CN106118548A - Carpenter precoats edge sealing polyolefin hot-melt compositions and preparation method thereof - Google Patents

Carpenter precoats edge sealing polyolefin hot-melt compositions and preparation method thereof Download PDF

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Publication number
CN106118548A
CN106118548A CN201610615855.4A CN201610615855A CN106118548A CN 106118548 A CN106118548 A CN 106118548A CN 201610615855 A CN201610615855 A CN 201610615855A CN 106118548 A CN106118548 A CN 106118548A
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Prior art keywords
polyolefin
weight
carpenter
edge sealing
unformed
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CN201610615855.4A
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Chinese (zh)
Inventor
周尚�
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Wuxi City Wan Li Jointing Material Limited-Liability Co
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Wuxi City Wan Li Jointing Material Limited-Liability Co
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Priority to CN201610615855.4A priority Critical patent/CN106118548A/en
Publication of CN106118548A publication Critical patent/CN106118548A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J123/00—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers
    • C09J123/02—Adhesives based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
    • C09J123/04—Homopolymers or copolymers of ethene
    • C09J123/08—Copolymers of ethene
    • C09J123/0807—Copolymers of ethene with unsaturated hydrocarbons only containing more than three carbon atoms
    • C09J123/0815—Copolymers of ethene with aliphatic 1-olefins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02—Non-macromolecular additives
    • C09J11/06—Non-macromolecular additives organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/08—Macromolecular additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2207/00—Properties characterising the ingredient of the composition
    • C08L2207/06—Properties of polyethylene
    • C08L2207/066—LDPE (radical process)

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Laminated Bodies (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention provides a kind of carpenter and precoat edge sealing polyolefin hot-melt compositions, glue is coated on edge band quickly surface drying rolling through frictioning or plastic roll mode, use the pre-edge band coated through professional equipment edge sealing, its glue consumption is little, can effectively reduce tree lace, and weather resistance is improved, particularly there is bigger thermostability, it is characterized in that: it includes following component: unformed polyolefin 45 ~ 55 parts (weight), Low Density Polyethylene 10 20 parts (weight), tackifying resin 20 ~ 30 parts (weight), metallocene catalysis polypropylene wax 2 ~ 5 parts (weight), maleic anhydride modified polypropylene wax 3 ~ 5 parts (weight) and 0.5 ~ 1 part of antioxidant (weight), invention also provides a kind of carpenter and precoat the preparation method of edge sealing polyolefin hot-melt compositions.

Description

Carpenter precoats edge sealing polyolefin hot-melt compositions and preparation method thereof
Technical field
The present invention relates to the technical field of polyolefin hot-melt, precoat edge sealing polyolefin hot melt particularly to a kind of carpenter Glue composition and preparation method thereof.
Background technology
TPO PUR is a kind of new type bonding agent, and room temperature is solid-state, is melt into liquid when being heated to uniform temperature State, can be used by spraying, roller coating and knife coating procedure, the most again in solid-state, when giving one after melted gluing Constant-pressure, cooling and solidifying i.e. produces good adhesive effect and does not contains any solvent, pollution-free, and production technology is simple, easy to use, Of many uses, can be used for defending the aspects such as material articles for use, packaging, bookbinding, timber, automobile industry.
Currently on the market EVA hot-melt adhesive is generally used for carpenter's edge sealing, after its technique typically uses plastic roll to edge sealing Directly fitting timber, glue consumption is big, the obvious defect of tree lace easily occurs, and weatherability is poor, and use has limitation.
Summary of the invention
For not enough present on prior art, the invention provides a kind of carpenter and precoat edge sealing polyolefin heat
Melt adhesive compound, glue is coated on edge band quickly surface drying rolling through frictioning or plastic roll mode, uses pre- The edge band coated is through professional equipment edge sealing, and its glue consumption is little, can effectively reduce tree lace, and weather resistance is improved, Particularly there is bigger thermostability, invention also provides a kind of carpenter and precoat edge sealing polyolefin hot-melt compositions Preparation method.
To achieve these goals, the present invention is to realize by the following technical solutions: a kind of carpenter precoats edge sealing and uses Polyolefin hot-melt compositions, it is characterised in that: it includes following component:
Unformed polyolefin 45～55 parts (weight), Low Density Polyethylene 10-20 part (weight), tackifying resin 20～30 parts (weight), metallocene catalysis polypropylene wax 2～5 parts (weight), maleic anhydride modified polypropylene wax 3～5 parts (weight) and antioxygen Agent 0.5～1 part (weight).
Described tackifying resin includes the first tackifying resin and the second tackifying resin；Described first tackifying resin is C9 hydrogenation tree Fat FP-125, described second tackifying resin is rosin resin TR7115.
Described unformed polyolefin includes the first unformed polyolefin, the second unformed polyolefin and the 3rd unformed polyene Hydrocarbon: described first unformed polyolefin is unformed polyolefin A PAO 792, described second unformed polyolefin is unformed poly- Alkene APAO888, the 3rd unformed polyolefin is unformed polyolefin A PAO408.
Described antioxidant includes the first antioxidant and the second antioxidant；
A kind of carpenter precoats the preparation method of edge sealing polyolefin hot-melt compositions, and step is as follows:
Metallocene catalysis polypropylene wax, maleic anhydride modified polypropylene wax, tackifying resin and antioxidant are put into electrical heating Heat up in reacting furnace heating, and heating and temperature control, at 180-190 DEG C, is opened stirring, treated to melt completely, add unformed polyolefin And Low Density Polyethylene, after stirring 20-40 minute, open evacuation, vacuum pressure is less than-0.9MPa, continues stirring 60-90 and divides Clock, it is ensured that material melts uniformly after and get final product.
In the above-mentioned component of the present invention, it includes following component: unformed polyolefin 45～55 parts (weight), low-density are gathered Ethylene 10-20 part (weight), tackifying resin 20～30 parts (weight), metallocene catalysis polypropylene wax 2～5 parts of (weight), Malaysias Anhydride modified polypropylene wax 3～5 parts (weight) and antioxidant 0.5～1 part (weight), glue is coated with through frictioning or plastic roll mode Cloth is quick surface drying rolling on edge band, uses the pre-edge band coated through professional equipment edge sealing, and its glue consumption is little, can be effective Reduction tree lace, and weather resistance is improved, and particularly has bigger thermostability.
Detailed description of the invention
A kind of carpenter precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: it includes following component:
Unformed polyolefin 45～55 parts (weight), Low Density Polyethylene 10-20 part (weight), tackifying resin 20～30 parts (weight), metallocene catalysis polypropylene wax 2～5 parts (weight), maleic anhydride modified polypropylene wax 3～5 parts (weight) and antioxygen Agent 0.5～1 part (weight).
In following embodiment: first unformed polyolefin A PAO the 792, second unformed polyolefin A PAO888, the 3rd nothing Sizing polyolefin A PAO408 can be buied by Germany's Degussa, and low density polyethylene 955 can be buied by Korea S Han Hua, and first Tackifying resin FP-125 can be buied by Taiwan and benefit, and the second tackifying resin TR7115 can be buied by Arizona, USA chemistry, cyclopentadienyl Metal catalytic polypropylene wax PP2602, maleic anhydride modified polypropylene wax PPMA7452 can be buied by Germany Ke Laien, and first resists Oxygen agent the 1010, second irgasfos 168 can be buied by Germany's BASF.
Embodiment 1
Preparation method is as follows:
By metallocene catalysis polypropylene wax PP2602, maleic anhydride modified polypropylene wax PPMA7452 tackifying resin FP- 125, TR7115 and the first antioxidant 1010, the first irgasfos 168 put into the heating that heats up in electrical heating reacting furnace, heating-up temperature control System, at 180 DEG C, is opened stirring, is treated to melt completely, adds the first unformed polyolefin A PAO792, the second unformed polyolefin APAO888, the 3rd unformed polyolefin A PAO408 and low density polyethylene 955, after stirring 30 minutes, open and take out very Sky, vacuum pressure is less than-0.9MPa, continues stirring 60 minutes, it is ensured that material melts uniformly after and get final product.
Unformed polyolefin is ethylene-propylene copolymer, comprehensive softening point, the strength of materials, and hardness etc. feature is preferred APAO 792, the comprehensive preferred proportion of APAO888, APAO408 45～55 parts (weight).
Low Density Polyethylene is LDPE 955, Vicat softening point 85 DEG C, melt index 6-8g/10min, preferred proportion 10- 20 parts (weight).
Tackifying resin is C9 hydrogenated resin FP-125, softening point 125 DEG C, rosin resin TR7115, softening point 115 DEG C, combines Close preferred proportion 20～30 parts (weight).
Metallocene catalysis polypropylene wax is PP2602, softening point 100 DEG C, preferred proportion 2-5 part (weight).Maleic anhydride changes Property polypropylene wax is PPMA7452, softening point 160 DEG C, preferred proportion 3-5 part (weight).
Embodiment 2
Preparation method is as follows:
By metallocene catalysis polypropylene wax PP2602, maleic anhydride modified polypropylene wax PPMA7452 tackifying resin FP- 125, TR7115 and the first antioxidant 1010, the first irgasfos 168 put into the heating that heats up in electrical heating reacting furnace, heating-up temperature control System, at 180 DEG C, is opened stirring, is treated to melt completely, adds the first unformed polyolefin A PAO792, the second unformed polyolefin APAO888, the 3rd unformed polyolefin A PAO408 and low density polyethylene 955, after stirring 20 minutes, open and take out very Sky, vacuum pressure is less than-0.9MPa, continues stirring 90 minutes, it is ensured that material melts uniformly after and get final product.
Unformed polyolefin is ethylene-propylene copolymer, comprehensive softening point, the strength of materials, and hardness etc. feature is preferred
APAO 792, the comprehensive preferred proportion of APAO888, APAO408 45～55 parts (weight).
Low Density Polyethylene is LDPE 955, Vicat softening point 85 DEG C, melt index 6-8g/10min, preferred proportion 10- 20 parts (weight).
Tackifying resin is C9 hydrogenated resin FP-125, softening point 125 DEG C, rosin resin TR7115, softening point 115 DEG C, combines Close preferred proportion 20～30 parts (weight).
Metallocene catalysis polypropylene wax is PP2602, softening point 100 DEG C, preferred proportion 2-5 part (weight).Maleic anhydride changes Property polypropylene wax is PPMA7452, softening point 160 DEG C, preferred proportion 3-5 part (weight).
Embodiment 3
Preparation method is as follows:
By metallocene catalysis polypropylene wax PP2602, maleic anhydride modified polypropylene wax PPMA7452 tackifying resin FP- 125, TR7115 and the first antioxidant 1010, the first irgasfos 168 put into the heating that heats up in electrical heating reacting furnace, heating-up temperature control System, at 190 DEG C, is opened stirring, is treated to melt completely, adds the first unformed polyolefin A PAO792, the second unformed polyolefin APAO888, the 3rd unformed polyolefin A PAO408 and low density polyethylene 955, after stirring 40 minutes, open and take out very Sky, vacuum pressure is less than-0.9MPa, continues stirring 90 minutes, it is ensured that material melts uniformly after and get final product.
Unformed polyolefin is ethylene-propylene copolymer, comprehensive softening point, the strength of materials, and hardness etc. feature is preferred
APAO 792, the comprehensive preferred proportion of APAO888, APAO408 45～55 parts (weight).
Low Density Polyethylene is LDPE 955, Vicat softening point 85 DEG C, melt index 6-8g/10min, preferred proportion 10- 20 parts (weight).
Tackifying resin is C9 hydrogenated resin FP-125, softening point 125 DEG C, rosin resin TR7115, softening point 115 DEG C, combines Close preferred proportion 20～30 parts (weight).
Metallocene catalysis polypropylene wax is PP2602, softening point 100 DEG C, preferred proportion 2-5 part (weight).
Maleic anhydride modified polypropylene wax is PPMA7452, softening point 160 DEG C, preferred proportion 3-5 part (weight).
Embodiment 4
Preparation method is as follows:
By metallocene catalysis polypropylene wax PP2602, maleic anhydride modified polypropylene wax PPMA7452 tackifying resin FP- 125, TR7115 and the first antioxidant 1010, the first irgasfos 168 put into the heating that heats up in electrical heating reacting furnace, heating-up temperature control System, at 185 DEG C, is opened stirring, is treated to melt completely, adds the first unformed polyolefin A PAO792, the second unformed polyolefin APAO888, the 3rd unformed polyolefin A PAO408 and low density polyethylene 955, after stirring 40 minutes, open and take out very Sky, vacuum pressure is less than-0.9MPa, continues stirring 75 minutes, it is ensured that material melts uniformly after and get final product.
Unformed polyolefin is ethylene-propylene copolymer, comprehensive softening point, the strength of materials, and hardness etc. feature is preferred APAO 792, the comprehensive preferred proportion of APAO888, APAO408 45～55 parts (weight).Low Density Polyethylene is LDPE 955, dimension Card softening point 85 DEG C, melt index 6-8g/10min, preferred proportion 10-20 part (weight).
Tackifying resin is C9 hydrogenated resin FP-125, softening point 125 DEG C, rosin resin TR7115, softening point 115 DEG C, combines Close preferred proportion 20～30 parts (weight).
Metallocene catalysis polypropylene wax is PP2602, softening point 100 DEG C, preferred proportion 2-5 part (weight).
Maleic anhydride modified polypropylene wax is PPMA7452, softening point 160 DEG C, preferred proportion 3-5 part (weight).
The carpenter of table 1 embodiment 1～4 preparation precoats edge sealing polyolefin hot-melt composition properties and compares

Claims (10)

1. a carpenter precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: it includes following component:
Unformed polyolefin 45 ~ 55 parts (weight), Low Density Polyethylene 10-20 part (weight), tackifying resin 20 ~ 30 parts (weight Amount), metallocene catalysis polypropylene wax 2 ~ 5 parts (weight), maleic anhydride modified polypropylene wax 3 ~ 5 parts (weight) and antioxidant 0.5 ~ 1 part (weight).
A kind of carpenter the most according to claim 1 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: without fixed Type polyolefin is ethylene-propylene copolymer.
A kind of carpenter the most according to claim 1 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described Low Density Polyethylene is LDPE 955, and described metallocene catalysis polypropylene wax is PP2602, described maleic anhydride modified polypropylene Wax is PPMA7452.
A kind of carpenter the most according to claim 1 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described Tackifying resin includes the first tackifying resin and the second tackifying resin.
A kind of carpenter the most according to claim 4 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described First tackifying resin is C9 hydrogenated resin FP-125, and described second tackifying resin is rosin resin TR7115.
6. precoating edge sealing polyolefin hot-melt compositions according to a kind of carpenter described in claims 1 or 2, its feature exists In: described unformed polyolefin includes the first unformed polyolefin, the second unformed polyolefin and the 3rd unformed polyolefin.
A kind of carpenter the most according to claim 6 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described First unformed polyolefin is unformed polyolefin A PAO 792, and described second unformed polyolefin is unformed polyolefin APAO888, the 3rd unformed polyolefin is unformed polyolefin A PAO408.
A kind of carpenter the most according to claim 1 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described Antioxidant includes the first antioxidant and the second antioxidant.
A kind of carpenter the most according to claim 8 precoats edge sealing polyolefin hot-melt compositions, it is characterised in that: described First antioxidant is antioxidant 1010, and described second antioxidant is irgasfos 168.
10. a carpenter precoats the preparation method of edge sealing polyolefin hot-melt compositions, it is characterised in that: it includes walking as follows Rapid:
Metallocene catalysis polypropylene wax, maleic anhydride modified polypropylene wax, tackifying resin and antioxidant are put into electrical heating reaction Heat up in stove heating, and heating and temperature control at 180-190 DEG C, is opened stirring, treated to melt completely, adds unformed polyolefin and low Density polyethylene, after stirring 20-40 minute, opens evacuation, and vacuum pressure is less than-0.9MPa, continues stirring 60-90 minute, Guarantee after material melts is uniformly and get final product.
CN201610615855.4A 2016-07-29 2016-07-29 Carpenter precoats edge sealing polyolefin hot-melt compositions and preparation method thereof Pending CN106118548A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108192531A (en) * 2017-12-29 2018-06-22 中山诚泰化工科技有限公司 High-temperature-resistance polyolefin hot melt adhesive and preparation method thereof
JP2020002283A (en) * 2018-06-29 2020-01-09 東洋インキＳｃホールディングス株式会社 Hot melt adhesive for laminate, and laminate film laminate using the same
CN111073552A (en) * 2020-01-02 2020-04-28 佛山市同人粘胶有限公司 Hot melt adhesive for coating wood section with decorative veneer and production process thereof
CN113563828A (en) * 2021-08-03 2021-10-29 广州波塞冬材料科技有限公司 Foaming hot melt adhesive applied to filter and preparation method

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US20120328805A1 (en) * 2011-06-27 2012-12-27 H.B. Fuller Company Hot melt adhesive compositions including olefinic polymer blends and articles including the same
CN103031100A (en) * 2012-12-13 2013-04-10 嘉兴市恒泰化工科技有限公司 Reactive polyurethane hot-melt adhesive for edge sealing in wood industry and preparation method thereof
US20140272214A1 (en) * 2013-03-12 2014-09-18 Henkel Ltd. Adhesive compostions with wide service temperature window and use thereof
CN105623556A (en) * 2014-10-25 2016-06-01 刘荣伟 Formula of hot melt adhesive for furniture edge sealing

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Publication number Priority date Publication date Assignee Title
US20120328805A1 (en) * 2011-06-27 2012-12-27 H.B. Fuller Company Hot melt adhesive compositions including olefinic polymer blends and articles including the same
CN102786895A (en) * 2012-09-11 2012-11-21 无锡市万力粘合材料有限公司 Hot-melt adhesive for transparent PP (polypropylene) boxes and preparation method of hot-melt adhesive
CN103031100A (en) * 2012-12-13 2013-04-10 嘉兴市恒泰化工科技有限公司 Reactive polyurethane hot-melt adhesive for edge sealing in wood industry and preparation method thereof
US20140272214A1 (en) * 2013-03-12 2014-09-18 Henkel Ltd. Adhesive compostions with wide service temperature window and use thereof
CN105623556A (en) * 2014-10-25 2016-06-01 刘荣伟 Formula of hot melt adhesive for furniture edge sealing

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108192531A (en) * 2017-12-29 2018-06-22 中山诚泰化工科技有限公司 High-temperature-resistance polyolefin hot melt adhesive and preparation method thereof
JP2020002283A (en) * 2018-06-29 2020-01-09 東洋インキＳｃホールディングス株式会社 Hot melt adhesive for laminate, and laminate film laminate using the same
JP7101933B2 (en) 2018-06-29 2022-07-19 東洋インキＳｃホールディングス株式会社 Hot melt adhesive for laminating and laminated film laminate using it
CN111073552A (en) * 2020-01-02 2020-04-28 佛山市同人粘胶有限公司 Hot melt adhesive for coating wood section with decorative veneer and production process thereof
CN113563828A (en) * 2021-08-03 2021-10-29 广州波塞冬材料科技有限公司 Foaming hot melt adhesive applied to filter and preparation method

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Application publication date: 20161116