CN106087558A - A kind of diatom soil type sizing composition for improving press quality and application thereof - Google Patents

A kind of diatom soil type sizing composition for improving press quality and application thereof Download PDF

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Publication number
CN106087558A
CN106087558A CN201610447893.3A CN201610447893A CN106087558A CN 106087558 A CN106087558 A CN 106087558A CN 201610447893 A CN201610447893 A CN 201610447893A CN 106087558 A CN106087558 A CN 106087558A
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Prior art keywords
starch
white color
color system
printing paper
weight portions
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CN201610447893.3A
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CN106087558B (en
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文起东
崔俊峰
文博
邹晓虎
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INNER MONGOLIA DONGSHENG DIATOMITE TECHNOLOGY INNOVATION INDUSTRIAL PARK CO., LTD.
Original Assignee
Beijing Dongtai Fubo New Material Science & Technology Co Ltd
Inner Mongolia Dongsheng Diatomite Technology Innovation Industrial Park Co Ltd
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Classifications

    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/16—Sizing or water-repelling agents
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/36—Coatings with pigments
    • D21H19/38—Coatings with pigments characterised by the pigments
    • D21H19/40—Coatings with pigments characterised by the pigments siliceous, e.g. clays
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/36—Coatings with pigments
    • D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
    • D21H19/54—Starch
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00—Coated paper; Coating material
    • D21H19/36—Coatings with pigments
    • D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
    • D21H19/64—Inorganic compounds
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/06—Paper forming aids
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/28—Colorants ; Pigments or opacifying agents

Abstract

The present invention relates to a kind of diatom soil type compositions for improving press quality and application thereof.Described compositions comprises: starch；Calcium chloride；Chelating agent；White color system dyestuff；Kieselguhr；Bentonite；And Muscovitum.The invention still further relates to a kind of method manufacturing printing paper, described method uses described compositions that printing paper is carried out top sizing.The invention still further relates to the application in printing paper manufactures of the described compositions.The whiteness of the printing paper that compositions of the present invention uses kieselguhr, the combination of bentonite and Muscovitum suppresses to use calcium chloride starch type sizing agent to prepare effectively and brightness, improve ratio of printing ink transfer simultaneously.

Description

A kind of diatom soil type sizing composition for improving press quality and application thereof
Technical field
The present invention relates to field of papermaking.Specifically, the present invention relates to emulsifying agent compositions and in papermaking Application.
Background technology
Starch is usually utilized to the key component of the sizing agent as printing paper, but relative to comprising other key components Sizing agent for, the ratio of printing ink transfer relative deficiency of starch type sizing agent.In printing practical operation, the normal transfer of ink It it is the condition determining Color Printing quality.The principal element affecting ink transfer quality is considered mainly have ink-water balance, print Brush speed, squeegee pressure, printing color-sequential etc..Therefore in terms of the research about ratio of printing ink transfer focuses primarily upon these.
It addition, be the printing characteristic such as ink density and drying time improving printing paper, a lot of papermaking producers are all making Paper gluing agents adds cationic metal.Wherein, calcium chloride is frequently utilized for improving printing density and drying time.But, Finding that calcium chloride can reduce brightness and the whiteness of paper, such as calcium chloride can make stilbene radicals optics white color system dyestuff cancellation, thus drop The brightness of low paper and whiteness.Particularly calcium chloride can affect the pH of sizing agent, thus causes the use of the starch in sizing agent, This is because too high pH can make starch turn yellow, too low pH can make starch separate out.Once calcium chloride have impact on pH, will affect To the use of starch starch in sizing agent, eventually affect brightness and the whiteness of printing paper.
But, the inventors discovered that, by improving the surface of printing paper in particular for printing body paper is carried out applying glue The composition of the composition of sizing agent, especially calcium chloride-starch type sizing agent, specifically adds kieselguhr in this sizing agent With other components such as component such as bentonite and/or bentonite, it is possible to significantly improve the whiteness of printing paper and measure and ink The rate of transform.
Then, the invention provides one especially to carry in the case of keeping whiteness and brightness for improving press quality The diatom soil type sizing composition of high ratio of printing ink transfer and application thereof.
Summary of the invention
Entering for solving one or more the problems referred to above that calcium chloride-starch type sizing agent exists at glue used in paper-making In the test of row, inventors have surprisingly found that adding the compositions such as kieselguhr in calcium chloride-starch type sizing agent can solve the problem that The problems referred to above existing for calcium chloride-starch type sizing agent, thus improve optical characteristics such as whiteness and the brightness of printing paper again Improve ratio of printing ink transfer simultaneously.
The present invention provides a kind of based on diatomaceous Cypres compositions, described compositions bag in first aspect Contain: starch；Calcium chloride；Chelating agent；White color system dyestuff；Kieselguhr；Bentonite and Muscovitum.
The present invention provides a kind of method manufacturing printing paper in second aspect, and wherein, described method uses the present invention the Compositions described in Yi Fangmian carries out top sizing to printing paper.
The present invention provides the application in printing paper manufactures of the compositions described in first aspect present invention in the third aspect.
Detailed description of the invention
The present invention provides a kind of based on diatomaceous Cypres compositions in first aspect, and described compositions comprises Or it is made up of following component: starch；Calcium chloride；Chelating agent；White color system dyestuff；Kieselguhr；Bentonite；And Muscovitum.
The type of described starch is not particularly limited by the present invention.Described starch can be unmodified starch can also be to change Property starch.It is preferred that modified starch；It may further be preferable that described modified starch choosing free oxidation modification starch, sun The group of ion modification starch, ethylization modified starch, hydrogen ethoxylation modified starch composition.Also it is preferred that described starch For natural origin starch；It is further preferred that described natural origin starch selects free corn starch, tapioca and potato starch The group of composition.Most preferably potato starch.Described starch can be prepared by known technology preparation, it is also possible to from passing through business Available from, such as can be from Gansu Chao Xing starch-based product company limited or port, Heilungkiang feed product Science and Technology Development Co., Ltd. business Available from.
Described chelating agent is had no particular limits by the present invention, as long as this chelating agent can have affinity i.e. to calcium ion Can.In some have the embodiment of choosing, described chelating agent is cellulose；It is further preferred that described chelating agent selects free hydroxyl first Base cellulose, hydroxy ethyl fiber and the group of hydroxypropyl cellulose composition；Most preferably, described chelating agent is hydroxy propyl cellulose Element.
There is no particular limitation to described white color system dyestuff for the present invention, and the most described white color system dyestuff selects free furan type white Colour system dyestuff, coumarin type white color system dyestuff, biphenyl type white color system dyestuff and the group of pyrazoles type white color system dyestuff composition.White color system Dyestuff can be such as commercially available from sources such as Dongguan City Ke Feng textile auxiliary Industrial Co., Ltd.s.
The present invention employs kieselguhr in the composition.Kieselguhr is a kind of biogenic silicastone, is In ocean or lake, the remains of the Diatomeae of growth are at subaqueous deposit, and the one gradually formed through natural environment effect is nonmetal Mineral.Kieselguhr is mainly distributed on the states such as China, the U.S., Denmark, France, Romania.It is a kind of biogenic siliceous heavy Long-pending rock, it is mainly made up of the remains of diatom in ancient times.China's kieselguhr reserves 3.2 hundred million tons, prospective reserves reaches more than 20 hundred million tons, main East China to be concentrated on and the Northeast, larger, what reserves were more have Jilin (54.8%), Zhejiang, Yunnan, Shandong, Sichuan etc. save.
Kieselguhr has the advantage that.(1) pH value is neutral, nontoxic, and suspendability is good, and absorption property is strong, and unit weight is light, mixing Uniformity is good；(2) kieselguhr makees additive in cement, can improve intensity, makes SiO in cement2Become activity；(3) kieselguhr tool There is excellent extensibility, have higher impact strength, hot strength, tearing strength, the soft wearability of light weight is good, comprcssive strength is good Aspect high-quality effect.
The present inventor is found through experiments, and kieselguhr and bentonitic combination can reduce calcium chloride to the pH's of sizing agent Impact, the starch its colour changed into yellow in suppression sizing agent, thus improve whiteness and the brightness of printing paper.If adding appropriate cloud again Female, additionally it is possible to improve ratio of printing ink transfer.Being not intended to be bound by theory, the present inventor speculates kieselguhr or kieselguhr Combination with bentonitic combination and kieselguhr, bentonite and Muscovitum can fetter some ion, such as H+ ion or OH Ion or discharge some antiparticle such that it is able to play the effect of stable pH；It addition, kieselguhr or kieselguhr, bentonite Combination with Muscovitum may improve the affinity to ink on printing paper surface, thus improves ratio of printing ink transfer.It addition, diatom The combination of soil or kieselguhr, bentonite and Muscovitum may be with other compositions of sizing agent such as calcium chloride, chelating agent, white color system Dyestuff or starch interact, thus bring above-mentioned favourable effect.
Whiteness of the present invention represents with CIE whiteness, and its measuring method is known, for example, see United States Patent (USP) 6, 893,473.Brightness of the present invention represents with ISO brightness, and its metering system is known, for example, see United States Patent (USP) 6, 893,473.These patent documentations are the most completely expressly incorporated herein.Ratio of printing ink transfer represents with IT%, and it is roll-in The amount of rear shifted optical density；It is expressed as the percentage by the optical density transferring to the non-printing of this printing paper after roll-in Number.Measure the method for ratio of printing ink transfer to be included on paper and print solid color lump, after waiting the time (5 seconds) of ormal weight, Doubling printing paper, so that the part of printing contacts with non-printing, and with 4.5 pounds of hands rollers (such as from Chem The roller of the article No. HR-100 of Instruments, Inc., Mentor, OH, USA) roll-in.By reflection densitometer (X-Rite, Macbeth.Etc.) facing to the transfer (OD of color lumpT), non-diverting (ODO) part and unimaged region (ODB) read optical density.Turn The percent (" IT " %) moved is calculated by equation below: IT%=[(ODT–ODB)/(ODO–ODB)]×100。
In the present invention, the particle diameter of kieselguhr, bentonite and Muscovitum is unsuitable excessive, the above-mentioned advantageous effects otherwise brought May weaken.Described kieselguhr and bentonitic particle diameter preferably no more than 100 microns, preferably no greater than 50 microns.? Some preferred embodiment in, their particle diameter is preferably 10 to 20 microns；For example, 10,11,12,13,14,15,16, 17,18,19 or 20 microns.
Some preferred embodiment in, the described compositions of the present invention comprises the starch of 100 weight portions；20 to 30 weights The calcium chloride (calcium chloride of for example, 20,21,22,23,24,25,26,27,28,29 or 30 weight portions) of amount part；2 to 4 weight The chelating agent (chelating agent of such as 2,3 or 4 weight portions) of part；The white color system dyestuff of 20 to 30 weight portions (such as 20,21,22, 23, the white color system dyestuff of 24,25,26,27,28,29 or 30 weight portions)；The kieselguhr of 5 to 15 weight portions (such as 5,6,7,8, 9, the kieselguhr of 10,11,12,13,14 or 15 weight portions；Bentonite (the swelling of such as 1,2 or 3 weight portions of 1 to 3 weight portion Soil)；Muscovitum (Muscovitums of such as 4,5,6,7 or 8 weight portions) with 4 to 8 weight portions.
The present invention provides a kind of method manufacturing printing paper in second aspect, and wherein, described method uses the present invention the Compositions described in Yi Fangmian carries out top sizing to printing paper.
In one preferred embodiment, the amount of the described sizing agent being applied on printing paper is at least 0.25gsm, excellent Select 0.25 to 10gsm, more preferably 3.5 to 10gsm, most preferably 4.0 to 10gsm, including anyon scope therein.
In one embodiment, described sizing composition prepares containing 10 to 50% as with water.For example, 10, 11, the solid content of 12,13,14,15,16,17,18,19,20,21,22,23,24,25,30,35,40,45 and 50 weight % Slurry uses.
The present invention provides the answering in printing paper manufactures of the compositions described in first aspect present invention in the third aspect With.
Hereafter by embodiment, the present invention will be further described, but these embodiments be not necessarily to be construed as right The restriction of protection scope of the present invention.
Embodiment
(starch is potato starch, and is 100 weight to prepare sizing composition according to the formula described in table 1 Part), and sizing composition distilled water is prepared as the slurry that solid content is 20, then uses from granary benefit machine forever The two-sided applying glue of amount with 4.0gsm of the X99 type sizing applicator is buied in from Nanning Lang Baisite Paper Co., Ltd by tool equipment company limited Commercially available grammes per square metre is the printing body paper of 14g.And measure the CIE whiteness of printing paper after applying glue and ISO brightness and ink transfer Rate, each experiment is repeated 5 times, and calculates meansigma methods.White color system dyestuff in embodiment is 5-furyl-1,3-diphenylpypazole Quinoline, chelating agent is hydroxypropyl cellulose, and the particle diameter of kieselguhr, bentonite and Muscovitum is no more than 20 microns.
Table 1 contains kieselguhr and the formula of bentonitic various sizing composition and on whiteness and the impact of brightness
Embodiment Calcium chloride Chelating agent White color system dyestuff Kieselguhr Bentonite CIE whiteness ISO brightness
1 30 4 30 0 2 86.2 145.1
2 30 4 30 2 2 87.3 147.6
3 30 4 30 5 2 91.2 151.4
4 30 4 30 10 2 92.8 152.3
5 30 4 30 15 2 93.4 153.6
6 30 4 30 20 2 93.1 153.7
7 30 4 30 10 0 89.8 148.7
8 30 4 30 10 0.5 90.1 148.9
9 30 4 30 10 1.0 92.1 151.2
10 30 4 30 10 3 93.0 152.4
11 30 4 30 10 5 93.1 152.6
12 0 4 30 10 2 94.1 152.3
13 20 4 30 10 2 93.3 152.7
14 30 0 30 10 2 91.4 152.4
15 30 2 30 10 2 92.4 152.1
16 30 4 0 10 2 76.4 118.0
17 30 4 20 10 2 92.5 152.4
18 30 4 30 0 0 86.0 144.8
From the results shown in Table 1, kieselguhr especially kieselguhr and bentonitic combination inhibit calcium chloride dialogue Degree and the impact of brightness.
Table 2 contains the formula of the various sizing compositions of kieselguhr, bentonite and Muscovitum and to ratio of printing ink transfer Impact
Embodiment Calcium chloride Chelating agent White color system dyestuff Kieselguhr Bentonite Muscovitum CIE whiteness ISO brightness IT%
19 30 4 30 10 2 0 92.8 152.3 25.3
20 30 4 30 10 2 2 92.9 152.1 20.4
21 30 4 30 10 2 4 92.4 151.9 18.6
22 30 4 30 10 2 6 92.1 151.7 17.6
23 30 4 30 10 2 8 91.0 150.4 17.1
24 30 4 30 10 2 10 88.7 Do not detect 16.9
From the results shown in Table 2, after adding appropriate Muscovitum, can be in the CIE whiteness and and 150 keeping more than 90 The ratio of printing ink transfer of printing paper is improved in the case of above ISO brightness.

Claims (9)

1. the method manufacturing printing paper, wherein, described method uses following compositions that printing paper carries out top sizing, institute State compositions to comprise:
The starch of 100 weight portions；
The calcium chloride of 20 to 30 weight portions；
The chelating agent of 2 to 4 weight portions；
The white color system dyestuff of 20 to 30 weight portions；
The kieselguhr of 5 to 15 weight portions；
The bentonite of 1 to 3 weight portion；
Muscovitum with 4 to 8 weight portions；Wherein,
Described diatomaceous particle diameter is 10 microns to 20 microns, the particle diameter of described bentonite and described Muscovitum be 10 microns micro-to 20 Rice；
Wherein, the amount of the compositions being applied on printing paper is 4.0-10gsm.
Method the most according to claim 1, wherein said starch is modified starch.
Method the most according to claim 2, the choosing of wherein said modified starch free oxidation modification starch, cation-modified shallow lake The group of powder, ethylization modified starch, hydrogen ethoxylation modified starch composition.
Method the most according to claim 1, wherein said starch is natural origin starch.
Method the most according to any one of claim 1 to 4, the wherein said natural origin starch free corn starch of choosing, Tapioca and the group of potato starch composition.
Method the most according to any one of claim 1 to 5, wherein said chelating agent is cellulose.
Method the most according to any one of claim 1 to 6, wherein said chelating agent choosing free hydroxymethyl cellulose, hydroxyl Ethyl cellulose and the group of hydroxypropyl cellulose composition.
Method the most according to claim 6, wherein said chelating agent is hydroxypropyl cellulose.
Method the most according to claim 1, wherein said white color system dyestuff choosing free furan type white color system dyestuff, coumarin Type white color system dyestuff, biphenyl type white color system dyestuff and the group of pyrazoles type white color system dyestuff composition.
CN201610447893.3A 2015-09-18 2015-09-18 A kind of diatom soil type sizing composition and its application for being used to improve press quality Active CN106087558B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101595261A (en) * 2006-12-11 2009-12-02 国际纸业公司 Paper glueing composition, sized paper and the method for paper being carried out applying glue
CN101864700A (en) * 2010-06-03 2010-10-20 中国制浆造纸研究院 Surface treatment method for light paper
CN103993509A (en) * 2014-04-25 2014-08-20 蚌埠德美过滤技术有限公司 Stable-quality zirconia-supported air filter paper for automobiles, and making method thereof
CN104119700A (en) * 2014-07-08 2014-10-29 东北林业大学 Preparation method of ultrasonic-assisted starch/rosin clathrate-based modified filler
WO2015110979A1 (en) * 2014-01-22 2015-07-30 Stora Enso Oyj Method of decreasing the dusting tendency of printing paper

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0908401D0 (en) * 2009-05-15 2009-06-24 Imerys Minerals Ltd Paper filler composition
US9174479B2 (en) * 2010-09-29 2015-11-03 Mitsubishi Paper Mills Limited Coated printing paper and method for forming printed images

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101595261A (en) * 2006-12-11 2009-12-02 国际纸业公司 Paper glueing composition, sized paper and the method for paper being carried out applying glue
CN101864700A (en) * 2010-06-03 2010-10-20 中国制浆造纸研究院 Surface treatment method for light paper
WO2015110979A1 (en) * 2014-01-22 2015-07-30 Stora Enso Oyj Method of decreasing the dusting tendency of printing paper
CN103993509A (en) * 2014-04-25 2014-08-20 蚌埠德美过滤技术有限公司 Stable-quality zirconia-supported air filter paper for automobiles, and making method thereof
CN104119700A (en) * 2014-07-08 2014-10-29 东北林业大学 Preparation method of ultrasonic-assisted starch/rosin clathrate-based modified filler

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Effective date of registration: 20191101

Address after: 013450, the Inner Mongolia Autonomous Region City, Wulanchabu County Industrial Park, county magistrate

Patentee after: INNER MONGOLIA DONGSHENG DIATOMITE TECHNOLOGY INNOVATION INDUSTRIAL PARK CO., LTD.

Address before: 013450, the Inner Mongolia Autonomous Region City, Wulanchabu County Industrial Park, county magistrate

Co-patentee before: BEIJING DONGTAI FUBO NEW MATERIAL SCIENCE & TECHNOLOGY CO., LTD.

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