CN106113214A - The preparation method of compound flame retardant fibre board - Google Patents
The preparation method of compound flame retardant fibre board Download PDFInfo
- Publication number
- CN106113214A CN106113214A CN201610485042.8A CN201610485042A CN106113214A CN 106113214 A CN106113214 A CN 106113214A CN 201610485042 A CN201610485042 A CN 201610485042A CN 106113214 A CN106113214 A CN 106113214A
- Authority
- CN
- China
- Prior art keywords
- fibre board
- fiber
- dry weight
- fire retardant
- gross dry
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 133
- 239000003063 flame retardant Substances 0.000 title claims abstract description 87
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 150000001875 compounds Chemical class 0.000 title claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 54
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 21
- 229920001131 Pulp (paper) Polymers 0.000 claims abstract description 17
- 239000010893 paper waste Substances 0.000 claims abstract description 17
- 239000003513 alkali Substances 0.000 claims abstract description 14
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052901 montmorillonite Inorganic materials 0.000 claims abstract description 12
- 229910021538 borax Inorganic materials 0.000 claims abstract description 8
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 8
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 8
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000010907 mechanical stirring Methods 0.000 claims abstract description 7
- 238000005070 sampling Methods 0.000 claims abstract description 7
- 230000008569 process Effects 0.000 claims description 34
- 229940059574 pentaerithrityl Drugs 0.000 claims description 19
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 19
- 239000011248 coating agent Substances 0.000 claims description 14
- 238000000576 coating method Methods 0.000 claims description 14
- 229920002472 Starch Polymers 0.000 claims description 13
- 239000008107 starch Substances 0.000 claims description 13
- 235000019698 starch Nutrition 0.000 claims description 13
- 238000007731 hot pressing Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 10
- 238000013019 agitation Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 238000010494 dissociation reaction Methods 0.000 claims description 6
- 230000005593 dissociations Effects 0.000 claims description 6
- 238000003825 pressing Methods 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 4
- 239000000463 material Substances 0.000 abstract description 28
- 230000007423 decrease Effects 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 12
- 239000000654 additive Substances 0.000 description 11
- 230000000996 additive effect Effects 0.000 description 11
- 238000005253 cladding Methods 0.000 description 11
- 230000008719 thickening Effects 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000011230 binding agent Substances 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 230000008961 swelling Effects 0.000 description 3
- 229910018557 Si O Inorganic materials 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229920002521 macromolecule Polymers 0.000 description 2
- 238000002464 physical blending Methods 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012757 flame retardant agent Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- -1 tripolycyanamide Chemical compound 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27N—MANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
- B27N3/00—Manufacture of substantially flat articles, e.g. boards, from particles or fibres
- B27N3/04—Manufacture of substantially flat articles, e.g. boards, from particles or fibres from fibres
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27N—MANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
- B27N3/00—Manufacture of substantially flat articles, e.g. boards, from particles or fibres
- B27N3/08—Moulding or pressing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27N—MANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
- B27N7/00—After-treatment, e.g. reducing swelling or shrinkage, surfacing; Protecting the edges of boards against access of humidity
- B27N7/005—Coating boards, e.g. with a finishing or decorating layer
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
- D21B1/00—Fibrous raw materials or their mechanical treatment
- D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
- D21B1/12—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
- D21B1/30—Defibrating by other means
- D21B1/32—Defibrating by other means of waste paper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21B—FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
- D21B1/00—Fibrous raw materials or their mechanical treatment
- D21B1/04—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
- D21B1/12—Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
- D21B1/30—Defibrating by other means
- D21B1/34—Kneading or mixing; Pulpers
- D21B1/345—Pulpers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/64—Paper recycling
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Manufacturing & Machinery (AREA)
- Forests & Forestry (AREA)
- Mechanical Engineering (AREA)
- Paper (AREA)
- Dry Formation Of Fiberboard And The Like (AREA)
Abstract
Description
Claims (3)
- The preparation method of the most compound flame retardant fibre board, it is characterised in that comprise the following steps:(1) process of waste paper pulp fiber:The waste paper pulp fiber collected is pulverized, adds and the NaOH alkali liquor of mass concentration 2% impregnates 24h, then clean with water, so Dissociate at 5000r/min with fiber dissociation device afterwards, and clean with water, by complete for alkali eccysis;Calculating fiber gross dry weight:Sampling drying, calculates sample moisture content, and then calculates fiber gross dry weight;(3) dispensing:The Borax of fiber gross dry weight 3%-6% will be accounted for, account for the Firebrake ZB of fiber gross dry weight 3%-5%, account for fiber gross dry weight 20%-40%'s Fiber after montmorillonite processes with step (1) mixes, under mechanical stirring, mix homogeneously, become blank, mixing speed is 200r/min-400r/min, time 30min-60min;(4) preparation of fibre board:Blank is put into fibre board mould middle berth and dresses up type, then be prepared as fibre board through cold, hot pressure two-step method, wherein, cold Pressure 4-6MPa during pressure, temperature of colding pressing is room temperature, pressure 4-6MPa during hot pressing, and hot pressing temperature is 120-180 DEG C;(5) coating:By the surface-coated expanding fire retardant of fibre board, room temperature is dried, flame retardant fibre board, described expanding fire retardant coating Amount is the 6-18% of fibre board gross weight;Described expanding fire retardant is by percentage by weight meter: APP 35-45%, tripolycyanamide 20-35%, tetramethylolmethane 15%-30%, starch 10%-20% make, and wherein, first APP, tripolycyanamide, tetramethylolmethane are sequentially added in beaker, then Add water, the addition of water be APP, tripolycyanamide, 1-1.5 times of tetramethylolmethane gross weight, magnetic agitation under room temperature 5min-10min, mixing speed is 200-300r/min, is subsequently adding starch, 60 DEG C of stirring 10min-30min, mix homogeneously, Become expanding fire retardant.
- The preparation method of compound flame retardant fibre board the most according to claim 1, it is characterised in that comprise the following steps:(1) process of waste paper pulp fiber:The waste paper pulp fiber collected is pulverized, adds and the NaOH alkali liquor of mass concentration 2% impregnates 24h, then clean with water, so Dissociate at 5000r/min with fiber dissociation device afterwards, and clean with water, by complete for alkali eccysis;(2) fiber gross dry weight is calculated:Sampling drying, calculates sample moisture content, and then calculates fiber gross dry weight;(3) dispensing:The Borax of fiber gross dry weight 4% will be accounted for, account for the Firebrake ZB of fiber gross dry weight 5%, the montmorillonite accounting for fiber gross dry weight 36% and step Suddenly the fiber after (1) processes mixes, under mechanical stirring, mix homogeneously, become blank, mixing speed is 200r/min- 400r/min, time 30min-60min;(4) preparation of fibre board:Blank is put into fibre board mould middle berth and dresses up type, then be prepared as fibre board through cold, hot pressure two-step method, wherein, cold Pressure 4-6MPa during pressure, temperature of colding pressing is room temperature, pressure 4-6MPa during hot pressing, and hot pressing temperature is 120-180 DEG C;(5) coating:By the surface-coated expanding fire retardant of fibre board, room temperature is dried, flame retardant fibre board, described expanding fire retardant coating Amount is the 15% of fibre board gross weight;Described expanding fire retardant is by percentage by weight meter: APP 41%, tripolycyanamide 30%, tetramethylolmethane 17%, shallow lake Powder 12% is made, and wherein, first APP, tripolycyanamide, tetramethylolmethane is sequentially added in beaker, adds water, the addition of water Amount is APP, tripolycyanamide, 1-1.5 times of tetramethylolmethane gross weight, magnetic agitation 5min-10min under room temperature, stirring is fast Degree is 200-300r/min, is subsequently adding starch, 60 DEG C of stirring 10min-30min, and mix homogeneously becomes expanding fire retardant.
- The preparation method of compound flame retardant fibre board the most according to claim 1, it is characterised in that comprise the following steps:(1) process of waste paper pulp fiber:The waste paper pulp fiber collected is pulverized, adds and the NaOH alkali liquor of mass concentration 2% impregnates 24h, then clean with water, so Dissociate at 5000r/min with fiber dissociation device afterwards, and clean with water, by complete for alkali eccysis;(2) fiber gross dry weight is calculated:Sampling drying, calculates sample moisture content, and then calculates fiber gross dry weight;(3) dispensing:By account for fiber gross dry weight 5% Borax, account for fiber gross dry weight 4% Firebrake ZB, account for the montmorillonite of fiber gross dry weight 37.5% with Fiber after step (1) processes mixes, under mechanical stirring, mix homogeneously, become blank, mixing speed is 200r/ Min-400r/min, time 30min-60min;(4) preparation of fibre board:Blank is put into fibre board mould middle berth and dresses up type, then be prepared as fibre board through cold, hot pressure two-step method, wherein, cold Pressure 4-6MPa during pressure, temperature of colding pressing is room temperature, pressure 4-6MPa during hot pressing, and hot pressing temperature is 120-180 DEG C;(5) coating:By the surface-coated expanding fire retardant of fibre board, room temperature is dried, flame retardant fibre board, described expanding fire retardant coating Amount is the 12% of fibre board gross weight;Described expanding fire retardant is by percentage by weight meter: APP 37%, tripolycyanamide 32%, tetramethylolmethane 21%, shallow lake Powder 10% is made, and wherein, first APP, tripolycyanamide, tetramethylolmethane is sequentially added in beaker, adds water, the addition of water Amount is APP, tripolycyanamide, 1-1.5 times of tetramethylolmethane gross weight, magnetic agitation 5min-10min under room temperature, stirring is fast Degree is 200-300r/min, is subsequently adding starch, 60 DEG C of stirring 10min-30min, and mix homogeneously becomes expanding fire retardant.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610485042.8A CN106113214B (en) | 2016-06-28 | 2016-06-28 | The preparation method of compound flame retardant fibre board |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610485042.8A CN106113214B (en) | 2016-06-28 | 2016-06-28 | The preparation method of compound flame retardant fibre board |
Publications (2)
Publication Number | Publication Date |
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CN106113214A true CN106113214A (en) | 2016-11-16 |
CN106113214B CN106113214B (en) | 2018-06-26 |
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CN201610485042.8A Expired - Fee Related CN106113214B (en) | 2016-06-28 | 2016-06-28 | The preparation method of compound flame retardant fibre board |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106812222A (en) * | 2017-03-24 | 2017-06-09 | 青岛博时阻燃织物有限公司 | A kind of fire-retardant abatvoix one-shot forming automatic production line of polyester fiber |
CN108894042A (en) * | 2018-07-17 | 2018-11-27 | 泾县汇鼎锋建筑装饰工程有限公司 | A kind of modified optimization environment-friendly preparation method of publicity brochure paper |
CN109468891A (en) * | 2018-11-22 | 2019-03-15 | 山东如意科技集团有限公司 | A kind of waste fabric fiberboard and its manufacturing method |
CN109853289A (en) * | 2019-03-15 | 2019-06-07 | 浙江科技学院 | A kind of fire-retardant paper base material and preparation method thereof using the preparation of reaction-type flame-retarding fiber |
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JP2006175832A (en) * | 2004-12-24 | 2006-07-06 | Mitsubishi Shoji Construction Materials Corp | Composite material |
CN101638874A (en) * | 2008-08-28 | 2010-02-03 | 杭州拜方生物科技有限公司 | Method for preparing fiber wallboard through wet process |
CN101716793A (en) * | 2009-11-27 | 2010-06-02 | 北京化工大学 | Aluminium hydroxide composite anti-flaming density fiber board and preparation method thereof |
CN101879739A (en) * | 2010-06-24 | 2010-11-10 | 郭明辉 | Manufacturing method for environmental-friendly fire-retardant fiber board |
CN102259369A (en) * | 2011-07-04 | 2011-11-30 | 南京林业大学 | Method for producing MDF (medium density fiberboard) with vermiculite flame retardancy |
CN103087414A (en) * | 2013-01-30 | 2013-05-08 | 北京化工大学常州先进材料研究院 | Composite intumescent flame retardant inflaming retarding general polypropylene and preparation method thereof |
CN103333406A (en) * | 2013-06-05 | 2013-10-02 | 华南理工大学 | Modified intumescent flame-retardant polypropylene composition and preparation method thereof |
-
2016
- 2016-06-28 CN CN201610485042.8A patent/CN106113214B/en not_active Expired - Fee Related
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006175832A (en) * | 2004-12-24 | 2006-07-06 | Mitsubishi Shoji Construction Materials Corp | Composite material |
CN101638874A (en) * | 2008-08-28 | 2010-02-03 | 杭州拜方生物科技有限公司 | Method for preparing fiber wallboard through wet process |
CN101716793A (en) * | 2009-11-27 | 2010-06-02 | 北京化工大学 | Aluminium hydroxide composite anti-flaming density fiber board and preparation method thereof |
CN101879739A (en) * | 2010-06-24 | 2010-11-10 | 郭明辉 | Manufacturing method for environmental-friendly fire-retardant fiber board |
CN102259369A (en) * | 2011-07-04 | 2011-11-30 | 南京林业大学 | Method for producing MDF (medium density fiberboard) with vermiculite flame retardancy |
CN103087414A (en) * | 2013-01-30 | 2013-05-08 | 北京化工大学常州先进材料研究院 | Composite intumescent flame retardant inflaming retarding general polypropylene and preparation method thereof |
CN103333406A (en) * | 2013-06-05 | 2013-10-02 | 华南理工大学 | Modified intumescent flame-retardant polypropylene composition and preparation method thereof |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106812222A (en) * | 2017-03-24 | 2017-06-09 | 青岛博时阻燃织物有限公司 | A kind of fire-retardant abatvoix one-shot forming automatic production line of polyester fiber |
CN108894042A (en) * | 2018-07-17 | 2018-11-27 | 泾县汇鼎锋建筑装饰工程有限公司 | A kind of modified optimization environment-friendly preparation method of publicity brochure paper |
CN109468891A (en) * | 2018-11-22 | 2019-03-15 | 山东如意科技集团有限公司 | A kind of waste fabric fiberboard and its manufacturing method |
CN109853289A (en) * | 2019-03-15 | 2019-06-07 | 浙江科技学院 | A kind of fire-retardant paper base material and preparation method thereof using the preparation of reaction-type flame-retarding fiber |
CN109853289B (en) * | 2019-03-15 | 2021-04-13 | 浙江科技学院 | Flame-retardant paper-based material prepared from reactive flame-retardant fibers and preparation method thereof |
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Publication number | Publication date |
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CN106113214B (en) | 2018-06-26 |
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Address after: 456400 south section of Huaxian civilization Road, Anyang, Henan Patentee after: Henan Watson Ultrasonic Technology Co.,Ltd. Address before: 456400 south section of Huaxian civilization Road, Anyang, Henan Patentee before: ANYANG HUASEN PAPER CO.,LTD. |
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Effective date of registration: 20200113 Address after: 456400 Intersection of Civilization Road and Huazhou Road at Huaxian Road Crossing, Anyang City, Henan Province Patentee after: Henan Jinshan Yinshan Biomass Technology Co.,Ltd. Address before: 456400 south section of Huaxian civilization Road, Anyang, Henan Patentee before: Henan Watson Ultrasonic Technology Co.,Ltd. |
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Effective date of registration: 20200408 Address after: 341300 guantian Industrial Park, guantian Town, Chongyi County, Ganzhou City, Jiangxi Province Patentee after: Jiangxi Zhongzhu Biomass Technology Co.,Ltd. Address before: 456400 Intersection of Civilization Road and Huazhou Road at Huaxian Road Crossing, Anyang City, Henan Province Patentee before: Henan Jinshan Yinshan Biomass Technology Co.,Ltd. |
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Granted publication date: 20180626 |