiment fragrant vegetable seed oil:
According to GB1534-2003, the fragrant vegetable seed oil preparing embodiment detects, each index of embodiment fragrant vegetable seed oil
Measurement result is shown in Table 1.
Table 1: the measurement result of each index of embodiment fragrant vegetable seed oil
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Abnormal smells from the patient | Delicate fragrance, free from extraneous odour | Delicate fragrance, free from extraneous odour | Delicate fragrance, free from extraneous odour |
| Moisture/(%) | 0.02 | 0.01 | 0.02 |
| Insoluble impurities/(%) | 0.02 | 0.02 | 0.01 |
| Solvent residual amount/(mg/kg) | Nothing | Nothing | Nothing |
| Peroxide value/(mmol/kg) | 1.3 | 1.4 | 1.1 |
The result of table 1 shows, fragrant vegetable seed oil prepared by the preparation method of the fragrant vegetable seed oil of embodiment, delicate fragrance, free from extraneous odour, moisture,
Insoluble impurities, solvent residual amount, peroxide value are below national standard, safety and Health.
Embodiment and the index evaluation of comparative example fragrant vegetable seed oil preparation method:
Fragrant vegetable seed oil, embodiment and the finger of comparative example fragrant vegetable seed oil preparation method is prepared respectively by the method for embodiment and comparative example
Mark evaluation is shown in Table 2.
Table 2: embodiment and the index evaluation of comparative example fragrant vegetable seed oil preparation method
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example |
| Extraction ratio/(%) | 87.2 | 86.8 | 87.4 | 24.7 |
| Improve income/(%) | 32.1 | 32.2 | 31.7 | — |
Note: " " indicate without.
The result of table 2 shows, the preparation method of the fragrant vegetable seed oil of embodiment, and relative to comparative example, extraction rate reached arrives
87.4%, improve income 32.2%, illustrate that the preparation method of the fragrant vegetable seed oil that the present invention provides has wide market prospect.
Claims (3)
1. the preparation method of a fragrant vegetable seed oil, it is characterised in that specifically include following steps:
(1) pulverize: select caraway seeds full, ripe, without disease pest, after carrying out selecting crude drugs with winnower, screening, be placed in clear water and clean, dewatering,
It is crushed to 80 ~ 100 mesh, obtains caraway seeds powder, in caraway seeds powder, add the distilled water of caraway seeds weight 1.6 ~ 1.8 times amount, stirring
Uniformly, caraway seeds slurry is obtained；
(2) enzymolysis: adding compound enzyme in caraway seeds slurry, mass concentration is 0.06 ~ 0.08%, after mix homogeneously, in 40 ~ 42
DEG C stirring enzymolysis 200 ~ 220 minutes, it is 25 ~ 30% that big fire is boiled to water content, obtains enzymolysis caraway seeds powder；
(3) extraction: add the food that volume fraction is 82 ~ 84% of enzymolysis caraway seeds grain weight amount 2 ~ 3 times amount in enzymolysis caraway seeds powder
With alcoholic solution, after backflow extraction, obtain lixiviating solution and caraway seeds granulated slag, add in caraway seeds granulated slag caraway seeds granulated slag weight 2 ~
The volume fraction of 3 times amount is the edible alcohol solution of 86 ~ 88%, repeats backflow extraction, merges all lixiviating solution, true in 46 ~ 48 DEG C
Empty spin concentration, to constancy of volume, obtains thick fragrant vegetable seed oil；
(4) refine: add the boiling water of thick fragrant vegetable seed oil weight 35 ~ 40% in thick fragrant vegetable seed oil, 40 ~ 42 revs/min of limits are stirred,
Limit heating keeps micro-boiling 10 ~ 15 minutes, insulation standing 90 ~ 100 minutes, carries out hyperfiltration through the filter membrane of 0.22 μm, and it is heavy to remove
Form sediment, by supernatant in 52 ~ 54 DEG C of rotary evaporation in vacuo to without moisture, obtain fragrant vegetable seed oil；
(5) packaging: packaging, in 7000 ~ 8000uW/c ultraviolet-sterilization 20 ~ 25 minutes, inspection, obtains finished product.
The preparation method of fragrant vegetable seed oil the most according to claim 1, it is characterised in that the compound enzyme of described step (2), by with
The enzyme preparation composition of lower weight ratio: cellulase: amylase: protease: pectase=23 ~ 25:15 ~ 17:12 ~ 14:9 ~ 11, enzyme
Vigor is 2700 ~ 2900U/mg.
Fragrant vegetable seed oil prepared by the preparation method of fragrant vegetable seed oil the most according to claim 1 or claim 2.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610698906.4A CN106147992A (en) | 2016-08-22 | 2016-08-22 | A kind of preparation method of fragrant vegetable seed oil |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610698906.4A CN106147992A (en) | 2016-08-22 | 2016-08-22 | A kind of preparation method of fragrant vegetable seed oil |
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| CN201610698906.4A Pending CN106147992A (en) | 2016-08-22 | 2016-08-22 | A kind of preparation method of fragrant vegetable seed oil |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109054991A (en) * | 2018-08-31 | 2018-12-21 | 湖南华诚生物资源股份有限公司 | A method of extracting arhat fruit seed oil from arhat fruit seed |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102250679A (en) * | 2011-06-09 | 2011-11-23 | 安徽中草香料有限公司 | Preparation process for fragrant vegetable seed oil |
| CN104745290A (en) * | 2015-04-20 | 2015-07-01 | 江苏金洲粮油食品有限公司 | High-oil-yield sunflower seed oil extraction production process |
-
2016
- 2016-08-22 CN CN201610698906.4A patent/CN106147992A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102250679A (en) * | 2011-06-09 | 2011-11-23 | 安徽中草香料有限公司 | Preparation process for fragrant vegetable seed oil |
| CN104745290A (en) * | 2015-04-20 | 2015-07-01 | 江苏金洲粮油食品有限公司 | High-oil-yield sunflower seed oil extraction production process |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109054991A (en) * | 2018-08-31 | 2018-12-21 | 湖南华诚生物资源股份有限公司 | A method of extracting arhat fruit seed oil from arhat fruit seed |
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