CN106087412A - A kind of submissive method of manual grass cloth - Google Patents

A kind of submissive method of manual grass cloth Download PDF

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Publication number
CN106087412A
CN106087412A CN201610426267.6A CN201610426267A CN106087412A CN 106087412 A CN106087412 A CN 106087412A CN 201610426267 A CN201610426267 A CN 201610426267A CN 106087412 A CN106087412 A CN 106087412A
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China
Prior art keywords
grass cloth
submissive
manual
test solution
softener
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Pending
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CN201610426267.6A
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Chinese (zh)
Inventor
田合伟
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Lingnan Normal University
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Lingnan Normal University
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Priority to CN201610426267.6A priority Critical patent/CN106087412A/en
Publication of CN106087412A publication Critical patent/CN106087412A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/04—Vegetal fibres
    • D06M2101/06—Vegetal fibres cellulosic

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention belongs to fabric-handling techniques field, disclose a kind of submissive method of manual grass cloth, it is that test solution is soaked in preparation, described immersion test solution is made up of ester based quaternary ammonium salt and fatty alcohol-polyoxyethylene ether, dries 20min after craft grass cloth is placed in described immersion test solution the taking-up of immersion a period of time at 118 DEG C.The softener of present invention selection and penetrating agent can reduce the combination of self hydrophilic group or hydrophobic group, make softener play bigger submissive effect, and the bending rigidity of the manual clean sample of grass cloth is 2.92 cN cm‑1, the sample compliance through the submissive arrangement of this method is all remarkably reinforced.The anti-firm camber of normal domestic use textile requires at 0.6 cN cm‑1～1.2 cN cm‑1Between, manual grass cloth, through submissive arrangement, can be applied in home textile and garment industry.

Description

A kind of submissive method of manual grass cloth
Technical field
The present invention relates to fabric-handling techniques field, more particularly, to a kind of submissive method of manual grass cloth.
Background technology
Manual grass cloth is a kind of traditional weaving process fabric of China, the most history in thousand.Grass cloth processing technology is Through being put into country's non-material cultural heritage register, but manual grass cloth has the shortcoming that feel is stiffening, so its range It is restricted.For expanding the application in home textile kimonos dress field of the manual grass cloth, need badly and manual grass cloth is carried out submissive arrangement.
Summary of the invention
The technical problem to be solved is the drawbacks described above overcoming prior art to exist, it is provided that a kind of manual grass cloth Submissive method.
It is an object of the invention to be achieved by the following technical programs:
A kind of submissive method of manual grass cloth, is that test solution is soaked in preparation, and described immersion test solution is by ester based quaternary ammonium salt and poly alkyl alcohol Oxygen vinyl Ether forms, and dries after craft grass cloth is placed in described immersion test solution the taking-up of immersion a period of time at 118 DEG C 20min。
The primary raw material of grass cloth is Boehmeria, and Boehmeria is a kind of fibre crops, although having multiple for difference in prior art The softener of fabric, but not for the softener of grass cloth, further, since the particularity of grass cloth raw material, select to be suitable for the summer The softener of cloth, here after screening, ester based quaternary ammonium salt is minimum as the anti-stiffness of grass cloth after softener, be best suitable for for The submissive process of grass cloth, it addition, according to the kind of softener, screening obtains suitable penetrating agent fatty alcohol-polyoxyethylene ether again.
Through orthogonal test and experiment of single factor, result shows, during submissive, and softener ester based quaternary ammonium salt A, infiltration Agent fatty alcohol-polyoxyethylene ether B, soak time C, drying time D, dry the temperature E influence degree to manual grass cloth bending rigidity Difference, it affects size and is ordered as E ＞ D ＞ B ＞ A ＞ C.
Preferably, in described immersion test solution, the concentration of ester based quaternary ammonium salt is 20 g L-1.Fatty alcohol-polyoxyethylene ether dense Degree is 2.2 g L-1.Manual grass cloth soak time in soaking test solution is 22min.
Compared with prior art, the method have the advantages that
The invention provides a kind of submissive method of manual grass cloth, be that test solution is soaked in preparation, described immersion test solution is by ester group quaternary ammonium Salt and fatty alcohol-polyoxyethylene ether composition, craft grass cloth is placed in described immersion test solution immersion a period of time taking-up after 118 20min is dried at DEG C.The softener of present invention selection and penetrating agent can reduce the combination of self hydrophilic group or hydrophobic group, make soft Playing bigger submissive effect along agent, the bending rigidity of the manual clean sample of grass cloth is 2.92 cN cm-1, submissive through this method The sample compliance arranged all is remarkably reinforced.The anti-firm camber of normal domestic use textile requires at 0.6 cN cm-1～1.2 cN·cm-1Between, manual grass cloth, through submissive arrangement, can be applied in home textile and garment industry.
Accompanying drawing explanation
Fig. 1 is the impact on the manual submissive effect of grass cloth of the softener concentration.
Fig. 2 is the osmotic agent concentration impact on the manual submissive effect of grass cloth.
Fig. 3 is the soak time impact on the manual submissive effect of grass cloth.
Fig. 4 is the drying time impact on the manual submissive effect of grass cloth.
Fig. 5 is the impact drying temperature to the manual submissive effect of grass cloth.
Detailed description of the invention
Further illustrate present disclosure below in conjunction with Figure of description and specific embodiment, but should not be construed as right The restriction of the present invention.In the case of present invention spirit and essence, the amendment that the inventive method, step, condition are made Or replace, belong to the scope of the present invention.Unless otherwise noted, experimental technique used in embodiment is people in the art Conventional method known to Yuan and technology, reagent or material are and are obtained by commercial sources.
Test select Longchang craft grass cloth as sample, size of sample a size of 250mm*25mm, materialsed and can not be had Affecting the fault of result of the test, sample quantities is 12 pieces, and the grass cloth that fabric width is 60cm chosen by sample, and chooses sample at least from cloth Limit 10cm, avoids limbs too much to contact sample as far as possible, sample exposes natural damping in an atmosphere simultaneously and is not less than 24h.
Instrument use LFY-207 automatic fabric stiffness test instrument, DHG-9420 type electric heating constant-temperature blowing drying box, FA2004 type electronic balance, additionally, prepare a water-bath, a shears, a rule, a flatiron, 5 kg Weight, the glass plate of two pieces of a size of 60 mm*120 mm * 2mm.
Embodiment 1
DHTDMAC, diamides based quaternary ammonium salt, imidazolines quaternary ammonium salt, several softener of ester based quaternary ammonium salt has been selected to carry out submissive Processing, its result shows: compared with DHTDMAC, diamides based quaternary ammonium salt, imidazolines quaternary ammonium salt, after ester based quaternary ammonium salt processes Sample all there is in terms of antistatic behaviour, wettability, yellowing resistance and biological degradability clear superiority, it is considered to fabric process After wearability and environmental friendliness performance, test finally determine ester based quaternary ammonium salt be test softener.
Embodiment 2
Reagent selects ester based quaternary ammonium salt softener and fatty alcohol-polyoxyethylene ether penetrating agent (JFC).
One, soft finish orthogonal test
By document analysis, according to limiting factors such as Instrument specifications, determine softener ester based quaternary ammonium salt concentration, penetrating agent fatty alcohol Polyoxyethylene ether concentration, soak time, drying time and the scope of drying temperature.It is orthogonal test water-glass as shown in table 1, L is carried out on the basis of this9(35) orthogonal test, result of the test is as shown in table 2.
As shown in Table 2, No. 5 result of the tests are ideal, and No. 8 result of the tests are taken second place.Single influence factor is tested, Obtaining each level corresponding bending rigidity average, result of the test is as shown in table 3.
Each column in table 3 being affected the single bending rigidity of level and carries out average ratio relatively, average the least expression result of the test is more Preferable.From data in table, in first row data, the average of level 2 is minimum, is designated as A2, in secondary series data, level 3 is equal Value minimum, is designated as B3, in the 3rd column data, the average of level 2 is minimum, is designated as C2, in the 4th column data, the average of level 2 is minimum, It is designated as D2, in the 5th column data, the average of level 3 is minimum, is designated as E3。
According to the bending rigidity of each level, the best level of single influence factor is combined, then draws A2B3C2D2E3, namely softener ester based quaternary ammonium salt concentration 20 g L-1, penetrating agent fatty alcohol-polyoxyethylene ether concentration 2 g L-1, soak time 20 min, drying time 20 min, drying temperature 110 DEG C may be best testing program.Divide according to extreme difference Analysis result understands, softener ester based quaternary ammonium salt A, penetrating agent fatty alcohol-polyoxyethylene ether B, soak time C, and drying time D is dried Temperature E is different to the influence degree of manual grass cloth bending rigidity, and it affects size and is ordered as E ＞ D ＞ B ＞ A ＞ C.
Two, factor of influence single factor experiment
In order to determine optimal testing program, in the range of orthogonal test water-glass limits, all levels are carried out single factor test examination Test.
(1) impact of test solution concentration
Softener ester based quaternary ammonium salt is carried out single factor experiment, and experimental condition is defined as 0 g L-1、12 g·L-1、16 g·L-1、20 g·L-1、22 g·L-1、24 g·L-1With 26 g L-1, penetrating agent fatty alcohol-polyoxyethylene ether concentration 2 g L-1, leaching Bubble time 25 min, drying time 20 min, dry temperature 110 DEG C, and result of the test is as shown in Figure 1.
Experiment ester based quaternary ammonium salt softener is the high concentration test solution passing through process, can the appropriate distilled water of direct matching Use.Process through softener, make the lubricating oil film of fabric face be affected, change the anti-firm camber of fabric, make fabric become Obtain soft.As shown in Figure 1, it is 20 g L in softener concentration-1Time, the bending rigidity of manual grass cloth is minimum, and i.e. pliability is High.When softener test solution concentration is higher than 20 g L-1Time, the compliance of manual grass cloth reduces on the contrary, and this is due to high concentration test solution The hydrophobic group of middle test solution is each connected with hydrophilic group, is unfavorable for the lubricating oil film reaction with fabric face, therefore 20 g L-1It is The optimal softener test solution concentration of this test.
Penetrating agent fatty alcohol-polyoxyethylene ether is carried out single factor experiment, and experimental condition is defined as 0 g L-1、1.4 g· L-1、1.8 g·L-1、2.0 g·L-1、2.4 g·L-1、2.6 g·L-1, softener ester based quaternary ammonium salt concentration 20 g L-1, leaching Bubble time 25 min, drying time 20 min, dry temperature 110 DEG C, and result of the test is as shown in Figure 2.
Due to ester based quaternary ammonium salt temperature limiting in quaternization process, process of the test uses the test temperature of gentleness, So also being able to keep the physics color and luster of manual grass cloth, penetrating agent can also play the surface reducing softener in submissive arrangement The effect of tension force.As shown in Figure 2, along with the increase of penetrating agent test solution concentration, the anti-firm camber of manual grass cloth is gradually reduced, and this is Because penetrating agent penetrates into and spreads at fabric fiber, softener is enable preferably to adsorb with fabric and fully to react, but It is when osmotic agent concentration is more than 2.2 g L-1Time, the anti-firm camber of manual grass cloth increased, and illustrates that penetrating agent is soft when 2.2 Tending to saturated along agent in the absorption of fabric face, the most optimal penetrating agent test solution concentration is 2.2 g L-1。
(2) soak time and the drying time impact on flexibility
Soak time is carried out single factor experiment, and experimental condition is ester based quaternary ammonium salt softener concentration 20 g L-1, penetrating agent fat Fat polyoxyethylenated alcohol concentration 2.2 g L-1, soak time be set as 14min, 16 min, 18 min, 20 min, 22 min, 24 min, 26 min, drying time is defined as 20min, and drying temperature is 110 DEG C, and result of the test is as shown in Figure 3.Can by Fig. 3 Knowing, optimal soak time is 22min, and when soaking 22min, the bending rigidity of craft grass cloth is minimum.
Drying time is carried out single factor experiment, and experimental condition is ester based quaternary ammonium salt softener concentration 20 g L-1, infiltration Agent fatty alcohol-polyoxyethylene ether concentration 2.2 g L-1, soak time be set as 22min, drying time be respectively 14 min, 16 Min, 18 min, 20 min, 22 min, 24 min, 26 min, drying temperature is 110 DEG C, and result of the test is as shown in Figure 4.By scheming Optimal drying time knowable to 4 is 20min, when drying time extends, does not reduce the anti-firm camber of manual grass cloth, on the contrary Feel is made to show slightly stiffening.
(3) temperature impact on flexibility is dried
Carrying out single factor experiment to drying temperature, experimental condition is ester based quaternary ammonium salt softener concentration 20 g L-1, penetrating agent fat Fat polyoxyethylenated alcohol concentration 2.2 g L-1, soak time is set as that 22min, drying time are respectively 20min, dries temperature Being 98 DEG C, 102 DEG C, 106 DEG C, 110 DEG C, 114 DEG C, 118 DEG C, 122 DEG C, result of the test is as shown in Figure 5.As seen from Figure 5, dry Before dry temperature is increased to 118 DEG C, the anti-firm camber change of manual grass cloth is little, when drying temperature is 118 DEG C, manual grass cloth Submissive best results.

Claims (4)

1. the submissive method of a manual grass cloth, it is characterised in that test solution is soaked in preparation, and described immersion test solution is by ester based quaternary ammonium salt With fatty alcohol-polyoxyethylene ether form, craft grass cloth is placed in described immersion test solution immersion a period of time taking-up after at 118 DEG C Lower drying 20min.
The submissive method of manual grass cloth the most according to claim 1, it is characterised in that ester group season in described immersion test solution The concentration of ammonium salt is 20 g L-1。
The submissive method of manual grass cloth the most according to claim 1, it is characterised in that fatty alcohol in described immersion test solution The concentration of polyoxyethylene ether is 2.2 g L-1。
The submissive method of manual grass cloth the most according to claim 1, it is characterised in that manual grass cloth is in soaking test solution Soak time is 22min.
CN201610426267.6A 2016-06-16 2016-06-16 A kind of submissive method of manual grass cloth Pending CN106087412A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106913000A (en) * 2017-05-10 2017-07-04 四川兴奥邦服饰有限公司 A kind of processing method of novel crease-resistant suit
CN110205793A (en) * 2019-04-30 2019-09-06 岭南师范学院 A kind of Clothing Specialty student cloth fixed-length cutting device

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101581037A (en) * 2009-06-09 2009-11-18 深圳市成为工贸有限公司 Particles capable of softening clothes and preparation method thereof
CN103834489A (en) * 2014-02-26 2014-06-04 南通优尼科化工有限公司 Ester quaternary ammonium salt laundry detergent
CN104060471A (en) * 2014-06-19 2014-09-24 宁波市川宁环保科技有限公司 Softener composition and application of composition
CN105484038A (en) * 2015-12-16 2016-04-13 常熟市华威服饰厂 Composite fabric dyeing and finishing process

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101581037A (en) * 2009-06-09 2009-11-18 深圳市成为工贸有限公司 Particles capable of softening clothes and preparation method thereof
CN103834489A (en) * 2014-02-26 2014-06-04 南通优尼科化工有限公司 Ester quaternary ammonium salt laundry detergent
CN104060471A (en) * 2014-06-19 2014-09-24 宁波市川宁环保科技有限公司 Softener composition and application of composition
CN105484038A (en) * 2015-12-16 2016-04-13 常熟市华威服饰厂 Composite fabric dyeing and finishing process

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106913000A (en) * 2017-05-10 2017-07-04 四川兴奥邦服饰有限公司 A kind of processing method of novel crease-resistant suit
CN110205793A (en) * 2019-04-30 2019-09-06 岭南师范学院 A kind of Clothing Specialty student cloth fixed-length cutting device
CN110205793B (en) * 2019-04-30 2024-01-05 岭南师范学院 Cloth fixed-length cutting device for clothing specialty students

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