CN106046807A - High heat stability precision casting wax and preparation method thereof - Google Patents
High heat stability precision casting wax and preparation method thereof Download PDFInfo
- Publication number
- CN106046807A CN106046807A CN201610444343.6A CN201610444343A CN106046807A CN 106046807 A CN106046807 A CN 106046807A CN 201610444343 A CN201610444343 A CN 201610444343A CN 106046807 A CN106046807 A CN 106046807A
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- parts
- wax
- casting wax
- weight
- thermal stability
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/06—Waxes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22C—FOUNDRY MOULDING
- B22C7/00—Patterns; Manufacture thereof so far as not provided for in other classes
- B22C7/02—Lost patterns
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses high heat stability precision casting wax which is prepared by following raw materials, in parts by weight: 10-16 parts of microcrystalline wax, 9-12 parts of terpene resin, 6-10 parts of ethylene-vinyl alcohol copolymer, 10-15 parts of carnauba wax, 18-25 parts of paraffin, 5-12 parts of candelilla wax, 4-6 parts of 1,3-oxazacyclohexane, 2-3 parts of zinc stearate, 3-6 parts of xylene, 3-7 parts of lauryl sodium sulfate, 12-16 parts of triethanolamine, 20-25 parts of water glass, 12-15 parts of silica sol, 8-16 parts of quartz powder, 5-9 parts of wetting agents and 12-15 parts of antifoaming agents. The casting wax is high in heat stability, moderate in softening point, low in linear shrinkage rate, high in bending strength and capable of effectively meeting the requirements of precision castings for high dimensional accuracy and surface quality.
Description
Technical field
The present invention relates to wax-pattern production technical field, be specifically related to a kind of high thermal stability hot investment casting wax-pattern material and system thereof
Preparation Method.
Background technology
Model casting is also known as precision-investment casting, and it is a kind of near net-shaped liquid metal moulding process, applies this technique
And each foundry goods obtained is jointly to cooperate comprehensive result through working procedures, multiple material, multiple technologies.Model casting is
Repeat several layers of fireproof coating in dip-coating on the surface of solubility mould, and through successively sanding, be dried and after hardening, with steam and hot water
Etc. heating means, molten for fusible pattern therein going is made overall shell, then carry out high-temperature roasting, cast and obtain the one of foundry goods
Plant casting method.Owing to the size of foundry goods is accurate obtained by this way, corner angle clear, smooth surface, close to zero suspension member
Final form, thus be a kind of Near net shape casting process, therefore be also called hot investment casting.
In model casting, when wax component is injected in mould, there is a defect always.In general, wax component needs
At high temperature become the preferable liquid of mobility, thus be beneficial to its every nook and cranny being filled into required casting object, at pressure
Under effect, this mobility is enhanced.Therefore, it is necessary to wax become completely liquid and be filled into ceramic die each
Time point keeps heated condition.But, when wax is injected in the complex model of zones of different thickness, due to heat stability not
Height, different-thickness region will be with different rate of temperature fall coolings.As suspected, thin region cooling is relatively fast, thick
Region cooling is relatively slow.Therefore, thin region can be to produce to have high-precision specific region.By contrast, thicker region
Wax will cooling time have the trend of contraction to cause dimensional accuracy the highest, since it is desired that manufacture object be an accurate duplication
Wax-pattern.Additionally, because the different cooling in the region of Bao Hehou and contraction, suitable pressure joins in injection wax-pattern, when
During removal mould, model may distort to alleviate pressure.
Summary of the invention
It is desirable to provide a kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof.
The present invention provides following technical scheme:
A kind of high thermal stability hot investment casting wax-pattern material, it is made up of the raw material of following parts by weight: microwax 10-16
Part, terpene resin 9-12 part, ethylene-vinyl alcohol copolymer 6-10 part, Brazil wax 10-15 part, paraffin 18-25 part, little candle
Vegetable wax 5-12 part, 1,3-oxaza hexamethylene 4-6 part, zinc stearate 2-3 part, dimethylbenzene 3-6 part, sodium lauryl sulphate 3-
7 parts, triethanolamine 12-16 part, waterglass 20-25 part, Ludox 12-15 part, silica flour 8-16 part, wetting agent 5-9 part, froth breaking
Agent 12-15 part.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin,
Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added
Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking
Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability
The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
Compared with prior art, the invention has the beneficial effects as follows: it is higher that the present invention casts wax-pattern heat stability, softening point is fitted
In, linear shrinkage ratio is less, and bending strength is bigger, it is possible to meet wanting of precision casting high dimensional accuracy and great surface quality well
Ask.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
1 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite
10 parts of wax, terpene resin 9 parts, ethylene-vinyl alcohol copolymer 6 parts, Brazil wax 10 parts, 18 parts of paraffin, candelilla wax 5 parts,
1,3-oxaza hexamethylene 4 parts, zinc stearate 2 parts, dimethylbenzene 3 parts, sodium lauryl sulphate 3 parts, triethanolamine 12 parts, water
20 parts of glass, Ludox 12 parts, silica flour 8 parts, wetting agent 5 parts, defoamer 12 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin,
Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added
Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking
Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability
The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
2 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite
16 parts of wax, terpene resin 12 parts, ethylene-vinyl alcohol copolymer 10 parts, Brazil wax 15 parts, 25 parts of paraffin, candelilla wax 12
Part, 1,3-oxaza hexamethylene 6 parts, zinc stearate 3 parts, dimethylbenzene 6 parts, sodium lauryl sulphate 7 parts, triethanolamine 16
Part, waterglass 25 parts, Ludox 15 parts, silica flour 16 parts, wetting agent 9 parts, defoamer 15 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin,
Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added
Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking
Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability
The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
3 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite
13 parts of wax, terpene resin 11 parts, ethylene-vinyl alcohol copolymer 9 parts, Brazil wax 12 parts, 22 parts of paraffin, candelilla wax 8 parts,
1,3-oxaza hexamethylene 5 parts, zinc stearate 3 parts, dimethylbenzene 5 parts, sodium lauryl sulphate 4 parts, triethanolamine 14 parts, water
22 parts of glass, Ludox 14 parts, silica flour 12 parts, wetting agent 8 parts, defoamer 14 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin,
Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added
Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking
Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability
The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
It is obvious to a person skilled in the art that the invention is not restricted to the details of described one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described explanation limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.Moreover, it will be appreciated that although this specification is been described by according to embodiment, but the most each
Embodiment only comprises an independent technical scheme, and this narrating mode of description is only for clarity sake, this area
Description should can also be formed this through appropriately combined as an entirety, the technical scheme in each embodiment by technical staff
Skilled person may be appreciated other embodiments.
Claims (4)
1. a high thermal stability hot investment casting wax-pattern material, it is characterised in that it is made up of the raw material of following parts by weight: micro-
Brilliant wax 10-16 part, terpene resin 9-12 part, ethylene-vinyl alcohol copolymer 6-10 part, Brazil wax 10-15 part, paraffin 18-
25 parts, candelilla wax 5-12 part, 1,3-oxaza hexamethylene 4-6 part, zinc stearate 2-3 part, dimethylbenzene 3-6 part, dodecane
Base sodium sulfate 3-7 part, triethanolamine 12-16 part, waterglass 20-25 part, Ludox 12-15 part, silica flour 8-16 part, wetting agent
5-9 part, defoamer 12-15 part.
2. high thermal stability hot investment casting wax-pattern material as claimed in claim 1 and preparation method thereof, it is characterised in that bag
Include following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, little candle
Vegetable wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) add in fused mass obtained above the zinc stearate of described parts by weight, dimethylbenzene, sodium lauryl sulphate and
Triethanolamine is stirred, and then proceedes to be heated to 125 DEG C and be passed through noble gas, obtains fused matter;
(3) by above-mentioned fused matter adds the waterglass of described parts by weight, Ludox, silica flour, wetting agent, defoamer, stir
It is cooled to 65-70 DEG C after mixing uniformly, filters with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high thermal stability
Hot investment casting wax-pattern.
A kind of high thermal stability hot investment casting wax-pattern material the most according to claim 1 and 2 and preparation method thereof, its feature exists
In: in described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
A kind of high thermal stability hot investment casting wax-pattern material the most according to claim 1 and 2 and preparation method thereof, its feature exists
In: the noble gas being passed through in described step (2) is helium or argon.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106914587A (en) * | 2017-01-10 | 2017-07-04 | 浙江美德光学有限公司 | A kind of processing technology of precision-investment casting housing |
CN107325566A (en) * | 2017-07-05 | 2017-11-07 | 天长市兴宇铸造有限公司 | A kind of train wheel node seat casting waxed Preparation Method of hot investment casting |
CN107337930A (en) * | 2017-08-12 | 2017-11-10 | 合肥市田源精铸有限公司 | The preparation of wax material and dewaxing technique in a kind of precision-investment casting |
CN108031792A (en) * | 2018-01-10 | 2018-05-15 | 芜湖市金贸流体科技股份有限公司 | A kind of cured material of silica sol precision casting and the mold making process based on the wax material |
CN115505274A (en) * | 2022-11-07 | 2022-12-23 | 常德市汉鼎精铸技术服务有限公司 | Formula and application process of medium-temperature environment-friendly casting wax |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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GB1403112A (en) * | 1972-05-05 | 1975-08-13 | Trw Inc | Pattern compositions for investment casting |
CN103934416A (en) * | 2014-04-11 | 2014-07-23 | 安徽霍山科皖特种铸造有限责任公司 | Method for producing precise stainless steel casting by sodium silicate shell making |
CN104759587A (en) * | 2015-03-31 | 2015-07-08 | 东莞理工学院 | Precision casting wax die material and preparation method thereof |
CN105522106A (en) * | 2015-12-15 | 2016-04-27 | 铜陵铜官府文化创意股份公司 | Cast wax mould with heat stability and preparation method thereof |
-
2016
- 2016-06-20 CN CN201610444343.6A patent/CN106046807A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1403112A (en) * | 1972-05-05 | 1975-08-13 | Trw Inc | Pattern compositions for investment casting |
CN103934416A (en) * | 2014-04-11 | 2014-07-23 | 安徽霍山科皖特种铸造有限责任公司 | Method for producing precise stainless steel casting by sodium silicate shell making |
CN104759587A (en) * | 2015-03-31 | 2015-07-08 | 东莞理工学院 | Precision casting wax die material and preparation method thereof |
CN105522106A (en) * | 2015-12-15 | 2016-04-27 | 铜陵铜官府文化创意股份公司 | Cast wax mould with heat stability and preparation method thereof |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106914587A (en) * | 2017-01-10 | 2017-07-04 | 浙江美德光学有限公司 | A kind of processing technology of precision-investment casting housing |
CN107325566A (en) * | 2017-07-05 | 2017-11-07 | 天长市兴宇铸造有限公司 | A kind of train wheel node seat casting waxed Preparation Method of hot investment casting |
CN107337930A (en) * | 2017-08-12 | 2017-11-10 | 合肥市田源精铸有限公司 | The preparation of wax material and dewaxing technique in a kind of precision-investment casting |
CN108031792A (en) * | 2018-01-10 | 2018-05-15 | 芜湖市金贸流体科技股份有限公司 | A kind of cured material of silica sol precision casting and the mold making process based on the wax material |
CN115505274A (en) * | 2022-11-07 | 2022-12-23 | 常德市汉鼎精铸技术服务有限公司 | Formula and application process of medium-temperature environment-friendly casting wax |
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Application publication date: 20161026 |