CN106047630A - Process for making solid particle healthy vinegar from Selaginella uncinata and Euryale ferox leaves - Google Patents
Process for making solid particle healthy vinegar from Selaginella uncinata and Euryale ferox leaves Download PDFInfo
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- CN106047630A CN106047630A CN201610400272.XA CN201610400272A CN106047630A CN 106047630 A CN106047630 A CN 106047630A CN 201610400272 A CN201610400272 A CN 201610400272A CN 106047630 A CN106047630 A CN 106047630A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
- C12J1/04—Vinegar; Preparation or purification thereof from alcohol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/06—Fungi, e.g. yeasts
- A61K36/07—Basidiomycota, e.g. Cryptococcus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/41—Crassulaceae (Stonecrop family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/54—Lauraceae (Laurel family), e.g. cinnamon or sassafras
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/57—Magnoliaceae (Magnolia family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/62—Nymphaeaceae (Water-lily family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/72—Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
- A61K36/725—Ziziphus, e.g. jujube
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
Abstract
The invention discloses a process for making solid particle healthy vinegar from Selaginella uncinata and Euryale ferox leaves. According to the solid particle healthy vinegar made from the Selaginella uncinata and the Euryale ferox leaves, the Selaginella uncinata and the Euryale ferox leaves are taken as the main raw materials, yams are taken as a substrate, and the healthy vinegar is prepared through the steps of pretreatment of the Selaginella uncinata and the Euryale ferox leaves, pretreatment of the yams, mixing, steaming, inoculation, fermentation, post-maturing, press filtering, aging and the like. The Selaginella uncinata and the Euryale ferox leaves are subjected to compound enzyme treatment after fixation, pungency and astringency of the Selaginella uncinata and the Euryale ferox leaves can be removed through fixation, the taste and flavor of the finished vinegar are improved, the utilization rate of the Selaginella uncinata and the Euryale ferox leaves can be increased through the compound enzyme treatment, the nutrients of the finished vinegar are enriched by taking the yams as the substrate, the taste and the quality of the finished solid particle healthy vinegar made from the Selaginella uncinata and the Euryale ferox leaves are further improved through aging, and the solid particle healthy vinegar made from the Selaginella uncinata and the Euryale ferox leaves is enabled to have the health care effects of clearing heat, promoting diuresis, stop bleeding, reliving a cough, eliminating phlegm, freeing channels, promoting the circulation of qi and blood and the like.
Description
Technical field
The present invention relates to the brewage process of a kind of vinegar, especially relate to a kind of CUIYUNCAO Folium Euryales solid particle health promoting vinegar
Brewage process.
Background technology
CUIYUNCAO, another name dragon palpus, Indigo Naturalis etc., for Selaginaceae Selaginella herbaceos perennial, with all herbal medicine.The whole year can
Adopt, using fresh herb or dry, its sweet in the mouth, light, cool in nature." florilegium " cloud: " property is good cloudy, and color is dark green lovely, the soft stem of spire, heavy broken sprains,
It is just like emerald green coin.Its root is met soil and is just given birth to, and sees that day then disappears, plants under Herba Damnacanthi, Musa basjoo Sieb. Et Zucc., Flos Begoniae Evansianae splendid." there is clearing away heat-damp and promoting diuresis, hemostasis
The health-care effect such as cough-relieving, eleminating phlegm and freeing channels.
Folium Euryales, another name Caput Gallus domesticus dish, thorn Folium Nelumbinis etc., for the leaf of Nymphaeceae annual large-scale aquatic herbaceous plant Semen Euryales, adopt June
Collection dries, and treats the disease such as retention of placenta, haematemesis.Its bitter in the mouth, pungent, property is put down, and returns liver, kidney channel." Chongqing medical herbs " is recorded: " circulation of qi promoting,
And blood, hemostasis.Control haematemesis." there is the health-care effect such as circulation of qi promoting and blood.
Along with the raising of people's health care consciousness, nutritious, the CUIYUNCAO of green health, wide material sources, Folium Euryales except
Outside Chinese herbal medicine, not yet being utilized by large-scale processing, associated product category is less, with CUIYUNCAO, Folium Euryales is especially
Primary raw material, Rhizoma Dioscoreae are the health promoting vinegar that substrate is brewageed, and there is not yet Related product listing.
Summary of the invention
It is an object of the invention to, for existing CUIYUNCAO, Folium Euryales in addition to as Chinese herbal medicine, not yet be added on a large scale
Work utilizes, and the less problem of associated product category, it is provided that the brewage process of a kind of CUIYUNCAO Folium Euryales solid particle health promoting vinegar is filled
Point make use of the nutritional labeling in raw material, improve CUIYUNCAO, the economic worth of Folium Euryales and nutritive value, abundant CUIYUNCAO,
The product category of Folium Euryales, is that finished product health promoting vinegar has the health care works such as clearing away heat-damp and promoting diuresis, hemostasis cough-relieving, eleminating phlegm and freeing channels, circulation of qi promoting and blood
With.
The present invention solves its technical problem and is adopted the technical scheme that:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: take fresh CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae, go the removal of impurity, clean with flowing water
The steam of 135 DEG C is used CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae to be completed 20s after clean, will after completing
10kg CUIYUNCAO, 7kg Folium Euryales, 2kg Herba Hemisteptae Lyratae, 1kg paddy skin rattan, 1kg Flos micheliae Albae fiberizer grind, and reenter colloid mill, mill
Become raw material rotten, in raw material gruel, add the cellulase of 0.4kg, the hemicellulase of 0.2kg, the pectase of 0.2kg, 0.1kg
Saccharifying enzyme, united hydrolysis 160min in 47 DEG C of conditions, make raw material mud;
B. Rhizoma Dioscoreae pretreatment: take Rhizoma Dioscoreae fresh, that nothing is rotten, rinse well, insert in digesting apparatus and cook, use defibrination after cooling
Machine grinds, and makes Rhizoma Dioscoreae mud;
C. mixing: take raw material mud 10kg, Rhizoma Dioscoreae mud 7kg, Folium Microcoris paniculatae powder 4kg, Rhizoma Gymnadeniae powder 2kg, spiny jujuba seed powder 2kg, eagle tea powder
2kg, Herba Sedi powder 1kg, black corn flour 1kg, Caulis Bambusae In Taeniam powder 1kg, wheat bran 1kg, Sorghum vulgare Pers. powder 1kg, stir, make mixing
Thing;
D. steaming: mixture enters in digesting apparatus, is passed through steam, steams 40min, and to well-done, rear airing, to room temperature, makes raw material
Unstrained spirits;
E. alcohol fermentation: add the yeast of 0.23kg, the Bulbus Lilii powder of 3kg, the Rhizoma Dioscoreae powder of 2kg, 2kg in 10kg raw material unstrained spirits
Rhizoma Polygonati powder, the powder of Radix Puerariae of 1kg, the Pseudobulbus Cremastrae Seu Pleiones powder of 1kg, the Semen Granati powder of 1kg, after stirring, add the drinking water of 45kg, temperature
Degree control is 32 DEG C, ferments 16 days, prepares raw vinegar;
F. acetic fermentation: add the acetic acid bacteria of 0.27kg in raw vinegar, stir, 46 DEG C of environment bottom fermentations are after 10 days, no longer
Temperature control, raw vinegar is naturally cooling to 35 DEG C, when fermentation to raw vinegar acidity reaches 9.6g/100ml, stops acetic fermentation;
G. after-ripening: add the Sal of 0.6kg in the raw vinegar after fermentation, stands 7 days after stirring;
H. squeeze and filter: by the raw vinegar after after-ripening through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The chitosan of 0.04kg, the activated carbon of 0.01kg, the fish glue of 0.01kg, stir, and stands 12h, prepares fermented vinegar liquid;
I. aging: fermented vinegar liquid is inserted in hermetic container and stand 15 days, after aging, fermented vinegar liquid is sterilized under 84 DEG C of environment
10min, is concentrated in vacuo the fermented vinegar liquid after sterilizing under the conditions of 0.18MPa, temperature 62 DEG C, and prepared moisture is
The mixing concentrate of 35%;
J. it is dried: by mixing concentrate under the conditions of-30 DEG C, freezing 8h, then presses 15kg/m in useful load2, operating pressure
It is dried under conditions of 53Pa, parsing pressure 36Pa, temperature 48 DEG C, prepares compound;
K. pelletize: compound relative humidity is 55%, in temperature is the closed job-shop of 15 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 40 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
Beneficial effect: the present invention uses after CUIYUNCAO, Folium Euryales being completed and carries out compound enzyme process, completes and can remove kingfisher
The harsh flavor carried in cloud grass, Folium Euryales, improves mouthfeel and the local flavor of finished product vinegar, is processed by compound enzyme and can improve emerald green cloud
Grass, the utilization ratio of Folium Euryales, with Rhizoma Dioscoreae as substrate, more enrich the nutrient substance of finished product vinegar, clear by compound clarifier
Clear process, improves the color and luster of finished product CUIYUNCAO Folium Euryales solid particle health promoting vinegar, by aging, further improves finished product emerald green
The mouthfeel of cloud grass Folium Euryales solid particle health promoting vinegar and quality, make finished product CUIYUNCAO Folium Euryales solid particle health promoting vinegar have heat clearing away
The health-care effects such as dampness removing, hemostasis cough-relieving, eleminating phlegm and freeing channels, circulation of qi promoting and blood.
Detailed description of the invention
Embodiment one:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: take fresh CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae, go the removal of impurity, clean with flowing water
The steam of 135 DEG C is used CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae to be completed 20s after clean, will after completing
10kg CUIYUNCAO, 7kg Folium Euryales, 2kg Herba Hemisteptae Lyratae, 1kg paddy skin rattan, 1kg Flos micheliae Albae fiberizer grind, and reenter colloid mill, mill
Become raw material rotten, in raw material gruel, add the cellulase of 0.4kg, the hemicellulase of 0.2kg, the pectase of 0.2kg, 0.1kg
Saccharifying enzyme, united hydrolysis 160min in 47 DEG C of conditions, make raw material mud;
B. Rhizoma Dioscoreae pretreatment: take Rhizoma Dioscoreae fresh, that nothing is rotten, rinse well, insert in digesting apparatus and cook, use defibrination after cooling
Machine grinds, and makes Rhizoma Dioscoreae mud;
C. mixing: take raw material mud 10kg, Rhizoma Dioscoreae mud 7kg, Folium Microcoris paniculatae powder 4kg, Rhizoma Gymnadeniae powder 2kg, spiny jujuba seed powder 2kg, eagle tea powder
2kg, Herba Sedi powder 1kg, black corn flour 1kg, Caulis Bambusae In Taeniam powder 1kg, wheat bran 1kg, Sorghum vulgare Pers. powder 1kg, stir, make mixing
Thing;
D. steaming: mixture enters in digesting apparatus, is passed through steam, steams 40min, and to well-done, rear airing, to room temperature, makes raw material
Unstrained spirits;
E. alcohol fermentation: add the yeast of 0.23kg, the Bulbus Lilii powder of 3kg, the Rhizoma Dioscoreae powder of 2kg, 2kg in 10kg raw material unstrained spirits
Rhizoma Polygonati powder, the powder of Radix Puerariae of 1kg, the Pseudobulbus Cremastrae Seu Pleiones powder of 1kg, the Semen Granati powder of 1kg, after stirring, add the drinking water of 45kg, temperature
Degree control is 32 DEG C, ferments 16 days, prepares raw vinegar;
F. acetic fermentation: add the acetic acid bacteria of 0.27kg in raw vinegar, stir, 46 DEG C of environment bottom fermentations are after 10 days, no longer
Temperature control, raw vinegar is naturally cooling to 35 DEG C, when fermentation to raw vinegar acidity reaches 9.6g/100ml, stops acetic fermentation;
G. after-ripening: add the Sal of 0.6kg in the raw vinegar after fermentation, stands 7 days after stirring;
H. squeeze and filter: by the raw vinegar after after-ripening through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The chitosan of 0.04kg, the activated carbon of 0.01kg, the fish glue of 0.01kg, stir, and stands 12h, prepares fermented vinegar liquid;
I. aging: fermented vinegar liquid is inserted in hermetic container and stand 15 days, after aging, fermented vinegar liquid is sterilized under 84 DEG C of environment
10min, is concentrated in vacuo the fermented vinegar liquid after sterilizing under the conditions of 0.18MPa, temperature 62 DEG C, and prepared moisture is
The mixing concentrate of 35%;
J. it is dried: by mixing concentrate under the conditions of-30 DEG C, freezing 8h, then presses 15kg/m in useful load2, operating pressure
It is dried under conditions of 53Pa, parsing pressure 36Pa, temperature 48 DEG C, prepares compound;
K. pelletize: compound relative humidity is 55%, in temperature is the closed job-shop of 15 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 40 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
Embodiment two:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: take fresh CUIYUNCAO, Folium Euryales, the Flos rosae multiflorae, Radix Sophorae Tonkinensis, Flos Sauropi changiani leaf, noodles dish, go the removal of impurity, take
10kg CUIYUNCAO, 6kg Folium Euryales, the 2kg Flos rosae multiflorae, 2kg Radix Sophorae Tonkinensis, 1kg Flos Sauropi changiani leaf, 1kg noodles dish mix homogeneously, prepare mixing
Raw material, cleans up mixing raw material flowing water, uses the steam of 128 DEG C to complete raw material leaf 35s, will after steam beating
Mixing raw material fiberizer grinds, and reenters colloid mill, wears into raw material rotten, add in raw material gruel 0.4kg cellulase,
The pectase of 0.04kg, the flavor protease of 0.03kg, the citric acid of 0.5kg, the wild grape juice of 2kg, the Sucus Rosae Normalis of 2kg, 2kg
Ground ear dish juice, the fiery spine juice of 1kg, the Radix Saurauiae Tristylae juice of 1kg, united hydrolysis 130min in 52 DEG C of conditions, make raw material mud;
B. Rhizoma Dioscoreae pretreatment: take Rhizoma Dioscoreae fresh, that nothing is rotten, Pedicellus et Pericarpium Trapae, Rhizoma Dioscoreae, rinse well, be cut into yam loaf, diamond-shaped block, mountain
Medicine block, inserts in digesting apparatus after taking 10kg yam loaf, 3kg diamond-shaped block, 1kg Rhizoma Dioscoreae block mix homogeneously and cooks, with mill after cooling
Pulp grinder grinds, and makes Rhizoma Dioscoreae mud;
C. mixing: take raw material cob 10kg, Rhizoma Dioscoreae mud 7.4kg, Folium Capsici powder 5kg, JIAOSANXIAN (Fructus Crataegi, Fructus Hordei Germinatus, Massa Medicata Fermentata) powder 3kg, one hundred days inulin 3kg, mountain
Short, bristly hair or beard juice 2kg, papaya 2kg, Aloe powder 1kg, Rhizoma Dioscoreae Semen Glycines powder 1kg, Holland Semen Glycines powder 1kg, Herba Houttuyniae powder 1kg, Gaster caprae seu Ovis mycopowder
1kg, Dioscorea subcalva Prain et Burhll powder 1kg, Radix Cynanchi Auriculati powder 1kg, stir, make mixture;
D. steaming: mixture enters in digesting apparatus, is passed through steam, steams 36min, and to well-done, rear airing, to room temperature, makes raw material
Unstrained spirits;
E. alcohol fermentation: add the brewer yeast of 0.33kg in 10kg raw material unstrained spirits, after stirring, the concentration adding 38kg is 3%
Selenium-rich water solution, the egg fruit juice of 3kg, 3kg oatmeal, the glucose of 2kg, the kernel juice of 2kg, the Radix Achyranthis Bidentatae inulin of 2kg,
The Folium Braseniae Schreberi juice of 1kg, the BrachybotryS paridiformis juice of 1kg, it is 34 DEG C that temperature controls, and ferments 11 days, prepares raw vinegar;
F. acetic fermentation: add the acetic acid yeast of 0.39kg in 10kg raw vinegar, stir, 45 DEG C of environment bottom fermentations 15 days
After, no longer temperature control, raw vinegar is naturally cooling to 32 DEG C, when fermentation to raw vinegar acidity reaches 7.9g/100ml, stops acetic fermentation;
G. after-ripening: add the Sal of 0.5kg in the raw vinegar after fermentation, stands 12 days after stirring;
H. squeeze and filter: by the raw vinegar after after-ripening through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The gelatin of 0.03kg, the agar of 0.01kg, stir, and stands 27h, prepares fermented vinegar liquid;
I. purification: be also 15MPa at pressure by fermented vinegar, the aperture of ultrafilter membrane is to carry out ultrafilter membrane purification under conditions of 8 μm:
J. aging: fermented vinegar liquid after purification is inserted aging 28 days in hermetic container, by fermented vinegar liquid at 126 DEG C of rings after aging
Sterilize under border 15s, is concentrated in vacuo by the fermented vinegar liquid after sterilizing under the conditions of 0.15MPa, temperature 66 DEG C, and prepared moisture contains
Amount is the mixing concentrate of 32%;
K. it is dried: setting drying curve, drying time is 12h, mixing concentrate is heated to 95 DEG C and keeps 30min, then
It is quickly cooled to 90 DEG C, after keeping 30 min, is quickly cooled to 80 DEG C, after keeping 30 min, then material is naturally cooled to 60
DEG C, be evacuated to 80Pa and be dried, prepare compound;
L. pelletize: compound relative humidity is 36%, in temperature is the closed job-shop of 24 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 50 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
Embodiment three:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: select the CUIYUNCAO of maturation, Folium Euryales, Herba Trigonotidis peduncularis, Rabdosia rubescens, Folium Granati, Flos kerriae japonicae, clean up
Rear be cut into 3mm respectively broken section, makes CUIYUNCAO section, Folium Euryales section, Herba Trigonotidis peduncularis section, Rabdosia rubescens section, Folium Granati section, Flos kerriae japonicae
Section, takes 10kg CUIYUNCAO, 7kg Folium Euryales, 3kg Herba Trigonotidis peduncularis section, 2kg Rabdosia rubescens section, 1kg Folium Granati section, the mixing of 1kg Flos kerriae japonicae section
Uniformly, prepare raw material section, standby;
B. soak: raw material section being put in the white vinegar that total acidity is 34% of 68kg and soak, soak time is 25 days, pass through
Filter obtains soaking vinegar and raw material slag, is filtered dry standby by raw material slag;
C. pulverize: the raw material slag after being filtered dry is pulverized through superfine wall-broken grinder, prepare raw material powder, standby;
D. Rhizoma Dioscoreae pretreatment: fresh Rhizoma Dioscoreae, Carlina acaulis, Rhizoma Polygonati, Rhizoma Polygonati Odorati is once purged, is cut into Rhizoma Dioscoreae grain, Carlina acaulis grain, Huang respectively
Essence grain, Rhizoma Polygonati Odorati grain, granularity is 7 grams/, takes the Rhizoma Dioscoreae grain of 10kg, the Carlina acaulis grain of 4kg, the Rhizoma Polygonati grain of 1kg, the Rhizoma Polygonati Odorati of 1kg
Place in digester after grain mix homogeneously and cook to ripe and do not stick with paste, spread cooling, prepare Rhizoma Dioscoreae material;
E. mixing: add the raw material powder of 12kg, 4kg linseed meal, 3kg medlar bud powder, the Semen Coicis of 2kg in the Rhizoma Dioscoreae material of 10kg
Powder, the Fructus Ligustri Lucidi powder of 2kg, the gorgon euryale seed powder of 2kg, the Caulis Polygoni Multiflori powder of 1kg, the Herba Peperomiae Dindygulensis powder of 1kg, the wild tapioca flour of 1kg, 1kg green
Tea powder, stirs, and prepares compound;
F. alcohol fermentation: add the brewer yeast of 0.36kg in compound, after stirring, adds the drinking water of 35kg, 7kg
Leaf of Moringa powder, 3kg Fructus rhois chinensis leaf powder, 3kg Herba Thesii powder, the Pleurotus eryngii powder of 2kg, the black cloth woods juice of 2kg, the juice of Fructus Hippophae of 1kg,
The melon tree powder of 1kg, the head powder of 1kg, the Caulis et folium euphorbiae milii fruit juice of 1kg, U.S.'s dense melon juice of 1kg, it is 54 DEG C that temperature controls, and ferment 90h,
Prepare alcohol fermentation material;
G. acetic fermentation: after alcohol fermentation terminates, adds the acetic acid yeast of 0.46kg, 4kg gold buckwheat in alcohol fermentation material
Wheat juice, the Fructus Sechii edulis juice of 3kg, the bilberry juice of 3kg, the Eucommia Leaf Powder of 2kg, the yacon juice of 1kg, the bean Sucus Pyri of 1kg, 1kg
Fructus Benincasae chiehquae juice, the Fructus Fici Pumilae fruit juice of 1kg, 1kg Fructus Rosae Davuricae juice, stir, 48 DEG C of environment bottom fermentation 200h, prepare acetic fermentation thing
Material;
H. squeeze and filter: by acetic fermentation material through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The Bentonite of 0.03kg, the chitosan of 0.02kg, stir, and stands 14 days, obtains fermented vinegar;
I. mixing, aging: take the fermented vinegar 8kg soaked in vinegar 13kg, step h in step b, stir, prepares mixed
Closing vinegar, put into by mixing vinegar in sterilized cylinder, potting sternly carries out aging, aging 35 days, temperature is 4 DEG C, continues after aging
5 days are stood in hermetic container;
J. sterilize, concentrate: sterilize the mixing vinegar after aging under 88 DEG C of environment 2min, is existed by the fermented vinegar liquid after sterilizing
0.22MPa, is concentrated in vacuo under the conditions of temperature 69 DEG C, and prepared moisture is the mixing concentrate of 37%;
K. it is dried: by the mixing concentrate after homogenizing under the conditions of-20 DEG C, freezing 5h, then presses 18kg/m in useful load2, work
It is dried under conditions of making pressure 58Pa, parsing pressure 32Pa, temperature 52 DEG C, prepares compound;
L. pelletize: compound relative humidity is 51%, in temperature is the closed job-shop of 19 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 30 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
Embodiment four:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: take fresh CUIYUNCAO, Folium Euryales, Herba Lophatheri, tumble-weed, Herba Saussureae Involueratae, Radix Rubiae, go the removal of impurity, take
10kg CUIYUNCAO, 8kg Folium Euryales, 2kg Herba Lophatheri, 1kg tumble-weed, 1kg Herba Saussureae Involueratae, the Radix Rubiae mix homogeneously of 1kg, prepare mixed
Close raw material, mixing raw material flowing water is cleaned up, use the steam of 140 DEG C raw material leaf to be completed 12s, after steam beating
Mixing raw material fiberizer is ground, reenters colloid mill, wear into raw material grass rotten, in raw material grass gruel, add the cellulose of 0.45kg
Enzyme, the pectase of 0.24kg, the flavor protease of 0.2kg, united hydrolysis 120min in 51 DEG C of conditions, makes raw material cob;
B. Rhizoma Dioscoreae pretreatment: take Rhizoma Dioscoreae fresh, that nothing is rotten, Smallanthus sonchifolius, Fructus Mali Asiaticae, Fructus Arctii, rinse well, be cut into yam loaf, Smallanthus sonchifolius
Block, Fructus Mali Asiaticae block, Fructus Arctii block, insert steaming and decocting after taking 10kg yam loaf, 4kg Smallanthus sonchifolius block, 1kg Fructus Mali Asiaticae block, 1kg Fructus Arctii block mix homogeneously
Equipment cooks, grinds with fiberizer after cooling, make Rhizoma Dioscoreae mud;
C. mixing: take raw material cob 10kg, Rhizoma Dioscoreae mud 9kg, bean curd fruit powder 4kg, seed of Fructus Crataegi powder 3kg, winter jasmine pollen 3kg, Ji silver
Pollen 2kg, Folium Ilicis Purpureae powder 2kg, maca powder 1kg, Althaea rosea (L.) Cavan. pollen 1kg, Radix Scrophulariae powder 1kg, Folium Cinnamomi burmannii powder 1kg, oatmeal 1kg, fill
Divide and stir, make mixture;
D. steaming: mixture enters in digesting apparatus, is passed through steam, steams 50min, and to well-done, rear airing, to room temperature, makes raw material
Unstrained spirits;
E. alcohol fermentation: add the bacillus subtilis of the brewer yeast of 0.28kg, 0.05kg in 10kg raw material unstrained spirits, after stirring,
Adding the drinking water of 25kg, it is 37 DEG C that temperature controls, and ferments 14 days, prepares raw vinegar;
F. acetic fermentation: add the acetic acid bacteria of 0.33kg in raw vinegar, stir, 48 DEG C of environment bottom fermentations are after 14 days, no longer
Temperature control, raw vinegar is naturally cooling to 32 DEG C, when fermentation to raw vinegar acidity reaches 8.9g/100ml, stops acetic fermentation;
G. after-ripening: add the Sal of 0.4kg in the raw vinegar after fermentation, stands 12 days after stirring;
H. squeeze and filter: by the raw vinegar after after-ripening through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The tannin of 0.04kg, the Bentonite of 0.01kg, stir, and stands 26h, prepares fermented vinegar liquid;
I. aging: fermented vinegar liquid is inserted in hermetic container and stand 35 days, after aging, fermented vinegar liquid is sterilized under 128 DEG C of environment
10s, is concentrated in vacuo the fermented vinegar liquid after sterilizing under the conditions of 0.23MPa, temperature 66 DEG C, and prepared moisture is 28%
Mixing concentrate;
J. it is dried: by the mixing concentrate after homogenizing under the conditions of-23 DEG C, freezing 16h, then presses 12kg/m in useful load2, work
It is dried under conditions of making pressure 60Pa, parsing pressure 31Pa, temperature 52 DEG C, prepares compound;
K. pelletize: compound relative humidity is 34%, in temperature is the closed job-shop of 24 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 60 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
Embodiment five:
A kind of brewage process of CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process use with
Lower step:
A. pretreatment of raw material: select the CUIYUNCAO of maturation, Folium Euryales, Folium Chrysanthemi, Flos Inulae, the dish that collapses, The Cloud Terrace grass, after cleaning up
It is cut into broken section of 2mm respectively, makes CUIYUNCAO section, Folium Euryales section, Folium Stevlae Rebaudianae section, Flos Inulae section, dish section of collapsing, The Cloud Terrace grass section, take
10kg CUIYUNCAO section, 8kg Folium Euryales section, 3kg Folium Stevlae Rebaudianae section, 2kg Flos Inulae section, 1kg collapse dish section, the mixing of 1kg The Cloud Terrace grass section all
Even, prepare raw material section, standby;
B. soak: raw material section being put in the white vinegar that total acidity is 38% of 72kg and soak, soak time is 28 days, pass through
Filter obtains soaking vinegar and raw material slag, is filtered dry standby by raw material slag;
C. pulverize: the raw material slag after being filtered dry is pulverized through superfine wall-broken grinder, prepare raw material powder, standby;
D. Rhizoma Dioscoreae pretreatment: fresh Rhizoma Dioscoreae, Herba Cichorii, porkling potato, Chinese yam beans is once purged, is cut into Rhizoma Dioscoreae grain, Herba Cichorii grain, pig respectively
Young potato grain, Rhizoma Dioscoreae beans, granularity is 5 grams/, takes the Rhizoma Dioscoreae grain of 10kg, the Herba Cichorii grain of 5kg, the porkling potato grain of 2kg, 1kg
Place in digester after Rhizoma Dioscoreae beans mix homogeneously and cook to ripe and do not stick with paste, spread cooling, prepare Rhizoma Dioscoreae material;
E. mixing: add the raw material powder of 14kg, 4kg Ilex cornuta Lindl. seed powder, 3kg thorn tender bud powder, the Fructus Alpiniae Oxyphyllae of 2kg in the Rhizoma Dioscoreae material of 10kg
Core powder, the spiny jujuba seed powder of 2kg, the Dutch inulin of 2kg, the Caulis Polygoni Multiflori powder of 1kg, the Herba Sedi powder of 1kg, the semen trichosanthis powder of 1kg,
The eagle tea powder of 1kg, the peony pollen of 1kg, stir, and prepares compound;
F. alcohol fermentation: add the brewer yeast of 0.38kg in compound, after stirring, adds the drinking water of 42kg, 7kg
Moringa seeds powder, the Folium Apocyni Veneti powder of 3kg, the Rabdosia japonica powder of 3kg, the arrowhead powder of 2kg, the Sucus Phyllanthi of 2kg, the Fructus Rosae Laevigatae fruit of 1kg
Juice, the Herba youngiae japonicae powder of 1kg, the Radix seu Caulis Embeliae Parviflorae powder of 1kg, the arhat juice of 1kg, the Fructus Elaeagni juice of 1kg, it is 58 DEG C that temperature controls, and sends out
Ferment 120h, prepares alcohol fermentation material;
G. acetic fermentation: after alcohol fermentation terminates, adds the acetic acid yeast of 0.45kg, 4kg Semen Hoveniae (Fructus Hoveniae) in alcohol fermentation material
Juice, the gooseberry juice of 3kg, 3kg thorn bubble juice, the powder of Folium Mori of 2kg, the Cassia surattensis leaf powder of 1kg, the wild grape juice of 1kg, five times of 1kg
Sub-juice, red Lee's juice of 1kg, 1kg sea mustard powder, stir, 47 DEG C of environment bottom fermentations 8 days, prepares acetic fermentation material;
H. squeeze and filter: by acetic fermentation material through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The activated carbon of 0.02kg, the gelatin of 0.02kg, the kieselguhr of 0.01kg, stir, and stands 9 days, obtains fermented vinegar;
I. mixing, aging: take the fermented vinegar 11kg soaked in vinegar 12kg, step h in step b, stir, prepares mixed
Closing vinegar, put into by mixing vinegar in sterilized cylinder, potting sternly carries out aging, aging 30 days, temperature is 5 DEG C, continues after aging
7 days are stood in hermetic container;
J. sterilize, concentrate: sterilize the mixing vinegar after aging under 122 DEG C of environment 15s, is existed by the fermented vinegar liquid after sterilizing
0.26MPa, is concentrated in vacuo under the conditions of temperature 68 DEG C, and prepared moisture is the mixing concentrate of 32%;
K. it is dried: by the mixing concentrate after homogenizing under the conditions of-26 DEG C, freezing 11h, then presses 12kg/m in useful load2, work
It is dried under conditions of making pressure 63Pa, parsing pressure 37Pa, temperature 55 DEG C, prepares compound;
L. pelletize: compound relative humidity is 38%, in temperature is the closed job-shop of 16 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 80 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned embodiment
Detail, in the technology concept of the present invention, technical scheme can be carried out multiple simple variant, this
A little simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technical characteristic described in above-mentioned detailed description of the invention, at not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to various can
The compound mode of energy illustrates the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as it is without prejudice to this
The thought of invention, it should be considered as content disclosed in this invention equally.
Part that the present invention does not relate to is the most same as the prior art maybe can use prior art to be realized.
Claims (1)
1. the brewage process of a CUIYUNCAO Folium Euryales solid particle health promoting vinegar, it is characterised in that described brewage process uses
Following steps:
A. pretreatment of raw material: take fresh CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae, go the removal of impurity, clean with flowing water
The steam of 135 DEG C is used CUIYUNCAO, Folium Euryales, Herba Hemisteptae Lyratae, paddy skin rattan, Flos micheliae Albae to be completed 20s after clean, will after completing
10kg CUIYUNCAO, 7kg Folium Euryales, 2kg Herba Hemisteptae Lyratae, 1kg paddy skin rattan, 1kg Flos micheliae Albae fiberizer grind, and reenter colloid mill, mill
Become raw material rotten, in raw material gruel, add the cellulase of 0.4kg, the hemicellulase of 0.2kg, the pectase of 0.2kg, 0.1kg
Saccharifying enzyme, united hydrolysis 160min in 47 DEG C of conditions, make raw material mud;
B. Rhizoma Dioscoreae pretreatment: take Rhizoma Dioscoreae fresh, that nothing is rotten, rinse well, insert in digesting apparatus and cook, use defibrination after cooling
Machine grinds, and makes Rhizoma Dioscoreae mud;
C. mixing: take raw material mud 10kg, Rhizoma Dioscoreae mud 7kg, Folium Microcoris paniculatae powder 4kg, Rhizoma Gymnadeniae powder 2kg, spiny jujuba seed powder 2kg, eagle tea powder
2kg, Herba Sedi powder 1kg, black corn flour 1kg, Caulis Bambusae In Taeniam powder 1kg, wheat bran 1kg, Sorghum vulgare Pers. powder 1kg, stir, make mixing
Thing;
D. steaming: mixture enters in digesting apparatus, is passed through steam, steams 40min, and to well-done, rear airing, to room temperature, makes raw material
Unstrained spirits;
E. alcohol fermentation: add the yeast of 0.23kg, the Bulbus Lilii powder of 3kg, the Rhizoma Dioscoreae powder of 2kg, 2kg in 10kg raw material unstrained spirits
Rhizoma Polygonati powder, the powder of Radix Puerariae of 1kg, the Pseudobulbus Cremastrae Seu Pleiones powder of 1kg, the Semen Granati powder of 1kg, after stirring, add the drinking water of 45kg, temperature
Degree control is 32 DEG C, ferments 16 days, prepares raw vinegar;
F. acetic fermentation: add the acetic acid bacteria of 0.27kg in raw vinegar, stir, 46 DEG C of environment bottom fermentations are after 10 days, no longer
Temperature control, raw vinegar is naturally cooling to 35 DEG C, when fermentation to raw vinegar acidity reaches 9.6g/100ml, stops acetic fermentation;
G. after-ripening: add the Sal of 0.6kg in the raw vinegar after fermentation, stands 7 days after stirring;
H. squeeze and filter: by the raw vinegar after after-ripening through Filter Press, obtain acetic acid fermentation liquid, adds in acetic acid fermentation liquid
The chitosan of 0.04kg, the activated carbon of 0.01kg, the fish glue of 0.01kg, stir, and stands 12h, prepares fermented vinegar liquid;
I. aging: fermented vinegar liquid is inserted in hermetic container and stand 15 days, after aging, fermented vinegar liquid is sterilized under 84 DEG C of environment
10min, is concentrated in vacuo the fermented vinegar liquid after sterilizing under the conditions of 0.18MPa, temperature 62 DEG C, and prepared moisture is
The mixing concentrate of 35%;
J. it is dried: by mixing concentrate under the conditions of-30 DEG C, freezing 8h, then presses 15kg/m in useful load2, operating pressure
It is dried under conditions of 53Pa, parsing pressure 36Pa, temperature 48 DEG C, prepares compound;
K. pelletize: compound relative humidity is 55%, in temperature is the closed job-shop of 15 DEG C, is broken into by compound with disintegrating machine
Uniform particulate matter, and by particulate matter through the screen filtration of 40 mesh, prepare CUIYUNCAO Folium Euryales solid particle health promoting vinegar.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107723198A (en) * | 2017-11-26 | 2018-02-23 | 陶然 | The brewage process of solid particle health-care vinegar |
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CN102399676A (en) * | 2010-09-14 | 2012-04-04 | 张伟 | Preparation method of vinegar powder |
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CN1044495A (en) * | 1989-01-25 | 1990-08-08 | 山西省晋宝实业公司 | A kind of production method of powder vinegar |
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