CN106046951A - High-ultraviolet-resistance butylbenzene waterproof coating and preparation method thereof - Google Patents
High-ultraviolet-resistance butylbenzene waterproof coating and preparation method thereof Download PDFInfo
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- CN106046951A CN106046951A CN201610405294.5A CN201610405294A CN106046951A CN 106046951 A CN106046951 A CN 106046951A CN 201610405294 A CN201610405294 A CN 201610405294A CN 106046951 A CN106046951 A CN 106046951A
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- butylbenzene
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D109/00—Coating compositions based on homopolymers or copolymers of conjugated diene hydrocarbons
- C09D109/06—Copolymers with styrene
- C09D109/08—Latex
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a high-ultraviolet-resistance butylbenzene waterproof coating and a preparation method thereof. The high-ultraviolet-resistance butylbenzene waterproof coating is made from the following materials according to parts by weight: 75-105 parts of butylbenzene emulsion 40% in solid content, 3-6 parts of natural colorful stone powder, 2-4 parts of nano zinc powder, 5-10 parts of aluminum chromium residue, 4-8 parts of dipropylene glycol monosalicylate, 6-9 parts of waste glass, 5-10 parts of epoxy alkyl silicone oil, 3-6 parts of disproportionated potassium rosinate, 8-12 parts of methylated amino resin, 2-4 parts of sodium lauroyl sarcosine, 1-3 parts of sorbitol polyoxyethylene ether tallate, 3-6 parts of tetraethyl orthosilicate, 40-50 parts of ethylene glycol diethyl ether, 3-5 parts of sodium carboxymethyl starch, 5-7 parts of lead and zinc tailings, 2-3 parts of 2-hydroxy-4-methoxybenzophenone-5-sulfonc acid, 1-2 parts of sophorolipid, and 8-10 parts of pebbles. The waterproof coating prepared herein has high ultraviolet resistance, high adhesion, high mechanical strength, good waterproof effect, stable properties, good convenience of use and good safety and reliability.
Description
Technical field
The present invention relates to strong butylbenzene water-repellent paint of a kind of anti-uv-ray and preparation method thereof, belong to water-repellent paint neck
Territory.
Background technology
The water-repellent paint used in architectural engineering becomes building water-proof paint, referred to as water-repellent paint, is by coating
Construction and form one layer of general name with the repellent membrane mate-rials of water resistance, be with waterproof, moistureproof, antiseepage, leakproof be main
The functional type building coating of purpose.Building water-proof paint is with synthesis macromolecule, Colophonium, polymer modified asphalt, inorganic material etc.
For main body, mix appropriate auxiliary agent, material modified, packing material etc. and be processed into.Compared with waterproof roll, water-repellent paint is constructed
Simple and convenient, it is adaptable to the basal plane of any shape, and fine and close seamless film can be formed, therefore, water-repellent paint has been widely used
In various waterproofing works.Along with the fast development of Architectural Paint in China, the harshest to the performance requirement of water-repellent paint.Existing
The uviolresistance of water-repellent paint increasingly cannot meet the demand of existing market.
Summary of the invention
In order to overcome above-mentioned deficiency, the invention provides the strong butylbenzene water-repellent paint of a kind of anti-uv-ray and system thereof
Preparation Method.
For achieving the above object, the present invention adopts the following technical scheme that:
The butylbenzene water-repellent paint that a kind of anti-uv-ray is strong, is made up of the raw material of following weight portion: solid content is 40%
Styrene-butadiene latex 75-105, natural color stone powder 3-6, nano zinc powder 2-4, aluminum chromium slag 5-10, a contracting propylene glycol list salicylate 4-
8, cullet 6-9, epoxyhydrocarbyl silicone oil 5-10, disproportionated rosin acid potassium 3-6, methyl-etherified amino resins 8-12, Hamposyl L
Sodium 2-4, sorbierite polyoxyethylene ether tall-oil acid ester 1-3, tetraethyl orthosilicate 3-6, ethylene glycol diethyl ether 40-50, carboxymethyl
Starch Sodium 3-5, Pb-Zn tailings 5-7, BP-4 2-3, sophorolipid 1-2, cobble 8-10.
The preparation method of the butylbenzene water-repellent paint that a kind of anti-uv-ray is strong, comprises the following steps:
(1) by aluminum chromium slag, cullet, cobble, Pb-Zn tailings mix homogeneously, pulverizing, sieve, then heating is fused into molten
Melt liquid, put into after stirring and clear water carries out shrend, de-dry；The glass particle material obtained is pulverized, sieves,
Under the rotating speed of 5000-8000r/min, ball milling 3-6h, sieves, then with nitrogen for current-carrying gas by dried powder body according to giving
Powder amount is that 200-250g/min sends in balling furnace oxygen-acetylene flame stream, and current-carrying gas nitrogen flow rate is 45-55L/min；Oxygen
In gas-natural bluster stream, oxygen flow is 50-60L/min, and gas discharge is 60-70L/min；Drop after nodularization leaves height
Warm fire flame cools down behind field, then through cyclone collection, obtains spherical glass powder；
(2) being mixed homogeneously with natural color stone powder, nano zinc powder by the spherical glass powder obtained, the stirring that then adds water is made dense
Degree is the suspension of 45-50%, is subsequently adding carboxymethyl starch sodium and sophorolipid, stirs under the rotating speed of 2000-4000r/min
10-15min, filters, and dries；
(3) ethylene glycol diethyl ether is added in blender, add sodium lauroyl sarcosine and sorbitol polyoxyethylene ether
Tallate, stirs, and is subsequently adding a contracting propylene glycol list salicylate, epoxyhydrocarbyl silicone oil, disproportionated rosin acid
Potassium, methyl-etherified amino resins, BP-4 and tetraethyl orthosilicate, at 500-700r/min
Rotating speed under stir 1-3min, add styrene-butadiene latex, under the rotating speed of 200-400r/min stir 3-5min, be eventually adding step
Suddenly the raw material after (2) dry, stirs 8-12min under the rotating speed of 300-500r/min, gets product.
Beneficial effects of the present invention:
The present invention by add natural color stone powder, nano zinc powder, a contracting propylene glycol list salicylate, epoxyhydrocarbyl silicone oil,
BP-4 so that water-repellent paint has good ultraviolet-resistent property and weatherability.The present invention
The water-repellent paint uvioresistant ability prepared is strong, good weatherability, and adhesive force is strong, and mechanical strength is high, and good water-proof effect, properties of product are steady
Fixed, easy to use, safe and reliable.
Detailed description of the invention
The butylbenzene water-repellent paint that a kind of anti-uv-ray is strong, is made up of the raw material of following weight (kg): solid content is
The styrene-butadiene latex 90 of 40%, natural color stone powder 4.5, nano zinc powder 3, aluminum chromium slag 8, contracting propylene glycol list salicylate 6, cullet
7, epoxyhydrocarbyl silicone oil 8, disproportionated rosin acid potassium 4, methyl-etherified amino resins 10, sodium lauroyl sarcosine 3, sorbitol polyoxyethylene
Ether tallate 2, tetraethyl orthosilicate 4, ethylene glycol diethyl ether 45, carboxymethyl starch sodium 4, Pb-Zn tailings 6,2-hydroxyl-4-
Methoxy benzophenone-5-sulfonic acid 2.5, sophorolipid 1.5, cobble 9.
The preparation method of the butylbenzene water-repellent paint that a kind of anti-uv-ray is strong, comprises the following steps:
(1) by aluminum chromium slag, cullet, cobble, Pb-Zn tailings mix homogeneously, pulverizing, sieve, then heating is fused into molten
Melt liquid, put into after stirring and clear water carries out shrend, de-dry；The glass particle material obtained is pulverized, sieves,
Under the rotating speed of 6000r/min, ball milling 4h, sieves, and then with nitrogen for current-carrying gas by dried powder body according to powder sending quantity is
230g/min sends in balling furnace oxygen-acetylene flame stream, and current-carrying gas nitrogen flow rate is 50L/min；In oxygen-natural bluster stream
Oxygen flow is 55L/min, and gas discharge is 65L/min；Drop after nodularization cools down after leaving thermal-flame field, then
Through cyclone collection, obtain spherical glass powder；
(2) being mixed homogeneously with natural color stone powder, nano zinc powder by the spherical glass powder obtained, the stirring that then adds water is made dense
Degree is the suspension of 48%, is subsequently adding carboxymethyl starch sodium and sophorolipid, stirs 12min, mistake under the rotating speed of 3000r/min
Filter, dries；
(3) ethylene glycol diethyl ether is added in blender, add sodium lauroyl sarcosine and sorbitol polyoxyethylene ether
Tallate, stirs, and is subsequently adding a contracting propylene glycol list salicylate, epoxyhydrocarbyl silicone oil, disproportionated rosin acid
Potassium, methyl-etherified amino resins, BP-4 and tetraethyl orthosilicate, turning at 600r/min
Stir 2min under speed, add styrene-butadiene latex, under the rotating speed of 300r/min, stir 4min, after being eventually adding step (2) drying
Raw material, under the rotating speed of 400r/min stir 10min, get product.
The performance test results of the water-repellent paint that above-described embodiment is produced is as shown in the table:
Claims (2)
1. the butylbenzene water-repellent paint that an anti-uv-ray is strong, it is characterised in that be made up of the raw material of following weight portion: admittedly contain
Amount be 40% styrene-butadiene latex 75-105, natural color stone powder 3-6, nano zinc powder 2-4, aluminum chromium slag 5-10, one contracting propylene glycol list
Poplar acid esters 4-8, cullet 6-9, epoxyhydrocarbyl silicone oil 5-10, disproportionated rosin acid potassium 3-6, methyl-etherified amino resins 8-12, Laurel
Acylsarcosine sodium 2-4, sorbierite polyoxyethylene ether tall-oil acid ester 1-3, tetraethyl orthosilicate 3-6, ethylene glycol diethyl ether 40-
50, carboxymethyl starch sodium 3-5, Pb-Zn tailings 5-7, BP-4 2-3, sophorolipid 1-2, river
Cobble 8-10.
2. the preparation method of the butylbenzene water-repellent paint that an anti-uv-ray as claimed in claim 1 is strong, it is characterised in that
Comprise the following steps:
(1) by aluminum chromium slag, cullet, cobble, Pb-Zn tailings mix homogeneously, pulverizing, sieve, then heating is fused into melted
Liquid, puts into after stirring and carries out shrend in clear water, de-dry；The glass particle material obtained is pulverized, sieves,
Under the rotating speed of 5000-8000r/min, ball milling 3-6h, sieves, then with nitrogen for current-carrying gas by dried powder body according to giving
Powder amount is that 200-250g/min sends in balling furnace oxygen-acetylene flame stream, and current-carrying gas nitrogen flow rate is 45-55L/min；Oxygen
In gas-natural bluster stream, oxygen flow is 50-60L/min, and gas discharge is 60-70L/min；Drop after nodularization leaves height
Warm fire flame cools down behind field, then through cyclone collection, obtains spherical glass powder；
(2) being mixed homogeneously with natural color stone powder, nano zinc powder by the spherical glass powder obtained, the stirring that then adds water is made concentration and is
The suspension of 45-50%, is subsequently adding carboxymethyl starch sodium and sophorolipid, stirs 10-under the rotating speed of 2000-4000r/min
15min, filters, and dries；
(3) ethylene glycol diethyl ether is added in blender, add sodium lauroyl sarcosine and the appropriate that of sorbitol polyoxyethylene ether
Oleate, stirs, and is subsequently adding a contracting propylene glycol list salicylate, epoxyhydrocarbyl silicone oil, disproportionated rosin acid potassium, first
Etherified amino resins, BP-4 and tetraethyl orthosilicate, turning at 500-700r/min
Stir 1-3min under speed, add styrene-butadiene latex, under the rotating speed of 200-400r/min, stir 3-5min, be eventually adding step
(2) raw material after drying, stirs 8-12min under the rotating speed of 300-500r/min, gets product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610405294.5A CN106046951A (en) | 2016-06-12 | 2016-06-12 | High-ultraviolet-resistance butylbenzene waterproof coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610405294.5A CN106046951A (en) | 2016-06-12 | 2016-06-12 | High-ultraviolet-resistance butylbenzene waterproof coating and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106046951A true CN106046951A (en) | 2016-10-26 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610405294.5A Pending CN106046951A (en) | 2016-06-12 | 2016-06-12 | High-ultraviolet-resistance butylbenzene waterproof coating and preparation method thereof |
Country Status (1)
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| CN (1) | CN106046951A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103540195A (en) * | 2013-09-26 | 2014-01-29 | 芜湖杰诺科技有限公司 | High-adhesion water-proof coating |
| CN104479508A (en) * | 2014-12-24 | 2015-04-01 | 湖州南浔双林振森实木加工厂 | Preparation method of corrosion-resistant flame-retardant paint |
-
2016
- 2016-06-12 CN CN201610405294.5A patent/CN106046951A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103540195A (en) * | 2013-09-26 | 2014-01-29 | 芜湖杰诺科技有限公司 | High-adhesion water-proof coating |
| CN104479508A (en) * | 2014-12-24 | 2015-04-01 | 湖州南浔双林振森实木加工厂 | Preparation method of corrosion-resistant flame-retardant paint |
Non-Patent Citations (1)
| Title |
|---|
| 刘万生主编: "《无机非金属材料概论》", 31 December 1996, 武汉工业大学出版社 * |
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Application publication date: 20161026 |
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