CN106140588B - A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell - Google Patents
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell Download PDFInfo
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- CN106140588B CN106140588B CN201610490934.7A CN201610490934A CN106140588B CN 106140588 B CN106140588 B CN 106140588B CN 201610490934 A CN201610490934 A CN 201610490934A CN 106140588 B CN106140588 B CN 106140588B
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- 238000000576 coating method Methods 0.000 title claims abstract description 57
- 238000004140 cleaning Methods 0.000 title claims abstract description 21
- 239000002002 slurry Substances 0.000 claims abstract description 106
- 239000011521 glass Substances 0.000 claims abstract description 78
- 239000000843 powder Substances 0.000 claims abstract description 66
- 238000010410 dusting Methods 0.000 claims abstract description 56
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 48
- 239000011347 resin Substances 0.000 claims abstract description 31
- 229920005989 resin Polymers 0.000 claims abstract description 31
- 239000003292 glue Substances 0.000 claims abstract description 29
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 25
- 239000011265 semifinished product Substances 0.000 claims abstract description 24
- 239000002994 raw material Substances 0.000 claims abstract description 23
- 238000002834 transmittance Methods 0.000 claims abstract description 20
- 239000002270 dispersing agent Substances 0.000 claims abstract description 19
- 239000000243 solution Substances 0.000 claims abstract description 19
- 238000010790 dilution Methods 0.000 claims abstract description 18
- 239000012895 dilution Substances 0.000 claims abstract description 18
- 239000002518 antifoaming agent Substances 0.000 claims abstract description 12
- 230000005484 gravity Effects 0.000 claims abstract description 8
- 238000007689 inspection Methods 0.000 claims abstract description 8
- 239000000047 product Substances 0.000 claims abstract description 8
- 238000005303 weighing Methods 0.000 claims abstract description 8
- 238000002156 mixing Methods 0.000 claims abstract description 4
- 239000011248 coating agent Substances 0.000 claims description 33
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 21
- 238000007664 blowing Methods 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 14
- 239000007787 solid Substances 0.000 claims description 11
- 238000001035 drying Methods 0.000 claims description 10
- 239000004744 fabric Substances 0.000 claims description 10
- 230000006837 decompression Effects 0.000 claims description 8
- 239000011440 grout Substances 0.000 claims description 8
- 239000007859 condensation product Substances 0.000 claims description 7
- 238000005259 measurement Methods 0.000 claims description 7
- 159000000000 sodium salts Chemical class 0.000 claims description 7
- 238000004018 waxing Methods 0.000 claims description 7
- 239000004925 Acrylic resin Substances 0.000 claims description 6
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 claims description 6
- 229920000178 Acrylic resin Polymers 0.000 claims description 5
- 238000006277 sulfonation reaction Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims 1
- 229910002114 biscuit porcelain Inorganic materials 0.000 abstract description 12
- 238000000034 method Methods 0.000 abstract description 9
- 230000008569 process Effects 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 4
- 230000021615 conjugation Effects 0.000 abstract description 3
- 238000001914 filtration Methods 0.000 abstract 1
- 239000001993 wax Substances 0.000 abstract 1
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 12
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 239000003085 diluting agent Substances 0.000 description 5
- 229930185605 Bisphenol Natural products 0.000 description 4
- 239000003822 epoxy resin Substances 0.000 description 4
- 229920000647 polyepoxide Polymers 0.000 description 4
- 239000001294 propane Substances 0.000 description 4
- RDOXTESZEPMUJZ-UHFFFAOYSA-N anisole Chemical class COC1=CC=CC=C1 RDOXTESZEPMUJZ-UHFFFAOYSA-N 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 2
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000003780 insertion Methods 0.000 description 2
- 230000037431 insertion Effects 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 125000003700 epoxy group Chemical group 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- UZKWTJUDCOPSNM-UHFFFAOYSA-N methoxybenzene Substances CCCCOC=C UZKWTJUDCOPSNM-UHFFFAOYSA-N 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000009955 starching Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
- B05D7/22—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to internal surfaces, e.g. of tubes
- B05D7/222—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to internal surfaces, e.g. of tubes of pipes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/02—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by baking
- B05D3/0254—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Formation Of Various Coating Films On Cathode Ray Tubes And Lamps (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The present invention relates to tube cell preparation technical fields, disclose a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising: a, match powder: weighing resin glue dilution, levelling agent, dispersant solution, hydrophilic agent, defoaming agent, water, water intaking dissolubility spread powder；After each raw material is mixed, slurry is obtained by filtration, adjusts slurry specific gravity and viscosity, after mixing evenly stand for standby use；B, it dusting: waxes to the both ends internal wall of pipe orifice of T8 straight tube glass tube, then carries out dusting；Semi-finished product are made after dusting；C, it examines: light transmittance inspection is carried out to each position of semi-finished product；D, it toasts: choosing and examine qualified semi-finished product, finished product after baking.Powder-coating method simple process of the invention, without being cleaned to tube cell after dusting；And tube cell obtained, powder layer thickness homogeneity is good, and each position light transmittance is essentially identical；The conjugation of bisque and glass tube is good simultaneously, not easily to fall off.
Description
Technical field
The present invention relates to tube cell preparation technical field more particularly to a kind of powder-coating methods free of cleaning of T8 straight tube LED tube cell.
Background technique
The tube cell of LED light during the preparation process, needs to carry out dusting to the inner wall of glass tube, the quality of dusting directly affects
To the translucent effect of fluorescent tube.Slurry is usually poured into pump from the upper end of glass tube, makes slurry by weight by current coating process
Power leaves, and flows out from the lower end of glass tube, and after then toasting, one layer of bisque is thus formed on glass inside pipe wall.
Such as application No. is 200910182998.0 Chinese patents to disclose a kind of powder coating method of fluorescent lamp tube, including following
Step: (1) washed bright pipe is put into starching machine on, is blown into hot wind and dries bright pipe；(2) when bright pipe advances to upper powder position
When, by one end nozzle of spraying pump pipette tips insertion fluorescent tube, starting pump carries out the slurry that dusts, and when slurry is sprayed at the top of fluorescent tube, stops
Dust slurry, and removes lance head；(3) by the other end nozzle of the pipette tips insertion fluorescent tube of air draught pump, starting air draught pumps air draught, works as powder
When slurry is flowed at nozzle, then stop air draught, and remove air draught pipette tips；(4) tube cell enters drying area drying.
Since the both ends of fluorescent tube are needed when in use for assembling, it cannot be coated with slurry at the both ends nozzle of fluorescent tube,
Bright pipe needs to carry out later period cleaning to the both ends bisque of bright pipe after the dusting by above-mentioned technical proposal.This method and process
Complexity, it is not convenient enough, reduce working efficiency.
In addition, after the dusting of above-mentioned technical proposal, the powder layer thickness that slurry is formed after solidifying in glass inside pipe wall is not equal enough
One, cause the light transmittance at each position of tube cell different, causes of low quality.
Summary of the invention
In order to solve the above-mentioned technical problems, the present invention provides a kind of powder-coating methods free of cleaning of T8 straight tube LED tube cell.This
The powder-coating method simple process of invention, without being cleaned to the bisque of tube cell both ends nozzle after dusting；And T8 straight tube obtained
The caliper uniformity of LED tube cell, bisque is good, and each position light transmittance of tube cell is essentially identical；The conjugation of bisque and glass tube simultaneously
It is good, it is not easily to fall off.
The specific technical proposal of the invention is: a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, including following step
It is rapid:
A, match powder: weighing the raw material of following volumes part respectively: 750-850 parts of resin glue dilutions, 1-2 parts of levelling agents,
35-45 parts of dispersant solutions, 35-45 parts of hydrophilic agents, 2-3 parts of defoaming agents, 700-900 parts of water；It weighs and the resin glue aqueous
Gu the water-soluble spread powder than 800mL/1kg；After above-mentioned each raw material is mixed, 250-350 mesh filter cloth is crossed, slurry is obtained, adds water
Slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stands 40- after mixing evenly
60h is spare.
The present invention with slurry, good dispersion, no large particulate matter, during dusting mobility, be solidified into film property
Moderate, thickness is uniform after solidification, and light transmittance is more average.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, is poured into slurry from the upper end of T8 straight tube glass tube, to its inner wall
Carry out dusting；It is blowed during dusting, blowing temperature is 20-75 DEG C；Semi-finished product are made after dusting.
Since wax has hydrophobicity, after wax layer is attached to glass tube both ends internal wall of pipe orifice, slurry will not be to painting when dusting
Wax position carries out dusting, so that not having bisque at the nozzle of glass tube both ends.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 3-5min, finished product at 150-300 DEG C.It is drying
During roasting, glass tube is not direct directly to be contacted with calandria.Under decompression baking, wax layer is waved since temperature raises and rapidly
Hair, so that keeping original appearance at the nozzle of glass tube both ends.The technique is easy to operate without cleaning, and is conducive to improve production efficiency.
Preferably, in step a each raw material order of addition are as follows: dispersant solution is added in water；Then water is added
Dissolubility spread powder stirs 40-80min；Continue to add resin glue dilution, stirs 20-40min；Then surplus stock is added,
Stir 10-14h.
Preferably, the resin glue dilution diluted in equal volume by S-3501 type water-based acrylic resin and water and
At；The levelling agent is levelling agent 420；The dispersant solution is the FD-40 dispersant solution of 8-12wt%；The water solubility
The model S-833 of spread powder；The hydrophilic agent is the N-80 hydrophilic agent of 10wt%；The defoaming agent is P-76 defoaming agent.
Preferably, further including naphthalene of the relative molecular mass in 3000-5000 of 4-8 parts by volume in the raw material of the slurry
Sulfonic acid and formaldehyde condensation product sodium salt, and sulfonation degree is 80% or more.Naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt, energy are added in slurry
The dispersibility for enough further increasing slurry keeps the stability of slurry higher, avoids that accumulation sedimentation occurs after preparing in slurry.
In addition, naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt can also avoid bubble during the dusting of slurry.
Preferably, further including the focus ratio of 8-12 parts by volume in the raw material of the slurry；The focus ratio
Relative molecular mass in 8-12 ten thousand, solid content 40-50wt%.Focus ratio is thermosetting resin, can improve slurry with
The adhesion of glass inside pipe wall, it is not easily to fall off after solidifying slurry；And focus ratio heat-resisting quantity is preferable, can prevent solid
The bisque of change is heated under long-time illumination and is fallen off.Focus ratio can be commercially available, can also make by oneself.
Preferably, T8 straight tube glass tube does the circular motion of individual pen, powder coating machine on powder coating machine in step b dusting
On by T8 straight tube glass tube motion profile be divided into the area 1-5, wherein 1st area blowing rate is 1-3m/s, dry 45-65 DEG C of temperature；2nd area
Blowing rate is 1-3m/s, is dried 52-72 DEG C of temperature；Rate is dried as 3-5m/s by 3rd area, dries 22-42 DEG C of temperature；The blowing of 4th area
Rate is 4-6m/s, is dried 21-41 DEG C of temperature；Rate is dried as 4-6m/s by 5th area, dries 35-55 DEG C of temperature.Powder coating machine is carried out
The blowing rate and blowing temperature of each region is set separately according to slurry in the curing degree of glass inside pipe wall in region division
Degree, it can be ensured that thickness of the slurry at each position of glass inside pipe wall is essentially identical.
Preferably, revolving speed of the T8 straight tube glass tube on powder coating machine is 1300-1340 branch/h.
Preferably, slurry is to recycle during dusting, slurry is collected after the outflow of T8 straight tube glass tube
It re-enters in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 150-250 mesh.Slurry is recycled
It utilizes, save the cost.Filter cloth is arranged in feed inlet and grout outlet to slurry bucket, can filter out mixed glass during dusting
The impurity such as pipe slag.
Preferably, the slurry in the slurry bucket is in vacuum environment during dusting.Since slurry is circulation benefit
, it is easy to be mixed into air in cyclic process, to generate bubble, is conducive to the row of the air in slurry under vacuum environment
Out.
It is compared with the prior art, the beneficial effects of the present invention are: powder-coating method simple process of the invention, is not necessarily to after dusting
The bisque of tube cell both ends nozzle is cleaned；And T8 straight tube LED tube cell obtained, the caliper uniformity of bisque is good, and tube cell is each
Position light transmittance is essentially identical；The conjugation of bisque and glass tube is good simultaneously, not easily to fall off.
Specific embodiment
The present invention will be further described with reference to the examples below.
Embodiment 1
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising the following steps:
A, match powder: weighing following raw material: 800mL resin glue dilution, 1.5mL levelling agent 420,40mL 10wt% respectively
FD-40 dispersant solution, 40mL 10wt% N-80 hydrophilic agent, 2.5mL P-76 defoaming agent, 800mL water；Weigh with it is described
The S-833 water solubility spread powder of resin glue liquid-solid ratio 800mL/1kg.The resin glue dilution is by S-3501 type aqueous third
Olefin(e) acid resin dilutes in equal volume with water.
Dispersant solution is added in water；Then water-soluble spread powder is added, 60min is stirred；Continue to add resin glue
Water diluent stirs 30min；Then surplus stock is added, 12h is stirred.After above-mentioned each raw material is mixed, 300 mesh filter clothes are crossed, are obtained
To slurry, add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stirring is equal
It is spare that 50h is stood after even.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, the slurry in the slurry bucket is under vacuum environment.From T8 straight tube glass
Slurry is poured at the upper end of glass pipe, dusting is carried out to the inner wall of T8 straight tube glass tube；T8 straight tube glass tube is done on powder coating machine
The circular motion of individual pen is blowed during dusting, and semi-finished product are made after dusting.
Wherein, it is divided into the area 1-5 by T8 straight tube glass tube motion profile on powder coating machine, wherein 1st area blowing rate is 2m/s, blows
55 DEG C of air temperature；Rate is dried as 2m/s by 2nd area, dries 62 DEG C of temperature；Rate is dried as 4m/s by 3rd area, dries 32 DEG C of temperature；4th area
Blowing rate is 5m/s, is dried 31 DEG C of temperature；Rate is dried as 5m/s by 5th area, temperature 45 C of drying.T8 straight tube glass tube is in dusting
Revolving speed on machine is 1320/h.
In addition, slurry is to recycle during dusting, slurry is collected again after the outflow of T8 straight tube glass tube
It inputs in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 200 mesh.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 4min, finished product at 250 DEG C.
Embodiment 2
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising the following steps:
A, match powder: weighing following raw material respectively: 750mL resin glue dilution, 1mL levelling agent 420,35mL 12wt%
FD-40 dispersant solution, the N-80 hydrophilic agent of 35mL 10wt%, 2mL P-76 defoaming agent, 700mL water；It weighs and the resin
The S-833 water solubility spread powder of glue liquid-solid ratio 800mL/1kg.The resin glue dilution is by S-3501 type water soluble acrylic acid
Resin dilutes in equal volume with water.
Dispersant solution is added in water；Then water-soluble spread powder is added, 40min is stirred；Continue to add resin glue
Water diluent stirs 20min；Then surplus stock is added, 14h is stirred.After above-mentioned each raw material is mixed, 250 mesh filter clothes are crossed, are obtained
To slurry, add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stirring is equal
It is spare that 40h is stood after even.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, the slurry in the slurry bucket is under vacuum environment.From T8 straight tube glass
Slurry is poured at the upper end of glass pipe, dusting is carried out to the inner wall of T8 straight tube glass tube；T8 straight tube glass tube is done on powder coating machine
The circular motion of individual pen is blowed during dusting, and semi-finished product are made after dusting.
Wherein, it is divided into the area 1-5 by T8 straight tube glass tube motion profile on powder coating machine, wherein 1st area blowing rate is 1m/s, blows
45 DEG C of air temperature；Rate is dried as 1m/s by 2nd area, dries 52 DEG C of temperature；Rate is dried as 3m/s by 3rd area, dries 22 DEG C of temperature；4th area
Blowing rate is 4m/s, is dried 21 DEG C of temperature；Rate is dried as 4m/s by 5th area, dries 35 DEG C of temperature.T8 straight tube glass tube is in dusting
Revolving speed on machine is 1300/h.
In addition, slurry is to recycle during dusting, slurry is collected again after the outflow of T8 straight tube glass tube
It inputs in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 150 mesh.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 5min, finished product at 150 DEG C.
Embodiment 3
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising the following steps:
A, match powder: weighing following raw material respectively: 850mL resin glue dilution, 2mL levelling agent 420,45mL 8wt%
FD-40 dispersant solution, the N-80 hydrophilic agent of 45mL 10wt%, 3mL P-76 defoaming agent, 8mL relative molecular mass exist
3000-5000, sulfonation degree are 40wt%, opposite point in 80% or more naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt, the solid content of 12 mL
Focus ratio, 900mL water of the protonatomic mass in 8-12 ten thousand；Weigh the S-833 water with the resin glue liquid-solid ratio 800mL/1kg
Dissolubility spread powder.The resin glue dilution is diluted by S-3501 type water-based acrylic resin with water in equal volume.
Focus ratio the preparation method comprises the following steps: by quality than bisphenol A type epoxy resin, bis-phenol base under atmosphere of inert gases
Propane, which is added in reaction vessel, to be uniformly mixed, and bisphenol A type epoxy resin and the total matter of bis-phenol base propane are added into reaction vessel
The methyl phenyl ethers anisole of amount 20%, is warming up to material dissolution.Wherein, the epoxy group in bisphenol A type epoxy resin and phenol hydroxyl in bis-phenol base propane
The molar ratio of base is 1.05:1.Urging for bisphenol A type epoxy resin and bis-phenol base propane gross mass 0.15% is added into reaction vessel
Agent, reaction temperature are 160 DEG C, and the reaction time is for 24 hours.When reaction proceeds to 20h, substance gross mass in reaction vessel is added
50% butanone, naturally cools to 70 DEG C after reaction, and obtained focus ratio is filtered after discharging.
Dispersant solution is added in water；Then water-soluble spread powder is added, 80min is stirred；Continue to add resin glue
Water diluent stirs 40min；Then surplus stock is added, 10h is stirred.After above-mentioned each raw material is mixed, 350 mesh filter clothes are crossed, are obtained
To slurry, add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stirring is equal
It is spare that 60h is stood after even.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, the slurry in the slurry bucket is under vacuum environment.From T8 straight tube glass
Slurry is poured at the upper end of glass pipe, dusting is carried out to the inner wall of T8 straight tube glass tube；T8 straight tube glass tube is done on powder coating machine
The circular motion of individual pen is blowed during dusting, and semi-finished product are made after dusting.
Wherein, it is divided into the area 1-5 by T8 straight tube glass tube motion profile on powder coating machine, wherein 1st area blowing rate is 3m/s, blows
65 DEG C of air temperature；Rate is dried as 3m/s by 2nd area, dries 72 DEG C of temperature；Rate is dried as 5m/s by 3rd area, dries 42 DEG C of temperature；4th area
Blowing rate is 6m/s, is dried 41 DEG C of temperature；Rate is dried as 6m/s by 5th area, dries 55 DEG C of temperature.T8 straight tube glass tube is in dusting
Revolving speed on machine is 1340/h.
In addition, slurry is to recycle during dusting, slurry is collected again after the outflow of T8 straight tube glass tube
It inputs in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 250 mesh.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 3min, finished product at 300 DEG C.
Embodiment 4
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising the following steps:
A, match powder: weighing following raw material: 800mL resin glue dilution, 1.5mL levelling agent 420,40mL 9wt% respectively
FD-40 dispersant solution, the N-80 hydrophilic agent of 40mL 10wt%, 2.5mL P-76 defoaming agent, 6mL relative molecular mass exist
3000-5000, sulfonation degree are 45wt%, opposite point in 80% or more naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt, the solid content of 10mL
Focus ratio, 800mL water of the protonatomic mass in 8-12 ten thousand；Weigh the S-833 water with the resin glue liquid-solid ratio 800mL/1kg
Dissolubility spread powder.The resin glue dilution is diluted by S-3501 type water-based acrylic resin with water in equal volume.
Dispersant solution is added in water；Then water-soluble spread powder is added, 50min is stirred；Continue to add resin glue
Water diluent stirs 25min；Then surplus stock is added, 11h is stirred.After above-mentioned each raw material is mixed, 300 mesh filter clothes are crossed, are obtained
To slurry, add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stirring is equal
It is spare that 55h is stood after even.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, the slurry in the slurry bucket is under vacuum environment.From T8 straight tube glass
Slurry is poured at the upper end of glass pipe, dusting is carried out to the inner wall of T8 straight tube glass tube；T8 straight tube glass tube is done on powder coating machine
The circular motion of individual pen is blowed during dusting, and semi-finished product are made after dusting.
Wherein, it is divided into the area 1-5 by T8 straight tube glass tube motion profile on powder coating machine, wherein 1st area blowing rate is 1.5m/s,
Blowing temperature 50 C；Rate is dried as 1.5m/s by 2nd area, temperature 60 C of drying；Rate is dried as 3.5m/s by 3rd area, temperature 30 of drying
℃；Rate is dried as 4.5m/s by 4th area, dries 30 DEG C of temperature；Rate is dried as 4.5m/s by 5th area, dries 40 DEG C of temperature.T8 straight tube glass
Revolving speed of the glass pipe on powder coating machine is 1320/h.
In addition, slurry is to recycle during dusting, slurry is collected again after the outflow of T8 straight tube glass tube
It inputs in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 200 mesh.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 4.5min, finished product at 200 DEG C.
Embodiment 5
A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, comprising the following steps:
A, match powder: weighing following raw material respectively: 750mL resin glue dilution, 2mL levelling agent 420,40mL 11wt%
FD-40 dispersant solution, the N-80 hydrophilic agent of 40mL 10wt%, 2mL P-76 defoaming agent, 4mL relative molecular mass exist
3000-5000, sulfonation degree are 50wt%, average molecular in 80% or more naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt, the solid content of 8mL
Focus ratio, 800mL water of the quality in 8-12 ten thousand；It weighs water-soluble with the S-833 of the resin glue liquid-solid ratio 800mL/1kg
Property spread powder.The resin glue dilution is diluted by S-3501 type water-based acrylic resin with water in equal volume.
Dispersant solution is added in water；Then water-soluble spread powder is added, 65min is stirred；Continue to add resin glue
Water diluent stirs 35min；Then surplus stock is added, 13h is stirred.After above-mentioned each raw material is mixed, 300 mesh filter clothes are crossed, are obtained
To slurry, add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, stirring is equal
It is spare that 55h is stood after even.
B, dusting: then that T8 straight tube glass tube is vertical to waxing at the inner wall of T8 straight tube glass tube both ends nozzle
It is packed into powder coating machine, slurry is loaded into the slurry bucket of powder coating machine, the slurry in the slurry bucket is under vacuum environment.From T8 straight tube glass
Slurry is poured at the upper end of glass pipe, dusting is carried out to the inner wall of T8 straight tube glass tube；T8 straight tube glass tube is done on powder coating machine
The circular motion of individual pen is blowed during dusting, and semi-finished product are made after dusting.
Wherein, it is divided into the area 1-5 by T8 straight tube glass tube motion profile on powder coating machine, wherein 1st area blowing rate is 2.5m/s,
Blowing temperature 60 C；Rate is dried as 2.5m/s by 2nd area, temperature 70 C of drying；Rate is dried as 4.5m/s by 3rd area, temperature 35 of drying
℃；Rate is dried as 5.5m/s by 4th area, dries 40 DEG C of temperature；Rate is dried as 5.5m/s by 5th area, temperature 50 C of drying.T8 straight tube glass
Revolving speed of the glass pipe on powder coating machine is 1340/h.
In addition, slurry is to recycle during dusting, slurry is collected again after the outflow of T8 straight tube glass tube
It inputs in the slurry bucket；The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 200 mesh.
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%.
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 3.5min, finished product at 250 DEG C.
T8 straight tube tube cell produced by the present invention, bisque firmness are not fallen off through 100 DEG C of boiling 6h；100 DEG C of thermostatic roastings are roasting
168h non yellowing.
Raw materials used in the present invention, equipment is unless otherwise noted the common raw material, equipment of this field；In the present invention
Method therefor is unless otherwise noted the conventional method of this field.
The above is only presently preferred embodiments of the present invention, is not intended to limit the invention in any way, it is all according to the present invention
Technical spirit any simple modification, change and equivalent transformation to the above embodiments, still fall within the technology of the present invention side
The protection scope of case.
Claims (8)
1. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell, it is characterised in that the following steps are included:
A, match powder: weighing the raw material of following volumes part: 750-850 parts of resin glue dilutions, 1-2 parts of levelling agents, 35-45 respectively
Part dispersant solution, 35-45 parts of hydrophilic agents, 2-3 parts of defoaming agents, 700-900 parts of water；It weighs and the resin glue dilution liquid
Gu the water-soluble spread powder than 800mL/1kg；After mixing by above-mentioned each raw material, 250-350 mesh filter cloth is crossed, slurry is obtained,
Add water that slurry specific gravity is adjusted to 1.28-1.32g/cm3, it is 15-18 seconds with 4 glasss of viscosimeter measurement viscosity are applied, it is quiet after mixing evenly
It is spare to set 40-60h；
The resin glue dilution is diluted by S-3501 type water-based acrylic resin with water in equal volume；The levelling agent is
Levelling agent 420；The dispersant solution is the FD-40 dispersant solution of 8-12wt%；The model S- of the water solubility spread powder
833；The hydrophilic agent is the N-80 hydrophilic agent of 10wt%；The defoaming agent is P-76 defoaming agent；
B, dusting: to waxing at the inner wall of T8 straight tube glass tube both ends nozzle, then T8 straight tube glass tube is vertically loaded into
Slurry is loaded into the slurry bucket of powder coating machine, pours into slurry from the upper end of T8 straight tube glass tube by powder coating machine, carries out to its inner wall
Dusting；It is blowed during dusting, blowing temperature is 20-75 DEG C；Semi-finished product are made after dusting；
C, it examines: light transmittance inspection being carried out to each position of semi-finished product, it is desirable that light transmittance is controlled in 91-93%；
D, it toasts: choosing and examine qualified semi-finished product, decompression baking 3-5min, finished product at 150-300 DEG C.
2. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as described in claim 1, which is characterized in that each in step a
The order of addition of raw material are as follows: dispersant solution is added in water；Then water-soluble spread powder is added, 40-80min is stirred；After
Continuous addition resin glue dilution, stirs 20-40min；Then surplus stock is added, 10-14h is stirred.
3. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as claimed in claim 1 or 2, which is characterized in that the powder
It further include naphthalenesulfonateformaldehyde formaldehyde condensation product sodium salt of the relative molecular mass in 3000-5000 of 4-8 parts by volume in the raw material of slurry, and
Sulfonation degree is 80% or more.
4. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as claimed in claim 1 or 2, which is characterized in that the powder
It further include the focus ratio of 8-12 parts by volume in the raw material of slurry；The relative molecular mass of the focus ratio in 8-12 ten thousand,
Solid content is 40-50wt%.
5. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as described in claim 1, which is characterized in that applied in step b
When powder, T8 straight tube glass tube does the circular motion of individual pen on powder coating machine, divides on powder coating machine by T8 straight tube glass tube motion profile
It dries 45-65 DEG C of temperature for the area 1-5 wherein 1st area blowing rate is 1-3m/s；Rate is dried as 1-3m/s by 2nd area, temperature of drying
52-72℃；Rate is dried as 3-5m/s by 3rd area, dries 22-42 DEG C of temperature；Rate is dried as 4-6m/s by 4th area, and dry temperature 21-41
℃；Rate is dried as 4-6m/s by 5th area, dries 35-55 DEG C of temperature.
6. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as described in claims 1 or 2 or 5, which is characterized in that institute
Stating revolving speed of the T8 straight tube glass tube on powder coating machine is 1300-1340 branch/h.
7. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as described in claims 1 or 2 or 5, which is characterized in that
During dusting, slurry is to recycle, and slurry is re-entered in the slurry bucket after the outflow of T8 straight tube glass tube by collection；
The feed inlet and grout outlet of slurry bucket are equipped with the filter cloth of 150-250 mesh.
8. a kind of powder-coating method free of cleaning of T8 straight tube LED tube cell as described in claims 1 or 2 or 5, which is characterized in that
During dusting, the slurry in the slurry bucket is in vacuum environment.
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| CN201610490934.7A CN106140588B (en) | 2016-06-29 | 2016-06-29 | A kind of powder-coating method free of cleaning of T8 straight tube LED tube cell |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5344667A (en) * | 1993-02-23 | 1994-09-06 | Rockwell International Corporation | Method and apparatus for manufacturing serpentine avionics fluorescent tubes with enhanced uniformity of luminance and chromaticity |
| CN103450758A (en) * | 2013-08-19 | 2013-12-18 | 广东雪莱特光电科技股份有限公司 | Water-based paint and preparation method thereof |
| CN103887127A (en) * | 2014-03-04 | 2014-06-25 | 孙向阳 | Method for waxing and powder coating of lamp tube of fluorescent energy-saving lamp |
-
2016
- 2016-06-29 CN CN201610490934.7A patent/CN106140588B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5344667A (en) * | 1993-02-23 | 1994-09-06 | Rockwell International Corporation | Method and apparatus for manufacturing serpentine avionics fluorescent tubes with enhanced uniformity of luminance and chromaticity |
| CN103450758A (en) * | 2013-08-19 | 2013-12-18 | 广东雪莱特光电科技股份有限公司 | Water-based paint and preparation method thereof |
| CN103887127A (en) * | 2014-03-04 | 2014-06-25 | 孙向阳 | Method for waxing and powder coating of lamp tube of fluorescent energy-saving lamp |
Non-Patent Citations (1)
| Title |
|---|
| 水性LED光扩散涂料应用工艺研究;苏荣欢等;《中国照明电器》;20151228(第11期);第33页左栏第4行至第35页右栏倒数第3行，图1-2，表1,3-5 |
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