CN106046807A - High heat stability precision casting wax and preparation method thereof - Google Patents

High heat stability precision casting wax and preparation method thereof Download PDF

Info

Publication number
CN106046807A
CN106046807A CN201610444343.6A CN201610444343A CN106046807A CN 106046807 A CN106046807 A CN 106046807A CN 201610444343 A CN201610444343 A CN 201610444343A CN 106046807 A CN106046807 A CN 106046807A
Authority
CN
China
Prior art keywords
parts
wax
casting wax
weight
thermal stability
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610444343.6A
Other languages
Chinese (zh)
Inventor
李俊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Yian Precision Machinery Parts Co Ltd
Original Assignee
Anhui Yian Precision Machinery Parts Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Yian Precision Machinery Parts Co Ltd filed Critical Anhui Yian Precision Machinery Parts Co Ltd
Priority to CN201610444343.6A priority Critical patent/CN106046807A/en
Publication of CN106046807A publication Critical patent/CN106046807A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L91/00Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • C08L91/06Waxes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22CFOUNDRY MOULDING
    • B22C7/00Patterns; Manufacture thereof so far as not provided for in other classes
    • B22C7/02Lost patterns
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

The invention discloses high heat stability precision casting wax which is prepared by following raw materials, in parts by weight: 10-16 parts of microcrystalline wax, 9-12 parts of terpene resin, 6-10 parts of ethylene-vinyl alcohol copolymer, 10-15 parts of carnauba wax, 18-25 parts of paraffin, 5-12 parts of candelilla wax, 4-6 parts of 1,3-oxazacyclohexane, 2-3 parts of zinc stearate, 3-6 parts of xylene, 3-7 parts of lauryl sodium sulfate, 12-16 parts of triethanolamine, 20-25 parts of water glass, 12-15 parts of silica sol, 8-16 parts of quartz powder, 5-9 parts of wetting agents and 12-15 parts of antifoaming agents. The casting wax is high in heat stability, moderate in softening point, low in linear shrinkage rate, high in bending strength and capable of effectively meeting the requirements of precision castings for high dimensional accuracy and surface quality.

Description

A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof
Technical field
The present invention relates to wax-pattern production technical field, be specifically related to a kind of high thermal stability hot investment casting wax-pattern material and system thereof Preparation Method.
Background technology
Model casting is also known as precision-investment casting, and it is a kind of near net-shaped liquid metal moulding process, applies this technique And each foundry goods obtained is jointly to cooperate comprehensive result through working procedures, multiple material, multiple technologies.Model casting is Repeat several layers of fireproof coating in dip-coating on the surface of solubility mould, and through successively sanding, be dried and after hardening, with steam and hot water Etc. heating means, molten for fusible pattern therein going is made overall shell, then carry out high-temperature roasting, cast and obtain the one of foundry goods Plant casting method.Owing to the size of foundry goods is accurate obtained by this way, corner angle clear, smooth surface, close to zero suspension member Final form, thus be a kind of Near net shape casting process, therefore be also called hot investment casting.
In model casting, when wax component is injected in mould, there is a defect always.In general, wax component needs At high temperature become the preferable liquid of mobility, thus be beneficial to its every nook and cranny being filled into required casting object, at pressure Under effect, this mobility is enhanced.Therefore, it is necessary to wax become completely liquid and be filled into ceramic die each Time point keeps heated condition.But, when wax is injected in the complex model of zones of different thickness, due to heat stability not Height, different-thickness region will be with different rate of temperature fall coolings.As suspected, thin region cooling is relatively fast, thick Region cooling is relatively slow.Therefore, thin region can be to produce to have high-precision specific region.By contrast, thicker region Wax will cooling time have the trend of contraction to cause dimensional accuracy the highest, since it is desired that manufacture object be an accurate duplication Wax-pattern.Additionally, because the different cooling in the region of Bao Hehou and contraction, suitable pressure joins in injection wax-pattern, when During removal mould, model may distort to alleviate pressure.
Summary of the invention
It is desirable to provide a kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof.
The present invention provides following technical scheme:
A kind of high thermal stability hot investment casting wax-pattern material, it is made up of the raw material of following parts by weight: microwax 10-16 Part, terpene resin 9-12 part, ethylene-vinyl alcohol copolymer 6-10 part, Brazil wax 10-15 part, paraffin 18-25 part, little candle Vegetable wax 5-12 part, 1,3-oxaza hexamethylene 4-6 part, zinc stearate 2-3 part, dimethylbenzene 3-6 part, sodium lauryl sulphate 3- 7 parts, triethanolamine 12-16 part, waterglass 20-25 part, Ludox 12-15 part, silica flour 8-16 part, wetting agent 5-9 part, froth breaking Agent 12-15 part.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
Compared with prior art, the invention has the beneficial effects as follows: it is higher that the present invention casts wax-pattern heat stability, softening point is fitted In, linear shrinkage ratio is less, and bending strength is bigger, it is possible to meet wanting of precision casting high dimensional accuracy and great surface quality well Ask.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all Belong to the scope of protection of the invention.
1 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite 10 parts of wax, terpene resin 9 parts, ethylene-vinyl alcohol copolymer 6 parts, Brazil wax 10 parts, 18 parts of paraffin, candelilla wax 5 parts, 1,3-oxaza hexamethylene 4 parts, zinc stearate 2 parts, dimethylbenzene 3 parts, sodium lauryl sulphate 3 parts, triethanolamine 12 parts, water 20 parts of glass, Ludox 12 parts, silica flour 8 parts, wetting agent 5 parts, defoamer 12 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
2 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite 16 parts of wax, terpene resin 12 parts, ethylene-vinyl alcohol copolymer 10 parts, Brazil wax 15 parts, 25 parts of paraffin, candelilla wax 12 Part, 1,3-oxaza hexamethylene 6 parts, zinc stearate 3 parts, dimethylbenzene 6 parts, sodium lauryl sulphate 7 parts, triethanolamine 16 Part, waterglass 25 parts, Ludox 15 parts, silica flour 16 parts, wetting agent 9 parts, defoamer 15 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
3 one kinds of high thermal stability hot investment casting wax-pattern material of embodiment, it is made up of the raw material of following parts by weight: crystallite 13 parts of wax, terpene resin 11 parts, ethylene-vinyl alcohol copolymer 9 parts, Brazil wax 12 parts, 22 parts of paraffin, candelilla wax 8 parts, 1,3-oxaza hexamethylene 5 parts, zinc stearate 3 parts, dimethylbenzene 5 parts, sodium lauryl sulphate 4 parts, triethanolamine 14 parts, water 22 parts of glass, Ludox 14 parts, silica flour 12 parts, wetting agent 8 parts, defoamer 14 parts.
A kind of high thermal stability hot investment casting wax-pattern material and preparation method thereof, comprises the following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, Candelilla wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) in fused mass obtained above, the zinc stearate of described parts by weight, dimethylbenzene, lauryl sulphate acid are added Sodium and triethanolamine are stirred, and then proceed to be heated to 125 DEG C and be passed through noble gas, obtain fused matter;
(3) above-mentioned fused matter will add the waterglass of described parts by weight, Ludox, silica flour, wetting agent, froth breaking Agent, is cooled to 65-70 DEG C after stirring, filter with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high heat stability The hot investment casting wax-pattern of property.
In described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
The noble gas being passed through in described step (2) is helium or argon.
It is obvious to a person skilled in the art that the invention is not restricted to the details of described one exemplary embodiment, Er Qie In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires rather than described explanation limits, it is intended that all by fall in the implication of equivalency and scope of claim Change is included in the present invention.Moreover, it will be appreciated that although this specification is been described by according to embodiment, but the most each Embodiment only comprises an independent technical scheme, and this narrating mode of description is only for clarity sake, this area Description should can also be formed this through appropriately combined as an entirety, the technical scheme in each embodiment by technical staff Skilled person may be appreciated other embodiments.

Claims (4)

1. a high thermal stability hot investment casting wax-pattern material, it is characterised in that it is made up of the raw material of following parts by weight: micro- Brilliant wax 10-16 part, terpene resin 9-12 part, ethylene-vinyl alcohol copolymer 6-10 part, Brazil wax 10-15 part, paraffin 18- 25 parts, candelilla wax 5-12 part, 1,3-oxaza hexamethylene 4-6 part, zinc stearate 2-3 part, dimethylbenzene 3-6 part, dodecane Base sodium sulfate 3-7 part, triethanolamine 12-16 part, waterglass 20-25 part, Ludox 12-15 part, silica flour 8-16 part, wetting agent 5-9 part, defoamer 12-15 part.
2. high thermal stability hot investment casting wax-pattern material as claimed in claim 1 and preparation method thereof, it is characterised in that bag Include following steps:
(1) by the microwax of described parts by weight, terpene resin, ethylene-vinyl alcohol copolymer, Brazil wax, paraffin, little candle Vegetable wax and 1,3-oxaza hexamethylene carries out heat treatment with prepared fused mass;
(2) add in fused mass obtained above the zinc stearate of described parts by weight, dimethylbenzene, sodium lauryl sulphate and Triethanolamine is stirred, and then proceedes to be heated to 125 DEG C and be passed through noble gas, obtains fused matter;
(3) by above-mentioned fused matter adds the waterglass of described parts by weight, Ludox, silica flour, wetting agent, defoamer, stir It is cooled to 65-70 DEG C after mixing uniformly, filters with prepared casting wax;
(4) by the described casting wax obtained heat, then in model moulding, cooling with prepare described in there is high thermal stability Hot investment casting wax-pattern.
A kind of high thermal stability hot investment casting wax-pattern material the most according to claim 1 and 2 and preparation method thereof, its feature exists In: in described step (1), heat treatment temperature is 95-110 DEG C, and heat treatment time is 40-45min.
A kind of high thermal stability hot investment casting wax-pattern material the most according to claim 1 and 2 and preparation method thereof, its feature exists In: the noble gas being passed through in described step (2) is helium or argon.
CN201610444343.6A 2016-06-20 2016-06-20 High heat stability precision casting wax and preparation method thereof Pending CN106046807A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610444343.6A CN106046807A (en) 2016-06-20 2016-06-20 High heat stability precision casting wax and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610444343.6A CN106046807A (en) 2016-06-20 2016-06-20 High heat stability precision casting wax and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106046807A true CN106046807A (en) 2016-10-26

Family

ID=57168694

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610444343.6A Pending CN106046807A (en) 2016-06-20 2016-06-20 High heat stability precision casting wax and preparation method thereof

Country Status (1)

Country Link
CN (1) CN106046807A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106914587A (en) * 2017-01-10 2017-07-04 浙江美德光学有限公司 A kind of processing technology of precision-investment casting housing
CN107325566A (en) * 2017-07-05 2017-11-07 天长市兴宇铸造有限公司 A kind of train wheel node seat casting waxed Preparation Method of hot investment casting
CN107337930A (en) * 2017-08-12 2017-11-10 合肥市田源精铸有限公司 The preparation of wax material and dewaxing technique in a kind of precision-investment casting
CN108031792A (en) * 2018-01-10 2018-05-15 芜湖市金贸流体科技股份有限公司 A kind of cured material of silica sol precision casting and the mold making process based on the wax material
CN115505274A (en) * 2022-11-07 2022-12-23 常德市汉鼎精铸技术服务有限公司 Formula and application process of medium-temperature environment-friendly casting wax

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1403112A (en) * 1972-05-05 1975-08-13 Trw Inc Pattern compositions for investment casting
CN103934416A (en) * 2014-04-11 2014-07-23 安徽霍山科皖特种铸造有限责任公司 Method for producing precise stainless steel casting by sodium silicate shell making
CN104759587A (en) * 2015-03-31 2015-07-08 东莞理工学院 Precision casting wax die material and preparation method thereof
CN105522106A (en) * 2015-12-15 2016-04-27 铜陵铜官府文化创意股份公司 Cast wax mould with heat stability and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1403112A (en) * 1972-05-05 1975-08-13 Trw Inc Pattern compositions for investment casting
CN103934416A (en) * 2014-04-11 2014-07-23 安徽霍山科皖特种铸造有限责任公司 Method for producing precise stainless steel casting by sodium silicate shell making
CN104759587A (en) * 2015-03-31 2015-07-08 东莞理工学院 Precision casting wax die material and preparation method thereof
CN105522106A (en) * 2015-12-15 2016-04-27 铜陵铜官府文化创意股份公司 Cast wax mould with heat stability and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106914587A (en) * 2017-01-10 2017-07-04 浙江美德光学有限公司 A kind of processing technology of precision-investment casting housing
CN107325566A (en) * 2017-07-05 2017-11-07 天长市兴宇铸造有限公司 A kind of train wheel node seat casting waxed Preparation Method of hot investment casting
CN107337930A (en) * 2017-08-12 2017-11-10 合肥市田源精铸有限公司 The preparation of wax material and dewaxing technique in a kind of precision-investment casting
CN108031792A (en) * 2018-01-10 2018-05-15 芜湖市金贸流体科技股份有限公司 A kind of cured material of silica sol precision casting and the mold making process based on the wax material
CN115505274A (en) * 2022-11-07 2022-12-23 常德市汉鼎精铸技术服务有限公司 Formula and application process of medium-temperature environment-friendly casting wax

Similar Documents

Publication Publication Date Title
CN106046807A (en) High heat stability precision casting wax and preparation method thereof
CN100506428C (en) Method for direct production of core in narrow groove and blind hole of wax mould
CN104759587B (en) A kind of hot investment casting wax-pattern material and preparation method thereof
CN110252958B (en) Blade casting mold preparation method for inhibiting edge plate mixed crystals based on hollow/porous structure
CN104001857A (en) Guide blade of gas turbine and precise casting technique of guide blade
CN104690256A (en) Directional solidification method for controlling foreign crystal defects of nickel-base superalloy step cast
CN105945226B (en) A kind of method for making metal filigree
CN108015231A (en) A kind of investment precision casting technology
CN105732014A (en) Silicon-based ceramic core preparation method
CN110732637A (en) turbine blade air film hole precision forming method
CN104399891A (en) Casting method combining investment precise shell-making process with vacuum suction molding technology
CN102672104A (en) Precision casting method for pouring evanescent mold through high-performance coating foam and mold laminating paraffin
CN101524739A (en) Precision-investment casting method
CN105057593A (en) Investment casting technology for copper alloy casting
CN109396349A (en) A kind of investment precision casting technology of small thin-wall
CN105907107A (en) Precision casting concocted wax and treatment process
CN106077472A (en) A kind of hot investment casting moulding process of foundry goods
CN108031792A (en) A kind of cured material of silica sol precision casting and the mold making process based on the wax material
CN109773124A (en) A kind of francis turbine runner integral casting process
CN104550719A (en) Ice mold based investment casting technology
CN109365749A (en) Precision-investment manufactures vacuum-thermoform production technology
CN110842145A (en) 3D printing wax pattern dust-free dewaxing method
CN108889924B (en) Short-flow precision casting method for ferromagnetic alloy vacuum casting
CN108997761A (en) A kind of precision-investment casting rosin basic mode material and preparation method thereof
CN104550735A (en) Precision casting method of last stage extra-long guide blade for million-kilowatt nuclear power unit

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20161026