CN106116447A - Antifreeze ceramic of corrosion-and high-temp-resistant and preparation method thereof - Google Patents
Antifreeze ceramic of corrosion-and high-temp-resistant and preparation method thereof Download PDFInfo
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3244—Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
- C04B2235/9669—Resistance against chemicals, e.g. against molten glass or molten salts
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Abstract
The present invention relates to a kind of antifreeze ceramic of corrosion-and high-temp-resistant and preparation method thereof, belong to ceramic technology field.The antifreeze ceramic of this corrosion-and high-temp-resistant includes the following raw material according to mass fraction meter: nepheline syenite 15 20 parts, Liling Kaolin 30 38 parts, Luochuan Loess 10 16 parts, waste old ceramics biscuit process 10 20 parts of material, Boccaro shale 59 parts, flint clay 47 parts, calcium zirconate 24 parts, andalusite 5 10 parts, Pulvis Talci 10 15 parts, bentonite 9 14 parts.The present invention is by studying ceramic raw material, obtain a kind of excellent performance and lower-cost Ceramic Material, its hardness of ceramic and the toughness fired according to the present invention are the most preferable, non-friable, and weatherability is preferable, the most easy to change, in addition, the present invention by waste old ceramics biscuit is reprocessed, be effectively ensured its in secondary recovery utilizes with the matching of other raw materials.
Description
Technical field
The invention belongs to ceramic technology field, be specifically related to a kind of antifreeze ceramic of corrosion-and high-temp-resistant and making side thereof
Method.
Background technology
Pottery is the general designation of pottery and porcelain, and ceramic material is oxide, nitride, boride and carbide etc. mostly,
Common ceramic material has clay, aluminium oxide, Kaolin etc., ceramic of a great variety, is broadly divided into domestic ceramics, building
Pottery, pottery and special cermacis etc., be typically based on the difference of ceramic species, and select different raw material compositions to burn
System, the topmost advantage of ceramic of excellent performance is exactly corrosion-resistant, but due to ceramic deficiency in dispensing, though
So it has the advantage that hardness is high, but its toughness is poor, heat-resisting quantity has much room for improvement, and freeze-proof is the best, too low in temperature
Time can produce tiny crackle, additionally, the decay resistance of ordinary pottery products also has much room for improvement.
The production cost of the ceramic of current existing excellent performance is the highest, and therefore it is popularized and is restricted, and
In brother Ceramic Production producer, there is substantial amounts of waste ceramic biscuit, waste ceramic biscuit will not be carried out by most of producers
Secondary recovery utilizes, if being because dealing with the secondary recovery of waste ceramic biscuit improperly, it is likely that can cause ceramic by the gross
Product are scrapped again, and therefore the recycling to waste old ceramics biscuit also seems particularly important.
In sum, how waste old ceramics biscuit is reprocessed, and be allowed to and other raw material Proper Matchs, and obtain
The ceramic raw material of a kind of superior performance is just particularly important.
Summary of the invention
The invention aims to solve the deficiencies in the prior art, and a kind of antifreeze ceramic of corrosion-and high-temp-resistant is provided
Product and preparation method thereof, ceramic of the present invention has heat-resisting quantity and the freeze-proof of excellence, and has splendid corrosion resistance.
The present invention adopts the following technical scheme that
The antifreeze ceramic of corrosion-and high-temp-resistant, the following raw material including according to mass fraction meter: nepheline syenite 15-20 part,
Liling Kaolin 30-38 part, Luochuan Loess 10-16 part, waste old ceramics biscuit process material 10-20 part, Boccaro shale 5-9 part, Jiao
Gem 4-7 part, calcium zirconate 2-4 part, andalusite 5-10 part, Pulvis Talci 10-15 part, bentonite 9-14 part.
Further, the antifreeze ceramic of described corrosion-and high-temp-resistant, the most former including according to mass fraction meter
Material: nepheline syenite 18 parts, Liling Kaolin 35 parts, Luochuan Loess 15 parts, waste old ceramics biscuit process material 15 parts, Boccaro shale
7 parts, flint clay 5 parts, calcium zirconate 3 parts, andalusite 7 parts, Pulvis Talci 12 parts, bentonite 11 parts.
Further, the antifreeze ceramic of described corrosion-and high-temp-resistant, wherein said waste old ceramics biscuit processes material
Prepare in accordance with the following methods: waste old ceramics biscuit is crushed to graininess, immerse the water reducer that mass concentration is 10%-20% water-soluble
In liquid, ultrasonic vibration 35-40min, filter, wash, dry,.
Further, the antifreeze ceramic of described corrosion-and high-temp-resistant, wherein said water reducer is lignin sulfonic acid
Calcium.
The manufacture method of the antifreeze ceramic of described corrosion-and high-temp-resistant, step is as follows:
Step one: according to described proportioning raw materials, nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit are processed
Material, Boccaro shale and flint clay mix homogeneously, pulverize, be ground to 800-900 mesh sieve, and obtained abrasive；
Step 2, according to described proportioning raw materials, by calcium zirconate, andalusite, Pulvis Talci and bentonite mix homogeneously, pulverizes, grinds
To crossing 800-850 mesh sieve, then after mixing homogeneously with step one gained abrasive, add the water of compound gross mass 10%-12%, mixed
Conjunction stirs, and obtains pug；
Step 3, by compressing for step 2 gained pug, depanning obtains moulded pottery not yet put in a kiln to bake；
Step 4, being dried step 3 gained moulded pottery not yet put in a kiln to bake to water content is 1%-2%, obtains dry body；
Step 5, fires 2-3h by step 4 gained dry body at 1280-1290 DEG C, obtains the antifreeze pottery of described corrosion-and high-temp-resistant
Ceramic products.
Further, the manufacture method of the antifreeze ceramic of described corrosion-and high-temp-resistant, wherein by step 3 gained
Moulded pottery not yet put in a kiln to bake is placed in dry kiln and is dried.
Compared with prior art, it has the beneficial effect that the present invention
The present invention by ceramic raw material is studied, obtain a kind of excellent performance and lower-cost pottery former
Material, by processing material, Boccaro shale, flint clay, zirconium by nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit
Acid calcium, andalusite, Pulvis Talci and bentonite reasonable coordination, make to fire and obtain ceramic and have excellent resistance to elevated temperatures, anti-
Freezing performance and decay resistance, its hardness of ceramic fired according to the present invention and toughness are all preferable, non-friable, and weatherability
Preferably, the most easy to change, additionally, the present invention is by reprocessing waste old ceramics biscuit, it is effectively ensured in secondary recovery
With the matching of other raw materials in utilization, energy-conserving and environment-protective.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is merely to illustrate the present invention, and should not be regarded as limiting this
Bright scope.
Embodiment 1
The antifreeze ceramic of corrosion-and high-temp-resistant, the following raw material including according to mass fraction meter: nepheline syenite 18 parts, Liling
Kaolin 35 parts, Luochuan Loess 15 parts, waste old ceramics biscuit process 15 parts of material, Boccaro shale 7 parts, flint clay 5 parts, calcium zirconate 3
Part, andalusite 7 parts, Pulvis Talci 12 parts, bentonite 11 parts.Wherein said waste old ceramics biscuit processes material and makes in accordance with the following methods
: waste old ceramics biscuit is crushed to graininess, immerses in the calcium lignosulfonate aqueous solution that mass concentration is 15%, ultrasonic shake
Swing 38min, filter, wash, dry,.
The manufacture method of the antifreeze ceramic of described corrosion-and high-temp-resistant, step is as follows:
Step one: according to described proportioning raw materials, nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit are processed
Material, Boccaro shale and flint clay mix homogeneously, pulverize, be ground to 900 mesh sieves, and obtained abrasive；
Step 2, according to described proportioning raw materials, by calcium zirconate, andalusite, Pulvis Talci and bentonite mix homogeneously, pulverizes, grinds
To crossing 850 mesh sieves, then after mixing homogeneously with step one gained abrasive, adding the water of compound gross mass 12%, mix and blend is equal
Even, obtain pug；
Step 3, by compressing for step 2 gained pug, depanning obtains moulded pottery not yet put in a kiln to bake；
Step 4, is placed in step 3 gained moulded pottery not yet put in a kiln to bake in dry kiln that to be dried to water content be 2%, obtains dry body；
Step 5, fires 2.5h by step 4 gained dry body at 1285 DEG C, obtains the antifreeze ceramic of described corrosion-and high-temp-resistant
Product.
Embodiment 2
The antifreeze ceramic of corrosion-and high-temp-resistant, the following raw material including according to mass fraction meter: nepheline syenite 15 parts, Liling
Kaolin 30 parts, Luochuan Loess 10 parts, waste old ceramics biscuit process 10 parts of material, Boccaro shale 5 parts, flint clay 4 parts, calcium zirconate 2
Part, andalusite 5 parts, Pulvis Talci 10 parts, bentonite 9 parts.Wherein said waste old ceramics biscuit processes material and prepares in accordance with the following methods:
Waste old ceramics biscuit is crushed to graininess, immerses in the calcium lignosulfonate aqueous solution that mass concentration is 10%, ultrasonic vibration
40min, filters, washes, and dries,.
The manufacture method of the antifreeze ceramic of described corrosion-and high-temp-resistant, step is as follows:
Step one: according to described proportioning raw materials, nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit are processed
Material, Boccaro shale and flint clay mix homogeneously, pulverize, be ground to 800 mesh sieves, and obtained abrasive；
Step 2, according to described proportioning raw materials, by calcium zirconate, andalusite, Pulvis Talci and bentonite mix homogeneously, pulverizes, grinds
To crossing 800 mesh sieves, then after mixing homogeneously with step one gained abrasive, adding the water of compound gross mass 10%, mix and blend is equal
Even, obtain pug；
Step 3, by compressing for step 2 gained pug, depanning obtains moulded pottery not yet put in a kiln to bake；
Step 4, is placed in step 3 gained moulded pottery not yet put in a kiln to bake in dry kiln that to be dried to water content be 1%, obtains dry body；
Step 5, fires 3h by step 4 gained dry body at 1280 DEG C, obtains the antifreeze ceramic of described corrosion-and high-temp-resistant.
Embodiment 3
The antifreeze ceramic of corrosion-and high-temp-resistant, the following raw material including according to mass fraction meter: nepheline syenite 20 parts, Liling
Kaolin 38 parts, Luochuan Loess 16 parts, waste old ceramics biscuit process 20 parts of material, Boccaro shale 9 parts, flint clay 7 parts, calcium zirconate 4
Part, andalusite 10 parts, Pulvis Talci 15 parts, bentonite 14 parts.Wherein said waste old ceramics biscuit processes material and makes in accordance with the following methods
: waste old ceramics biscuit is crushed to graininess, immerses in the calcium lignosulfonate aqueous solution that mass concentration is 20%, ultrasonic shake
Swing 35min, filter, wash, dry,.
The manufacture method of the antifreeze ceramic of described corrosion-and high-temp-resistant, step is as follows:
Step one: according to described proportioning raw materials, nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit are processed
Material, Boccaro shale and flint clay mix homogeneously, pulverize, be ground to 900 mesh sieves, and obtained abrasive；
Step 2, according to described proportioning raw materials, by calcium zirconate, andalusite, Pulvis Talci and bentonite mix homogeneously, pulverizes, grinds
To crossing 850 mesh sieves, then after mixing homogeneously with step one gained abrasive, adding the water of compound gross mass 12%, mix and blend is equal
Even, obtain pug；
Step 3, by compressing for step 2 gained pug, depanning obtains moulded pottery not yet put in a kiln to bake；
Step 4, is placed in step 3 gained moulded pottery not yet put in a kiln to bake in dry kiln that to be dried to water content be 2%, obtains dry body；
Step 5, fires 2h by step 4 gained dry body at 1290 DEG C, obtains the antifreeze ceramic of described corrosion-and high-temp-resistant.
The rupture strength of the ceramic fired according to embodiment 1 to 3 is respectively 26.9MPa, 25.6MPa, 25.8MPa,
It is the aqueous hydrochloric acid solution of 30% every 2h in its surface sprinkling mass concentration, after 48h, checks ceramic surface, ceramic table
Face is not all any change, and clear water checks again for surface after rinsing, and ceramic surface color is the most unchanged；Additionally, will implement
The ceramic that example 1 to 3 is fired is under 200 DEG C of high temperature after constant temperature holding 2h, and at subzero 20 DEG C, constant temperature keeps 1h, ceramic
Surface and inner cross-sectional have no significant change, and crackle do not occur.
Skilled person will appreciate that of the industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation
The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, the present invention also has
Various changes and modifications, these changes and improvements both fall within scope of the claimed invention.Claimed scope
Defined by appending claims and equivalent thereof.
Claims (6)
1. the antifreeze ceramic of corrosion-and high-temp-resistant, it is characterised in that include the following raw material according to mass fraction meter: nepheline is just
Anhydrite 15-20 part, Liling Kaolin 30-38 part, Luochuan Loess 10-16 part, waste old ceramics biscuit process material 10-20 part, boccaro
Shale 5-9 part, flint clay 4-7 part, calcium zirconate 2-4 part, andalusite 5-10 part, Pulvis Talci 10-15 part, bentonite 9-14 part.
The antifreeze ceramic of corrosion-and high-temp-resistant the most according to claim 1, it is characterised in that include according to mass fraction
The following raw material of meter: nepheline syenite 18 parts, Liling Kaolin 35 parts, Luochuan Loess 15 parts, waste old ceramics biscuit process material 15
Part, Boccaro shale 7 parts, flint clay 5 parts, calcium zirconate 3 parts, andalusite 7 parts, Pulvis Talci 12 parts, bentonite 11 parts.
The antifreeze ceramic of corrosion-and high-temp-resistant the most according to claim 1, it is characterised in that described waste old ceramics biscuit
Processing material to prepare in accordance with the following methods: waste old ceramics biscuit is crushed to graininess, immersing mass concentration is the diminishing of 10%-20%
In agent aqueous solution, ultrasonic vibration 35-40min, filter, wash, dry,.
The antifreeze ceramic of corrosion-and high-temp-resistant the most according to claim 3, it is characterised in that described water reducer is wooden
Element sulfoacid calcium.
5. the manufacture method of the antifreeze ceramic of corrosion-and high-temp-resistant described in claim 1, it is characterised in that step is as follows:
Step one: according to described proportioning raw materials, nepheline syenite, Liling Kaolin, Luochuan Loess, waste old ceramics biscuit are processed
Material, Boccaro shale and flint clay mix homogeneously, pulverize, be ground to 800-900 mesh sieve, and obtained abrasive；
Step 2, according to described proportioning raw materials, by calcium zirconate, andalusite, Pulvis Talci and bentonite mix homogeneously, pulverizes, grinds
To crossing 800-850 mesh sieve, then after mixing homogeneously with step one gained abrasive, add the water of compound gross mass 10%-12%, mixed
Conjunction stirs, and obtains pug；
Step 3, by compressing for step 2 gained pug, depanning obtains moulded pottery not yet put in a kiln to bake；
Step 4, being dried step 3 gained moulded pottery not yet put in a kiln to bake to water content is 1%-2%, obtains dry body；
Step 5, fires 2-3h by step 4 gained dry body at 1280-1290 DEG C, obtains the antifreeze pottery of described corrosion-and high-temp-resistant
Ceramic products.
The manufacture method of the antifreeze ceramic of corrosion-and high-temp-resistant the most according to claim 5, it is characterised in that by step
Three gained moulded pottery not yet put in a kiln to bakes are placed in dry kiln and are dried.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110002849A (en) * | 2019-04-28 | 2019-07-12 | 福建省德化县盛鼎瓷艺有限公司 | A kind of preparation method preparing high-performance abrasion-proof domestic ceramics using waste old ceramics |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110002849A (en) * | 2019-04-28 | 2019-07-12 | 福建省德化县盛鼎瓷艺有限公司 | A kind of preparation method preparing high-performance abrasion-proof domestic ceramics using waste old ceramics |
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Application publication date: 20161116 |