CN106147502A - A kind of cabin epoxy zinc rich primer preparation technology - Google Patents

A kind of cabin epoxy zinc rich primer preparation technology Download PDF

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Publication number
CN106147502A
CN106147502A CN201610543380.2A CN201610543380A CN106147502A CN 106147502 A CN106147502 A CN 106147502A CN 201610543380 A CN201610543380 A CN 201610543380A CN 106147502 A CN106147502 A CN 106147502A
Authority
CN
China
Prior art keywords
parts
cabin
zinc
preparation technology
manganese naphthenate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201610543380.2A
Other languages
Chinese (zh)
Inventor
祝秀凤
汪鹏程
孙巨福
戴宇钧
祝盆鑫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANCHANG YINHU PAINT Co Ltd
Original Assignee
TIANCHANG YINHU PAINT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TIANCHANG YINHU PAINT Co Ltd filed Critical TIANCHANG YINHU PAINT Co Ltd
Priority to CN201610543380.2A priority Critical patent/CN106147502A/en
Publication of CN106147502A publication Critical patent/CN106147502A/en
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
    • C09D161/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C09D161/26—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds
    • C09D161/28—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with heterocyclic compounds with melamine
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08—Anti-corrosive paints
    • C09D5/10—Anti-corrosive paints containing metal dust
    • C09D5/106—Anti-corrosive paints containing metal dust containing Zn
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Plant Pathology (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The invention discloses cabin epoxy zinc rich primer preparation technology, by weight, it is made up of following raw material: melamine resin 28 30 parts, hydroxyacetic acid 35 parts, titanium dioxide 3.2 4 parts, zinc yellow 2.5 5.5 parts, chlorinated paraffin 2.5 4.5 parts, 47 parts of butanol, manganese naphthenate 12 parts, zinc metal powder 2.5 3.5 parts, basic unit's penetrating agent 0.2 0.5 parts, 40 44 parts of water；With the addition of basic unit's penetrating agent in raw material of the present invention, the penetrating power of paint strengthens, and manganese naphthenate, tripentaerythritol have good anti-corrosive antibacterial performance, and technique is simply efficient, and the prices of raw materials are low, Harmful chemicals consumption is few.

Description

A kind of cabin epoxy zinc rich primer preparation technology
Technical field
The present invention relates to anticorrosive paint field, particularly belong to a kind of cabin epoxy zinc rich primer preparation technology.
Background technology
The corrosive environment of ocean is complicated, and marine atmosphere zone (the most not contacting the part of sea water), ocean can be divided into splash District (position that the splashing of sea water can be sprayed onto), Tidal zone, ocean (can be by the position of seawater immersion during high tide), sea Ocean submerged zone (throughout the year by the region of sea water immersion) and earth district, seabed (part below water immersion district)；Corrosion type divides again For homogeneous corrosion, spot corrosion, crevice corrosion, turbulent flow corrosion, cavitation damage, galvanic corrosion and corrosion fatigue etc..Boats and ships, especially sea Ocean boats and ships, the environment faced is sufficiently complex, the ocean submerged zone of hull bottom, is immersed in all the year round in the environment of high salt concentration, to anti- The requirement of rotten coating is the highest.
Summary of the invention
It is an object of the invention to provide a kind of cabin epoxy zinc rich primer preparation technology, raw material with the addition of basic unit's infiltration Agent, the penetrating power of paint strengthens, and manganese naphthenate, tripentaerythritol have good anti-corrosive antibacterial performance, and technique is simply efficient, The prices of raw materials are low, Harmful chemicals consumption is few.
The technical solution used in the present invention is as follows:
A kind of cabin epoxy zinc rich primer preparation technology, includes following processing step:
1), by weight, it is made up of following raw material: melamine resin 28-30 part, hydroxyacetic acid 3-5 part, titanium dioxide 3.2- 4 parts, zinc yellow 2.5-5.5 part, chlorinated paraffin 2.5-4.5 part, butanol 4-7 part, manganese naphthenate 1-2 part, zinc metal powder 2.5-3.5 Part, basic unit's penetrating agent 0.2-0.5 part, water 40-44 part；
2), titanium dioxide, zinc metal powder, manganese naphthenate are pulverized through Ultrafine Grinding, after mixing, add with magnetic force at 40-50 DEG C Thermal agitation device moderate-speed mixer 1-1.5h, then uses centrifuge to be each centrifuged by mixture under the rotating speed of 2500-2700r/min 30-40min, centrifugal after supernatant pour room temperature in beaker into and place, precipitate is dried in the air dry oven of 90-100 DEG C, Standby；
3), by step 2) product that obtains mixes with remaining component, stirs and be heated to 80-100 DEG C, and 1-1.5 is little in insulation Time, it is cooled to 30-32 DEG C, is incubated 1.5-2 hour, is again heated to 130-140 DEG C, be incubated 1-2 hour, cold with 10-15 DEG C/min But to room temperature, finished product paint is i.e. prepared.
Step 2) in, titanium dioxide, zinc metal powder, manganese naphthenate are pulverized through Ultrafine Grinding, after mixing, uses at 45 DEG C Magnetic force heating stirrer moderate-speed mixer 1.2h, then uses centrifuge to be each centrifuged by mixture under the rotating speed of 2600r/min 35min, centrifugal after supernatant pour room temperature in beaker into and place, precipitate is dried in the air dry oven of 95 DEG C, standby.
Raw material of the present invention, with melamine resin, hydroxyacetic acid as major ingredient, with the addition of zinc yellow simultaneously, and the penetrating power of paint increases By force, manganese naphthenate, zinc metal powder have good anti-corrosive antibacterial performance, and technique is simply efficient, and the prices of raw materials are low, harmful chemicals Product consumption is few, meets the use requirement of cabin.
Detailed description of the invention
Embodiment 1
A kind of cabin epoxy zinc rich primer preparation technology, includes following processing step:
1), by weight, it is made up of following raw material: melamine resin 29 parts, hydroxyacetic acid 4 parts, titanium dioxide 3.6 parts, zinc Chrome yellow 4 parts, chlorinated paraffin 3.5 parts, 5.5 parts of butanol, manganese naphthenate 1.5 parts, zinc metal powder 3 parts, basic unit's penetrating agent 0.35 part, water 42 parts；
2), titanium dioxide, zinc metal powder, manganese naphthenate are pulverized through Ultrafine Grinding, after mixing, stir with magnetic force heating at 45 DEG C Mix device moderate-speed mixer 1.2h, then use centrifuge that mixture is each centrifuged under the rotating speed of 2600r/min 35min, centrifugal After supernatant pour in beaker room temperature into and place, precipitate is dried in the air dry oven of 95 DEG C, standby；
3), by step 2) product that obtains mixes with remaining component, stirs and be heated to 90 DEG C, be incubated 1.2 hours, cooling To 31 DEG C, it is incubated 1.8 hours, is again heated to 135 DEG C, be incubated 1.5 hours, be cooled to room temperature with 12 DEG C/min, i.e. prepare finished product Paint.
Paint prepared by the present invention is coated with in being placed in cabin possesses following performance:
Adhesive force 4.20N/mm2
Bin stability, 28 days/40 DEG C excellent
Wet rubbing is washed, 28 days > 10430 times
Film thickness, 0-2000 μm does not ftractures.

Claims (2)

1. a cabin epoxy zinc rich primer preparation technology, it is characterised in that include following processing step:
1), by weight, it is made up of following raw material: melamine resin 28-30 part, hydroxyacetic acid 3-5 part, titanium dioxide 3.2- 4 parts, zinc yellow 2.5-5.5 part, chlorinated paraffin 2.5-4.5 part, butanol 4-7 part, manganese naphthenate 1-2 part, zinc metal powder 2.5- 3.5 parts, basic unit's penetrating agent 0.2-0.5 part, water 40-44 part；
2), titanium dioxide, zinc metal powder, manganese naphthenate are pulverized through Ultrafine Grinding, after mixing, add with magnetic force at 40-50 DEG C Thermal agitation device moderate-speed mixer 1-1.5h, then uses centrifuge to be each centrifuged by mixture under the rotating speed of 2500-2700r/min 30-40min, centrifugal after supernatant pour room temperature in beaker into and place, precipitate is dried in the air dry oven of 90-100 DEG C, Standby；
3), by step 2) product that obtains mixes with remaining component, stirs and be heated to 80-100 DEG C, and 1-1.5 is little in insulation Time, it is cooled to 30-32 DEG C, is incubated 1.5-2 hour, is again heated to 130-140 DEG C, be incubated 1-2 hour, cold with 10-15 DEG C/min But to room temperature, finished product paint is i.e. prepared.
Cabin epoxy zinc rich primer preparation technology the most according to claim 1, it is characterised in that step 2) in, by dioxy Change titanium, zinc metal powder, manganese naphthenate are pulverized through Ultrafine Grinding, after mixing, with magnetic force heating stirrer moderate-speed mixer at 45 DEG C 1.2h, then uses centrifuge that mixture is each centrifuged under the rotating speed of 2600r/min 35min, and the supernatant after being centrifuged falls Entering room temperature in beaker to place, precipitate is dried in the air dry oven of 95 DEG C, standby.
CN201610543380.2A 2016-07-12 2016-07-12 A kind of cabin epoxy zinc rich primer preparation technology Withdrawn CN106147502A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610543380.2A CN106147502A (en) 2016-07-12 2016-07-12 A kind of cabin epoxy zinc rich primer preparation technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610543380.2A CN106147502A (en) 2016-07-12 2016-07-12 A kind of cabin epoxy zinc rich primer preparation technology

Publications (1)

Publication Number Publication Date
CN106147502A true CN106147502A (en) 2016-11-23

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Family Applications (1)

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CN201610543380.2A Withdrawn CN106147502A (en) 2016-07-12 2016-07-12 A kind of cabin epoxy zinc rich primer preparation technology

Country Status (1)

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CN (1) CN106147502A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1343749A (en) * 2001-10-17 2002-04-10 中国人民解放军海军舰船维修研究所 Priming paint for wet and rusted surface
CN103589271A (en) * 2013-10-18 2014-02-19 青岛昊源环境工程技术有限公司 Special antirust paint for ship
CN103980801A (en) * 2014-06-05 2014-08-13 唐山尼克涂料有限公司 Zinc-rich primer and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1343749A (en) * 2001-10-17 2002-04-10 中国人民解放军海军舰船维修研究所 Priming paint for wet and rusted surface
CN103589271A (en) * 2013-10-18 2014-02-19 青岛昊源环境工程技术有限公司 Special antirust paint for ship
CN103980801A (en) * 2014-06-05 2014-08-13 唐山尼克涂料有限公司 Zinc-rich primer and preparation method thereof

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Application publication date: 20161123