CN106147551A - A kind of preparation method of alkyd resin fire-retardant paint - Google Patents
A kind of preparation method of alkyd resin fire-retardant paint Download PDFInfo
- Publication number
- CN106147551A CN106147551A CN201510160994.8A CN201510160994A CN106147551A CN 106147551 A CN106147551 A CN 106147551A CN 201510160994 A CN201510160994 A CN 201510160994A CN 106147551 A CN106147551 A CN 106147551A
- Authority
- CN
- China
- Prior art keywords
- alkyd resin
- preparation
- fireproof coating
- fire
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Paints Or Removers (AREA)
Abstract
The invention discloses the preparation method of a kind of alkyd resin fire-retardant paint, this coating is formulated according to weight proportion by following component: the alkyd resin of 100-130 part halogenation, 8-14 part Lithium metasilicate, 10-15 part antimony oxide, 10-15 part decabromodiphenyl oxide, 5-8 part dehydrant, 4-9 part carbon forming agent, 3-7 part foaming agent, 15-20 part stibium trioxide powder, 10-15 part asbestos fibre, 8-12 part tricresyl phosphate, 15-25 part epoxy resin, 50-70 part water.Beneficial effect: add Decabromodiphenyl Ether so that the fireproof coating of the present invention is efficient；Use filler stibium trioxide powder, both played the effect of pigment, and be improved fire-retardant synergy；Asbestos fibre makes the fireproof coating adhesive force height of the present invention, and intensity is big；Tricresyl phosphate makes the fireproof coating pliability of the present invention strong；Epoxy resin provides the fireproof coating stability of the present invention.
Description
Technical field
The present invention relates to fireproof coating field, particularly relate to the preparation method of a kind of alkyd resin fire-retardant paint.
Background technology
Currently, fireproof coating is widely used, and fireproof coating is applied to flammable substrates surface, and in order to change material surface combustion characteristics, retardance fire spreads rapidly；Or be applied on building element, in order to improve the fire endurance of component.The usage of fireproof coating is to brush on the surface of combustible material, improves the refractory ability of material, slows down propagation of flame spread speed, or can stop burning within a certain period of time.But, general fireproof coating is inefficient, and pliability, adhesive force are the most undesirable, accordingly, it would be desirable to a kind of new technical scheme solves the problems referred to above.
Summary of the invention
The present invention provide a kind of efficiently, the preparation method of the alkyd resin fire-retardant paint of high-flexibility.
The technical solution used in the present invention: a kind of alkyd resin fire-retardant paint is formulated according to weight proportion by following component: the alkyd resin of 100-130 part halogenation, 8-14 part Lithium metasilicate, 10-15 part antimony oxide, 10-15 part decabromodiphenyl oxide, 5-8 part dehydrant, 4-9 part carbon forming agent, 3-7 part foaming agent, 15-20 part stibium trioxide powder, 10-15 part asbestos fibre, 8-12 part tricresyl phosphate, 15-25 part epoxy resin, 50-70 part water.
Dehydrant is one or both of three (2 one chloropropyl) phosphate esters and APP.
Carbon forming agent is one or the mixture of tetramethylolmethane, dipentaerythritol or tripentaerythritol.
Foaming agent is one or both of tripolycyanamide or dicyandiamide.
The preparation method of a kind of alkyd resin fire-retardant paint, it is characterised in that preparation process is:
A, dehydrant, carbon forming agent and foaming agent are placed in mortar grinding in described ratio, powdered after be transferred in beaker, and add antimony oxide, decabromodiphenyl oxide and stibium trioxide powder, be stirred mix homogeneously；
B, in beaker, add the alkyd resin of the halogenation of described ratio, Lithium metasilicate, asbestos fibre, tricresyl phosphate and epoxy resin, and be stirred uniformly in being placed on magnetic stirrer；
C, the material in beaker is poured in disperse mill, and the water pouring described ratio into carries out high speed dispersion 1-3h, obtains alkyd resin fire proofing material.
Beneficial effects of the present invention: add Decabromodiphenyl Ether so that the fireproof coating of the present invention is efficient；Use filler stibium trioxide powder, both played the effect of pigment, and be improved fire-retardant synergy；Asbestos fibre makes the fireproof coating adhesive force height of the present invention, and intensity is big；Tricresyl phosphate makes the fireproof coating pliability of the present invention strong；Epoxy resin provides the fireproof coating stability of the present invention.
Specific embodiments
Embodiment 1
5 parts of APPs, 4 parts of tetramethylolmethanes and 3 parts of tripolycyanamide are placed in mortar grinding, powdered after be transferred in beaker, and add 10 parts of antimony oxides, 10 parts of decabromodiphenyl oxides and 15 parts of stibium trioxide powder, be stirred mix homogeneously；In beaker, add the alkyd resin of 100 parts of halogenations, 8 parts of Lithium metasilicates, 10 parts of asbestos fibres, 8 parts of tricresyl phosphates and 15 parts of epoxy resin, and be stirred uniformly in being placed on magnetic stirrer；Material in beaker is poured in disperse mill, and pours 50 parts of water into and carry out high speed dispersion 1h, obtain alkyd resin fire proofing material.
Add Decabromodiphenyl Ether so that the fireproof coating of the present invention is efficient；Use filler stibium trioxide powder, both played the effect of pigment, and be improved fire-retardant synergy；Asbestos fibre makes the fireproof coating adhesive force height of the present invention, and intensity is big；Tricresyl phosphate makes the fireproof coating pliability of the present invention strong；Epoxy resin provides the fireproof coating stability of the present invention.
Embodiment 2
6 part of three (2 one chloropropyl) phosphate ester, 7 parts of dipentaerythritols and 5 parts of dicyandiamides are placed in mortar grinding, it is transferred to after powdered in beaker, and add 13 parts of antimony oxides, 13 parts of decabromodiphenyl oxides and 17 parts of stibium trioxide powder, it is stirred mix homogeneously；In beaker, add the alkyd resin of 120 parts of halogenations, 11 parts of Lithium metasilicates, 13 parts of asbestos fibres, 10 parts of tricresyl phosphates and 20 parts of epoxy resin, and be stirred uniformly in being placed on magnetic stirrer；Material in beaker is poured in disperse mill, and pours 60 parts of water into and carry out high speed dispersion 2h, obtain alkyd resin fire proofing material.
Add Decabromodiphenyl Ether so that the fireproof coating of the present invention is efficient；Use filler stibium trioxide powder, both played the effect of pigment, and be improved fire-retardant synergy；Asbestos fibre makes the fireproof coating adhesive force height of the present invention, and intensity is big；Tricresyl phosphate makes the fireproof coating pliability of the present invention strong；Epoxy resin provides the fireproof coating stability of the present invention.
Embodiment 3
By 8 part of three (2 one chloropropyl) phosphate ester and the mixture of APP, 9 parts of tetramethylolmethanes, dipentaerythritol and the mixture of tripentaerythritol, 7 parts of dicyandiamides and mixture of tripolycyanamide be placed in mortar grinding, it is transferred to after powdered in beaker, and add 15 parts of antimony oxides, 15 parts of decabromodiphenyl oxides and 20 parts of stibium trioxide powder, it is stirred mix homogeneously；In beaker, add the alkyd resin of 130 parts of halogenations, 14 parts of Lithium metasilicates, 15 parts of asbestos fibres, 12 parts of tricresyl phosphates and 25 parts of epoxy resin, and be stirred uniformly in being placed on magnetic stirrer；Material in beaker is poured in disperse mill, and pours 70 parts of water into and carry out high speed dispersion 3h, obtain alkyd resin fire proofing material.
Add Decabromodiphenyl Ether so that the fireproof coating of the present invention is efficient；Use filler stibium trioxide powder, both played the effect of pigment, and be improved fire-retardant synergy；Asbestos fibre makes the fireproof coating adhesive force height of the present invention, and intensity is big；Tricresyl phosphate makes the fireproof coating pliability of the present invention strong；Epoxy resin provides the fireproof coating stability of the present invention.
Claims (5)
1. the preparation method of an alkyd resin fire-retardant paint, it is characterised in that this fireproof coating is formulated according to weight proportion by following component: the alkyd resin of 100-130 part halogenation, 8-14 part Lithium metasilicate, 10-15 part antimony oxide, 10-15 part decabromodiphenyl oxide, 5-8 part dehydrant, 4-9 part carbon forming agent, 3-7 part foaming agent, 15-20 part stibium trioxide powder, 10-15 part asbestos fibre, 8-12 part tricresyl phosphate, 15-25 part epoxy resin, 50-70 part water.
The preparation method of a kind of alkyd resin fire-retardant paint the most according to claim 1, it is characterised in that: described dehydrant is one or both of three (2 one chloropropyl) phosphate esters and APP.
The preparation method of a kind of alkyd resin fire-retardant paint the most according to claim 1, it is characterised in that；Described carbon forming agent is one or the mixture of tetramethylolmethane, dipentaerythritol or tripentaerythritol.
The preparation method of a kind of alkyd resin fire-retardant paint the most according to claim 1, it is characterised in that: described foaming agent is one or both of tripolycyanamide or dicyandiamide.
The preparation method of a kind of alkyd resin fire-retardant paint the most according to claim 1, it is characterised in that preparation process is:
A, dehydrant, carbon forming agent and foaming agent are placed in mortar grinding in described ratio, powdered after be transferred in beaker, and add antimony oxide, decabromodiphenyl oxide and stibium trioxide powder, be stirred mix homogeneously；
B, in beaker, add the alkyd resin of the halogenation of described ratio, Lithium metasilicate, asbestos fibre, tricresyl phosphate and epoxy resin, and be stirred uniformly in being placed on magnetic stirrer；
C, the material in beaker is poured in disperse mill, and the water pouring described ratio into carries out high speed dispersion 1-3h, obtains alkyd resin fire proofing material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510160994.8A CN106147551A (en) | 2015-04-08 | 2015-04-08 | A kind of preparation method of alkyd resin fire-retardant paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510160994.8A CN106147551A (en) | 2015-04-08 | 2015-04-08 | A kind of preparation method of alkyd resin fire-retardant paint |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106147551A true CN106147551A (en) | 2016-11-23 |
Family
ID=57338773
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510160994.8A Pending CN106147551A (en) | 2015-04-08 | 2015-04-08 | A kind of preparation method of alkyd resin fire-retardant paint |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106147551A (en) |
-
2015
- 2015-04-08 CN CN201510160994.8A patent/CN106147551A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101302396B (en) | High temperature-resistant flame-retardant insulating paint and preparation thereof | |
| CN103555165A (en) | Alkyd resin fireproof coating as well as preparation method thereof | |
| CN103102134A (en) | Fireproof and flame retardant mineral compound filling material and cable containing the same | |
| CN101857760A (en) | Aqueous ultra-thin expansion type steel structure fire-proof anti-corrosive paint and preparation method thereof | |
| CN104449135B (en) | Preparation method of reflective insulation type really stone paint | |
| JP4344399B1 (en) | Curable inorganic composition | |
| CN105777150A (en) | Improved isolation layer fireproof material for fireproof wires and cables and manufacturing method thereof | |
| CN106699225A (en) | Flame-retardant heat-retaining board and production method thereof | |
| CN109266159A (en) | A kind of aqueous brake disc coating of high anti-corrosion high heat resistance and its preparation process | |
| JPWO2006104290A1 (en) | Water-based paint composition and heat shielding paint | |
| CN106147551A (en) | A kind of preparation method of alkyd resin fire-retardant paint | |
| CN106281035A (en) | A kind of fire-resistant coating for steel structure and preparation method thereof | |
| CN105062288A (en) | Fireproof corrosion resistant coating | |
| CN102849947B (en) | Foaming agent for preparation of hollow glass beads and application of foaming agent | |
| CN104650676A (en) | High-efficient aqueous expansion fireproof coating and preparation method thereof | |
| CN105062289A (en) | Preparation method of fireproof corrosion resistant coating | |
| CN108948807A (en) | Environment-friendly novel heat resistant fire-proof agent | |
| CN106699101B (en) | A kind of preparation method for the inorfil fireproof and heat-insulating material that foams | |
| CN107286768A (en) | A kind of nano ceramic high-temperature-resistant thermal-insulation coating and preparation method thereof | |
| CN103087525A (en) | Preparation method of polysulfone composite flame-retardant material | |
| CN105733406A (en) | Fireproof heat-insulation paint | |
| CN102910865B (en) | Special bonding agent for anti-radiation fireproofing organic insulation board | |
| CN106588114A (en) | Processing method of concrete for anti-scaling wall | |
| CN105969163A (en) | Efficient fireproof coating for steel structure | |
| CN103087439A (en) | Preparation method of polyvinyl chloride composite flame-retardant material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161123 |