CN106140027B - A kind of reaction kettle quantitative liquid feeding device and its application method - Google Patents

A kind of reaction kettle quantitative liquid feeding device and its application method Download PDF

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Publication number
CN106140027B
CN106140027B CN201610690065.2A CN201610690065A CN106140027B CN 106140027 B CN106140027 B CN 106140027B CN 201610690065 A CN201610690065 A CN 201610690065A CN 106140027 B CN106140027 B CN 106140027B
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China
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liquid
quantitative
sealing
storage container
reaction kettle
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CN201610690065.2A
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CN106140027A (en
Inventor
余建龙
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Hunan Jinneng Machinery Manufacturing Co., Ltd.
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黄国镇
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/007Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/02Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest

Abstract

The invention discloses a kind of reaction kettle quantitative liquid feeding devices and its application method.Including housing, case top connects liquid injecting pipeline, and quantitative liquor charging component and lifting assembly are set on housing, and quantitative liquor charging component includes flexible liquid storage container and liquid collecting container, it is quantitative to cooperate between liquor charging component and lifting assembly, while device is also connected with a stirring structure.The present invention with other compositions by merging stirring again by the larger liquid component equivalent of accounting being added in reaction kettle in batches, the small amount of liquids ingredient of equivalent is added in while stirring, so as to promote stirring efficiency, ensure that stirring fusion is uniform, increase product qualification rate, while also there is the effect for avoiding waste.

Description

A kind of reaction kettle quantitative liquid feeding device and its application method
Technical field
The present invention relates to perfume production reaction kettle technical field, the quantitative liquid feeding device of especially a kind of reaction kettle and its Application method.
Background technology
Perfume needs to use reaction kettle when preparing, and is stirred by the way that heterogeneity is added in reaction kettle according to a certain percentage It is obtained after mixing, and this ratio is fixed with a perfume.
At present frequently with agitating mode, be directly to be stirred by the way that various deployed ingredients are implanted sequentially in reaction kettle It mixes, this agitating mode is although easy to operate, but stirring efficiency is relatively low, such as a kind of larger liquid component of accounting is direct When all in the liquid in injection reaction kettles, generally requiring the stirring long period can merge the two completely uniformly, and stir The uneven overall effect that can directly influence perfume is mixed, generates substandard product.
Invention content
The present invention provides a kind of reaction kettle with quantitative liquid feeding device and its user for deficiency of the prior art Method, by the way that the larger liquid component equivalent of accounting being added in reaction kettle in batches is merged stirring with other compositions again, The small amount of liquids ingredient of equivalent is added in while stirring, so as to promote stirring efficiency, is ensured that stirring fusion is uniform, is increased product Qualification rate, while also there is the effect for avoiding waste.
In order to solve the above technical problems, the present invention is addressed by following technical proposals:A kind of reaction kettle is with quantitatively sending Liquid device offers the housing of cavity including inside, and the case top is connected with liquid injecting pipeline, and it is fixed to be provided on the housing Liquor charging component and the lifting assembly with the quantitative liquor charging component cooperation are measured, the quantitative liquor charging component includes being arranged on described Flexible liquid storage container in housing and several collection for being arranged on the housing exterior walls and being connected with the flexible liquid storage container Liquid container, the flexibility liquid storage container are located at immediately below the liquid injecting pipeline, and the liquid collecting container bottom offers liquid outlet, institute It states lifting assembly and includes the connecting pole being slidably connected in the inner walls, the connection being arranged on the connecting pole top surface Several cylinders that bar, the seal assembly for being arranged on the connection boom end and the control connecting pole rise or fall, it is described The jacking block with the flexible liquid storage container cooperation is provided in connecting rod, groove body, the sealing group are offered in the connecting rod Part is arranged on the groove body inner wall, the seal assembly include engaged successively from outside toward inside No.1 rack, gear with And sealing plug assembly, the No.1 rack are slidably connected on the groove body inner wall, and the No.1 rack lower end is set There is link block, No.1 spring is provided between the link block and the connecting rod bottom surface, the gear is rotatably connected on described On groove body inner wall, the sealing plug assembly includes No. two racks being slidably connected on the groove body inner wall and is arranged on described Sealing-plug at the top of No. two racks, while the mandril group coordinated with the No.1 rack is provided on the liquid collecting container outer wall Part, the push rod component include the fixed block being fixed on the liquid collecting container outer wall, are opened on the fixed block Through-hole, the mandril being plugged in the through-hole, several grooves being opened on the mandril and it is rotatably connected on the fixation Block bottom surface and with the clamping block of groove cooperation, mandril upper end end set has connection sheet, and the connection sheet and institute It states and No. two springs is provided between fixed block top surface, torsion is provided at the clamping block and the link position of the fixed block bottom surface Spring, when the jacking block is contacted with the rising of the connecting pole with the flexible liquid storage container bottom, the sealing-plug is close The liquid outlet is sealed, cavity is opened up inside the connecting pole and forms cavity body, motor is provided in the cavity body, it is described Motor is connected with the stirring blade being arranged on immediately below the connecting pole.
In above-mentioned technical proposal, it is preferred that the sealing-plug is interference fitted with the liquid outlet.
In above-mentioned technical proposal, it is preferred that be provided with arc-shaped convex block at the top of the sealing-plug.It is come out due to liquid outlet Liquid can be directly flushed at the top of sealing-plug, therefore sets arc-shaped convex block that can ensure sealing-plug top not residual liquid, ensured The consistency of actual ratio and desired proportions promotes product qualification rate.
In above-mentioned technical proposal, it is preferred that the case top is provided with several supporting rods.By set supporting rod by Whole device is fixed in reaction kettle.
In above-mentioned technical proposal, it is preferred that waterproof coating is coated on the seal assembly outer surface.Liquid is avoided close Sealing assembly remains on outer surface, influences overall ratio.
Using a kind of reaction kettle as described above method of quantitative liquid feeding device, its step are as follows:1., pass through liquid injecting pipeline Injection needs liquid to be added in flexible liquid storage container;2., start cylinder and motor, connecting pole and rise after by cylinder action, Stirring blade is persistently mixed movement by motor control;3., with the rising of connecting pole, sealing plug assembly rises therewith, when one After number rack is blocked by mandril, No.1 rack is moved relative to connecting pole, and gear is promoted to rotate, meanwhile, gear drives No. two Rack up moves, and sealing-plug rises therewith;4., when the jacking block in connecting rod is contacted with flexible liquid storage container bottom, sealing Plug seals up liquid outlet;5., jacking block continue to rise the liquid level for promoting liquid in flexible liquid storage container and rise, more than liquid collecting container It is flowed into liquid collecting container with the liquid at the position of flexible liquid storage container connector, cylinder stops operation at this time;6., cylinder stops Only after operation 30 seconds, cylinder starts that connecting pole is driven to move down;7., redundance liquid reflux is held to flexible liquid storage in liquid collecting container In device, liquid level keeps horizontal consistent with above-mentioned connector bottom surface in liquid collecting container, reaches quantitative;8., moving down with connecting pole, Sealing-plug leaves liquid outlet, and the liquid in liquid collecting container is flowed into from liquid outlet in reaction kettle, is mixed with other liquid;9., it is complete Into after 2 minutes of the 8. step, cylinder controls connecting pole to rise again.
The beneficial effects of the invention are as follows:The present invention passes through the larger liquid component equivalent of accounting being added in batches is anti- It answers and merges stirring in kettle with other compositions again, i.e., add in the small amount of liquids ingredient of equivalent while stirring, so as to promote stirring effect Rate ensures that stirring fusion is uniform, increases product qualification rate, while also have the effect for avoiding waste.
Description of the drawings
Fig. 1 is schematic cross-section of the present invention.
Fig. 2 is schematic cross-section when jacking block of the present invention is contacted with flexible liquid storage container bottom.
Fig. 3 flows to schematic cross-section during liquid collecting container for the liquid in the flexible liquid storage container of the present invention.
Fig. 4 is the schematic cross-section of connecting rod of the present invention.
Specific embodiment
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings:It is a kind of anti-referring to Fig. 1-Fig. 4 The quantitative liquid feeding device of kettle is answered, the housing 1 of cavity is offered including inside, 1 top of housing is connected with liquid injecting pipeline 2, institute It states and quantitative liquor charging component and the lifting assembly with the quantitative liquor charging component cooperation is provided on housing 1.
The quantitative liquor charging component includes the flexible liquid storage container 3 being arranged in the housing 1 and is arranged on the shell Several liquid collecting containers 4 connected on 1 outer wall of body and with the flexible liquid storage container 3, the flexibility liquid storage container 3 are located at the note Immediately below liquid pipe road 2,4 bottom of liquid collecting container offers liquid outlet 41.
The lifting assembly includes the connecting pole 5 being slidably connected on 1 inner wall of housing, is arranged on the connecting pole 5 Connecting rod 51 on top surface, the seal assembly 52 for being arranged on 51 end of connecting rod and the control connecting pole 5 rise or Several cylinders 53 declined are provided with the jacking block 511 coordinated with the flexible liquid storage container 3, the company in the connecting rod 51 Groove body 512 is offered on extension bar 51, the seal assembly 52 is arranged on 512 inner wall of groove body.
The seal assembly 52 includes the No.1 rack 521, gear 522 and the sealing-plug that are engaged successively from outside toward inside Component, the No.1 rack 521 are slidably connected on 512 inner wall of groove body, and 521 lower end of No.1 rack is set There is link block 5211, the link block 5211 and the connecting rod are provided with No.1 spring 5212, the gear between 51 bottom surface 522 are rotatably connected on 512 inner wall of groove body.
The sealing plug assembly includes No. two racks 523 being slidably connected on 512 inner wall of groove body and is arranged on The sealing-plug 524 at 523 top of No. two racks, the sealing-plug 524 are interference fitted, while with the liquid outlet 41 described The push rod component 6 coordinated with the No.1 rack 521 is provided on 4 outer wall of liquid collecting container.
The push rod component 6 include be fixed on 4 outer wall of liquid collecting container fixed block 61, be opened in it is described solid Determine the through-hole on block 61, the mandril being plugged in the through-hole 62, several grooves 63 being opened on the mandril 62 and turn Dynamic to be connected to 61 bottom surface of fixed block and the clamping block 64 coordinated with the groove 63, the 62 upper end end set of mandril has Connection sheet 65, and No. two springs 66 are provided between 61 top surface of the connection sheet 65 and the fixed block, the clamping block 64 with Be provided with torsional spring at the link position of 61 bottom surface of fixed block, when the jacking block 511 with the rising of the connecting pole 5 and with During the contact of 3 bottom of the flexibility liquid storage container, the sealing-plug 524 seals up the liquid outlet 41, is opened inside the connecting pole 5 If cavity forms cavity body 54, motor 55 is provided in the cavity body 54, the motor 55 is with being arranged on the connecting pole 5 The stirring blade 56 of underface is connected.
524 top of sealing-plug is provided with arc-shaped convex block 5241.Since the liquid that liquid outlet comes out can be directly flushed to Sealing-plug top, therefore set arc-shaped convex block that can ensure sealing-plug top not residual liquid, ensure actual ratio and ideal The consistency of ratio promotes product qualification rate.
1 top of housing is provided with several supporting rods 7.By setting supporting rod that whole device is fixed on reaction kettle It is interior.
Waterproof coating is coated on 52 outer surface of seal assembly.Liquid is avoided to be remained on seal assembly outer surface, Influence overall ratio.
Using a kind of reaction kettle as described above method of quantitative liquid feeding device, its step are as follows:1., pass through liquid injecting pipeline Injection needs liquid to be added in flexible liquid storage container;2., start cylinder and motor, connecting pole and rise after by cylinder action, Stirring blade is persistently mixed movement by motor control;3., with the rising of connecting pole, sealing plug assembly rises therewith, when one After number rack is blocked by mandril, No.1 rack is moved relative to connecting pole, and gear is promoted to rotate, meanwhile, gear drives No. two Rack up moves, and sealing-plug rises therewith;4., when the jacking block in connecting rod is contacted with flexible liquid storage container bottom, sealing Plug seals up liquid outlet;5., jacking block continue to rise the liquid level for promoting liquid in flexible liquid storage container and rise, more than liquid collecting container It is flowed into liquid collecting container with the liquid at the position of flexible liquid storage container connector, cylinder stops operation at this time;6., cylinder stops Only after operation 30 seconds, cylinder starts that connecting pole is driven to move down;7., redundance liquid reflux is held to flexible liquid storage in liquid collecting container In device, liquid level keeps horizontal consistent with above-mentioned connector bottom surface in liquid collecting container, reaches quantitative;8., moving down with connecting pole, Sealing-plug leaves liquid outlet, and the liquid in liquid collecting container is flowed into from liquid outlet in reaction kettle, is mixed with other liquid;9., it is complete Into after 2 minutes of the 8. step, cylinder controls connecting pole to rise again.
The fit system cause of setting sealing plug assembly and push rod component is because being added to the amount in flexible liquid storage container Difference can change the position of flexible liquid storage container bottom.
The principle of the fit system is the position by adjusting mandril, to change the position of sealing-plug, so as to according to reality The amount for the liquid being added in flexible liquid storage container controls the position of sealing-plug, ensures in connecting pole and flexible liquid storage container bottom When portion contacts, it can be ensured that sealing-plug seals up liquid outlet, and liquid outlet leakage is avoided to lead to excessive fluid injection.
The fundamental prerequisite of the fit system is that the position of mandril is adjustable.

Claims (6)

1. a kind of quantitative liquid feeding device of reaction kettle, it is characterised in that:The housing of cavity is offered including inside(1), the shell Body(1)Top is connected with liquid injecting pipeline(2), the housing(1)On be provided with quantitative liquor charging component and with the quantitative liquor charging The lifting assembly of component cooperation, the quantitative liquor charging component include being arranged on the housing(1)Interior flexible liquid storage container(3)With And it is arranged on the housing(1)On outer wall and with the flexible liquid storage container(3)Several liquid collecting containers of connection(4), it is described soft Property liquid storage container(3)Positioned at the liquid injecting pipeline(2)Underface, the liquid collecting container(4)Bottom offers liquid outlet(41), institute Lifting assembly is stated to include being slidably connected at the housing(1)Connecting pole on inner wall(5), be arranged on the connecting pole(5)Top surface On connecting rod(51), be arranged on the connecting rod(51)The seal assembly of end(52)And the control connecting pole(5)On Several cylinders for rising or declining(53), the connecting rod(51)On be provided with and the flexible liquid storage container(3)The jacking block of cooperation (511), the connecting rod(51)On offer groove body(512), the seal assembly(52)It is arranged on the groove body(512)Inner wall On, the seal assembly(52)Including the No.1 rack engaged successively from outside toward inside(521), gear(522)And sealing Plug assembly, the No.1 rack(521)It is slidably connected at the groove body(512)On inner wall, and the No.1 rack(521)Lower end End set has link block(5211), the link block(5211)With the connecting rod(51)No.1 spring is provided between bottom surface (5212), the gear(522)It is rotatably connected on the groove body(512)On inner wall, the sealing plug assembly includes being slidably connected In the groove body(512)No. two racks on inner wall(523)And it is arranged on No. two racks(523)The sealing-plug at top (524), while in the liquid collecting container(4)It is provided on outer wall and the No.1 rack(521)The push rod component of cooperation(6), The push rod component(6)Including being fixed at the liquid collecting container(4)Fixed block on outer wall(61), be opened in the fixation Block(61)On through-hole, the mandril that is plugged in the through-hole(62), be opened in the mandril(62)On several grooves(63) And it is rotatably connected on the fixed block(61)Bottom surface and with the groove(63)The clamping block of cooperation(64), the mandril(62) Upper end end set has connection sheet(65), and the connection sheet(65)With the fixed block(61)No. two bullets are provided between top surface Spring(66), the clamping block(64)With the fixed block(61)Torsional spring is provided at the link position of bottom surface, when the jacking block (511)With the connecting pole(5)Rising and with the flexible liquid storage container(3)When bottom contacts, the sealing-plug(524) Seal up the liquid outlet(41), the connecting pole(5)Inside opens up cavity and forms cavity body(54), in the cavity body(54) Inside it is provided with motor(55), the motor(55)With being arranged on the connecting pole(5)The stirring blade of underface(56)It is connected.
2. a kind of quantitative liquid feeding device of reaction kettle according to claim 1, it is characterised in that:The sealing-plug(524) With the liquid outlet(41)Interference fit.
3. a kind of quantitative liquid feeding device of reaction kettle according to claim 1, it is characterised in that:The sealing-plug(524) Top is provided with arc-shaped convex block(5241).
4. a kind of quantitative liquid feeding device of reaction kettle according to claim 1, it is characterised in that:The housing(1)Top It is provided with several supporting rods(7).
5. a kind of quantitative liquid feeding device of reaction kettle according to claim 1, it is characterised in that:The seal assembly(52) Waterproof coating is coated on outer surface.
6. using a kind of reaction kettle as described in claim 1 method of quantitative liquid feeding device, its step are as follows:1., pass through Liquid injecting pipeline(2)Toward flexibility liquid storage container(3)Interior injection needs liquid to be added;2., start cylinder(53)And motor(55), even Connect column(5)By cylinder(53)Rise after effect, stirring blade(56)By motor(55)Control persistently mixes movement;3., with Connecting pole(5)Rising, sealing plug assembly rise therewith, when No.1 rack(521)By mandril(62)After blocking, No.1 rack (521)Relative to connecting pole(5)It is mobile, promote gear(522)Rotation, meanwhile, gear(522)Drive No. two racks(523)It is past Upper movement, sealing-plug(524)Rise therewith;4., work as connecting rod(51)On jacking block(511)With flexible liquid storage container(3)Bottom During contact, sealing-plug(524)Seal up liquid outlet(41);5., jacking block(511)Continue to rise and promote flexible liquid storage container(3)It is interior Liquid liquid level rise, more than liquid collecting container(4)With flexible liquid storage container(3)Liquid at the position of connector is flowed into collection Liquid container(4)It is interior, cylinder at this time(53)It stops operation;6., cylinder(53)After stopping operation 30 seconds, cylinder(53)Start the company of drive Connect column(5)It moves down;7., liquid collecting container(4)Interior redundance liquid reflux is to flexible liquid storage container(3)It is interior, liquid collecting container(4)It is interior Liquid level keeps horizontal consistent with above-mentioned connector bottom surface, reaches quantitative;8., with connecting pole(5)Move down, sealing-plug(524) Leave liquid outlet(41), liquid collecting container(4)Interior liquid is from liquid outlet(41)It is flowed into reaction kettle, is mixed with other liquid; 9., complete 2 minutes of the 8. step after, cylinder(53)Connecting pole is controlled again(5)Rise.
CN201610690065.2A 2016-08-19 2016-08-19 A kind of reaction kettle quantitative liquid feeding device and its application method Active CN106140027B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4402349A (en) * 1978-11-16 1983-09-06 Basf Aktiengesellschaft Process and apparatus for charging tubular reactors with granular solids, more particularly catalysts
CN1572667A (en) * 2003-05-27 2005-02-02 圣-戈宾卡尔玛公司 Twirling dip tube
CN1721292A (en) * 2004-07-15 2006-01-18 增田胜利 Fluid-dispensing pump and container provided therewith
CN101946164A (en) * 2008-02-11 2011-01-12 梅特勒-托利多公开股份有限公司 The dosage-dispensing device that is used for powder and lotion
CN103736612A (en) * 2013-12-21 2014-04-23 中山市美捷时包装制品有限公司 Series sprayer

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4402349A (en) * 1978-11-16 1983-09-06 Basf Aktiengesellschaft Process and apparatus for charging tubular reactors with granular solids, more particularly catalysts
CN1572667A (en) * 2003-05-27 2005-02-02 圣-戈宾卡尔玛公司 Twirling dip tube
CN1721292A (en) * 2004-07-15 2006-01-18 增田胜利 Fluid-dispensing pump and container provided therewith
CN101946164A (en) * 2008-02-11 2011-01-12 梅特勒-托利多公开股份有限公司 The dosage-dispensing device that is used for powder and lotion
CN103736612A (en) * 2013-12-21 2014-04-23 中山市美捷时包装制品有限公司 Series sprayer

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Effective date of registration: 20180315

Address after: No. 77, Wenfeng village, Dongping Town, Yongchun County, Quanzhou, Fujian

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Address before: 362603 No. 77 Wenfeng Village, Dongping Town, Yongchun County, Quanzhou City, Fujian Province

Patentee before: Huang Guozhen