CN1060867A - The production technique of natural refined jasmine oil and equipment - Google Patents
The production technique of natural refined jasmine oil and equipment Download PDFInfo
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- CN1060867A CN1060867A CN 90108638 CN90108638A CN1060867A CN 1060867 A CN1060867 A CN 1060867A CN 90108638 CN90108638 CN 90108638 CN 90108638 A CN90108638 A CN 90108638A CN 1060867 A CN1060867 A CN 1060867A
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Abstract
A kind of vapor phase process that adopts is directly told production technique and the equipment that extracts natural refined jasmine oil the fragrance of putting from Flower of Arabian Jasmine, this technology is simple, production safety, the jasmin quintessence oil productive rate reaches more than 2.5%, essential oil quality height has complete jasmin breath simultaneously, and fragrance is pure, natural jasmin sense is strong, is a kind of perfuming agent that is specially adapted on highclass perfumes and the food.
Description
The present invention relates to a kind of production technique and equipment that from Flower of Arabian Jasmine fragrance, directly extracts natural refined jasmine oil.
Natural jasmine fragrance only has two kinds of jasmine concrete and jasmine absolute, still there is not the jasmin quintessence oil product, all adopt sherwood oil lixiviate Flower of Arabian Jasmine to produce jasmine concrete at present both at home and abroad, contain the vegetable wax about 50%, the impurity of pollen and protein and so on, only as the usefulness of the perfuming of low-grade makeup, jasmine absolute is to be raw material with the jasmine concrete, with concentration is dissolve with ethanol more than 95%, freezing and filter, remove impurity, distillation recovery ethanol makes then, this method is complex process not only, and production security is poor, and solvent consumption is big, and do not meet that Flower of Arabian Jasmine is open to tell fragrant life process and condition, only utilized Flower of Arabian Jasmine partly to tell the aromatoising substance of fragrant process, the jasmine oil yield is low, the cost height.
At present, also have a kind ofly constantly to blow out fragrance in the Flower of Arabian Jasmine, use " the air blowing absorption method " of charcoal absorption to extract jasmin quintessence oil again, but also can't reach the industrial production requirement with damp atmosphere.
The purpose of this invention is to provide a kind of production technique and equipment that directly extracts natural refined jasmine oil from Flower of Arabian Jasmine fragrance, this method technology is simple, production safety, jasmin quintessence oil yield height.
Production technique of the present invention is that branch is told suction and two stages of desorb, telling pumping phases adopts by telling fragrant tower (5), heat exchanger (6), the tower (7) of enfleuraging, oxygen supply (8), variable valve (9), blower fan (1), preheater (2), the loop that differential pressure flow meter (3) and humidity regulator (4) are concatenated into and the process flow system of sealing and circulating, in closed system, form a continuous round-robin air-flow by blower fan (1), the Flower of Arabian Jasmine that this air-flow will be told in the fragrant tower (5) tells the aromatoising substance of emitting, by the tower of enfleuraging (7), being absorbed agent absorbs, aromatoising substance in Flower of Arabian Jasmine has been told, extract aromatoising substance in the absorption agent with extraction agent then, obtain jasmin quintessence oil through distillation again.
Open oxygen, moisture, temperature and the wind speed of telling in the fragrant process of Flower of Arabian Jasmine regulated and control realization by oxygen supply (8), heat exchanger (6), preheater (2), variable valve (9) and differential pressure flow meter (3).
The processing condition that the present invention adopts are as follows:
Temperature: 20～100 ℃ of humidity: 20～95%
Oxygen level: 5～80% wind speed: 0.01～1.5 meter per second
Flower layer thickness: 5～60 centimetres of extraction times: 4～48 hours
Absorption agent: can be liquid such as ethanol, benzene, acetone, chloroform, ether, sherwood oil, tetracol phenixin, grease, sweet oil; Also available solid such as gac, zeolite, diatomite, the most handy gac.
Extraction agent: the organic solvent of monobasic or binary, the preferably binary solvent of chloroform or chloroform and methyl alcohol.
Production technique of the present invention is used tells the cylindrical shell that fragrant tower (5) is an axial square or garden shape, have charging and discharging mouth and upper and lower breather line, its inside be provided with multilayer movable or fixed have the colored frame of sieve aperture, the used blower fan (1) of this technology is a high pressure positive blower.
Advantage of the present invention: technology is simple, production safety, and jasmin quintessence oil has complete jasmin breath, and fragrance is pure, and natural jasmin sense is strong, and the essential oil productive rate reaches more than 2.5 ‰, is a kind of perfuming agent that is specially adapted on highclass perfumes and the food.
Description of drawings:
Fig. 1 is the process flow sheet that the present invention tells pumping phases.Wherein (1) is blower fan; (2) be preheater; (3) be differential pressure flow meter; (4) be humidity regulator; (5) be to tell fragrant tower; (6) be heat exchanger; (7) be the tower of enfleuraging; (8) be oxygen supply; (9) be variable valve.
Embodiment 1: the Flower of Arabian Jasmine consumption is 30 kilograms, temperature is 30～80 ℃, humidity is 30～90%, and wind speed is 0.05～1.2 meter per second, and oxygen level is 10～70%, the flower layer thickness is 10～50 centimeters, extraction time is 8～36 hours, and absorption agent adopts grease, extraction agent ethanol, obtain jasmin quintessence oil 77.41 grams, the essential oil yield is 2.58 ‰.
Embodiment 2: the Flower of Arabian Jasmine consumption is 26.75 kilograms, temperature is 35～60 ℃, humidity is 70～85%, and wind speed is 0.1～0.3 meter per second, and oxygen level is 17～25%, the flower layer thickness is 10～25 centimetres, extraction time is 18～24 hours, and absorption agent adopts gac, the extraction agent binary solvent of chloroform and methyl alcohol, obtain jasmin quintessence oil 73.15 grams, the essential oil yield is 2.74 ‰.
Claims (6)
1, a kind of production technique and equipment that from Flower of Arabian Jasmine fragrance, directly extracts jasmin quintessence oil, divide to tell and inhale and two stages of desorb, it is characterized in that telling pumping phases adopts by telling fragrant tower, heat exchanger, the tower of enfleuraging, oxygen supply, variable valve, blower fan, preheater, the loop that differential pressure flow meter and humidity regulator are concatenated into and the process flow system of sealing and circulating, in closed system, form a continuous round-robin air-flow by blower fan, the Flower of Arabian Jasmine that this air-flow will be told in the fragrant tower tells the aromatoising substance of releasing, by the tower of enfleuraging, being absorbed agent absorbs, aromatoising substance in Flower of Arabian Jasmine has been told, extract aromatoising substance in the absorption agent with extraction agent then, obtain jasmin quintessence oil through distillation again, its processing condition are as follows: temperature is 20～100 ℃, humidity is 20～95%, wind speed is 0.01～1.5 meter per second, oxygen level is 5～80%, and the flower layer thickness is 5～60 centimetres, and extraction time is 4～48 hours.
2, production technique according to claim 1 is characterized in that telling in the desorption system by oxygen supply input pure oxygen.
3, production technique according to claim 1 and 2 is characterized in that absorption agent can adopt liquid or solid, as ethanol, benzene, acetone, chloroform, ether, sherwood oil, tetracol phenixin, grease, gac, zeolite, diatomite, preferably adopts gac.
4, production technique according to claim 3 is characterized in that extraction agent is the organic solvent of monobasic or binary, preferably the binary solvent of chloroform or chloroform and methyl alcohol.
5, the equipment of using according to the described production technique of claim 1 is characterized in that telling fragrant tower and is the cylindrical shell of an axial square or garden shape, has charging and discharging mouth and upper and lower breather line, inside be provided with multilayer movable or fixed have the colored frame of sieve aperture.
6, the equipment of using according to the described production technique of claim 1 is characterized in that used blower fan is a high pressure positive blower.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90108638 CN1060867A (en) | 1990-10-22 | 1990-10-22 | The production technique of natural refined jasmine oil and equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90108638 CN1060867A (en) | 1990-10-22 | 1990-10-22 | The production technique of natural refined jasmine oil and equipment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1060867A true CN1060867A (en) | 1992-05-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90108638 Pending CN1060867A (en) | 1990-10-22 | 1990-10-22 | The production technique of natural refined jasmine oil and equipment |
Country Status (1)
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| CN (1) | CN1060867A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100387698C (en) * | 2005-04-18 | 2008-05-14 | 宋开泉 | Extraction method of jasmine flower absolute oil |
| CN103262929A (en) * | 2013-05-21 | 2013-08-28 | 南宁市化工研究设计院 | Method for directly scenting scented tea by using fragrance adsorbent |
| CN103933827A (en) * | 2014-04-24 | 2014-07-23 | 福建农林大学 | Jasmine aroma adsorption device and adsorption method |
| CN103937613A (en) * | 2014-04-24 | 2014-07-23 | 福建农林大学 | Method for sub-critically extracting jasmine flower head fragrance essential oil |
| CN104431942A (en) * | 2014-11-11 | 2015-03-25 | 青岛信和源生物科技有限公司 | Spice preparation system |
| CN105441194A (en) * | 2015-12-03 | 2016-03-30 | 李嘉 | Purification method for jasmine essential oil |
| CN107460058A (en) * | 2017-09-04 | 2017-12-12 | 河南省明天食品有限公司 | A kind of extraction equipment and its extracting process of orange osmanthus flower essential oil |
| CN108130187A (en) * | 2017-11-24 | 2018-06-08 | 昆明理工大学 | A kind of device and process of cyclic absorption production face cream |
| CN108410619A (en) * | 2018-05-30 | 2018-08-17 | 新疆农业大学 | Rose champignon grape wine process equipment, rose champignon grape wine processing method and the grape wine of preparation |
| CN109207263A (en) * | 2018-10-19 | 2019-01-15 | 福建农林大学 | A method of makings flower essential oil is prepared by propylene glycol absorption method |
| CN109628224A (en) * | 2018-12-13 | 2019-04-16 | 福建农林大学 | Airflow circulating fat-based absorbs the method that Jasmine aromatic substance prepares face cream and fragrant dew |
-
1990
- 1990-10-22 CN CN 90108638 patent/CN1060867A/en active Pending
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100387698C (en) * | 2005-04-18 | 2008-05-14 | 宋开泉 | Extraction method of jasmine flower absolute oil |
| CN103262929A (en) * | 2013-05-21 | 2013-08-28 | 南宁市化工研究设计院 | Method for directly scenting scented tea by using fragrance adsorbent |
| CN103262929B (en) * | 2013-05-21 | 2016-04-20 | 南宁市化工研究设计院 | The method of the direct scenting tea of fragrance adsorbent |
| CN103937613A (en) * | 2014-04-24 | 2014-07-23 | 福建农林大学 | Method for sub-critically extracting jasmine flower head fragrance essential oil |
| CN103933827A (en) * | 2014-04-24 | 2014-07-23 | 福建农林大学 | Jasmine aroma adsorption device and adsorption method |
| CN104431942A (en) * | 2014-11-11 | 2015-03-25 | 青岛信和源生物科技有限公司 | Spice preparation system |
| CN105441194A (en) * | 2015-12-03 | 2016-03-30 | 李嘉 | Purification method for jasmine essential oil |
| CN107460058A (en) * | 2017-09-04 | 2017-12-12 | 河南省明天食品有限公司 | A kind of extraction equipment and its extracting process of orange osmanthus flower essential oil |
| CN108130187A (en) * | 2017-11-24 | 2018-06-08 | 昆明理工大学 | A kind of device and process of cyclic absorption production face cream |
| CN108130187B (en) * | 2017-11-24 | 2023-07-18 | 昆明理工大学 | Device and process for producing balsam by cyclic absorption |
| CN108410619A (en) * | 2018-05-30 | 2018-08-17 | 新疆农业大学 | Rose champignon grape wine process equipment, rose champignon grape wine processing method and the grape wine of preparation |
| CN109207263A (en) * | 2018-10-19 | 2019-01-15 | 福建农林大学 | A method of makings flower essential oil is prepared by propylene glycol absorption method |
| CN109207263B (en) * | 2018-10-19 | 2021-09-28 | 福建农林大学 | Method for preparing airiness flower essential oil by propylene glycol adsorption method |
| CN109628224A (en) * | 2018-12-13 | 2019-04-16 | 福建农林大学 | Airflow circulating fat-based absorbs the method that Jasmine aromatic substance prepares face cream and fragrant dew |
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