CN106040139B - A kind of reaction kettle - Google Patents
A kind of reaction kettle Download PDFInfo
- Publication number
- CN106040139B CN106040139B CN201610491215.7A CN201610491215A CN106040139B CN 106040139 B CN106040139 B CN 106040139B CN 201610491215 A CN201610491215 A CN 201610491215A CN 106040139 B CN106040139 B CN 106040139B
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- CN
- China
- Prior art keywords
- reaction kettle
- agitating device
- lifting
- kettle body
- input end
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
Abstract
The invention discloses a kind of reaction kettles detachably filtered, including reaction kettle body, the reaction kettle body include upper reaction kettle body, the lower reaction kettle body being connected with the upper reaction kettle body, the first sealing ring for sealing and the second sealing ring, be located on the reaction kettle body for the negative-pressure cyclic filter device that is filtered to raw material, the negative-pressure cyclic filter device includes the first filter device being connected with motor and the second filter device being connected with first filter device.The reaction kettle of the present invention carries filter device, reaction kettle can be divided into two, reaction kettle carries filter device, just the impurity in raw material can be filtered before raw material is chemically reacted, it is simple and convenient, so that product obtained by the reaction is purer, reaction kettle is divided into two, and has both facilitated the cleaning that the chemicrystallization on kettle wall is remained in after repeatedly reacting reaction kettle, is also more conducive to and cleans up.
Description
Technical field
The present invention relates to technical field of chemical, more specifically to a kind of reaction kettle.
Background technology
Chemical liquid reaction kettle generally comprises autoclave body and stirring system, is equipped with charge door at the top of autoclave body, autoclave body bottom is equipped with
Drain hole, stirring system include the motor being arranged at the top of autoclave body and are arranged at the in vivo blender of kettle, and blender includes stirring
Shaft and agitating vane, stirring shaft are connected with motor, and agitating vane is fixedly connected with stirring shaft;Impurity in raw material is such as
Some Solid-state Chemistry particles can also participate in reacting, and both waste raw material, and generate other products, with the product for planning to obtain
Be not inconsistent or raw material in impurity be not involved in reacting, but react after product in adulterate impurity, leverage the matter of product
Amount in addition, after reaction kettle is used for multiple times, can accumulate certain chemicrystallization, traditional reaction kettle is only on the kettle wall of reaction kettle
It can be cleaned by a some holes such as feed inlet on kettle wall, and clean inconvenience, not washed clean clearly, in addition, blender exists
To that during liquid agitation, can generate whirlpool clockwise or counterclockwise in autoclave body, in autoclave body the rotation of liquid runs down whirlpool mixed,
But mixed along whirlpool rotation, this mixed method inefficiency, and when the various liquid reactions in autoclave body need one
During fixed temperature, being mixed along whirlpool rotation can also make the fluid temperature of each area uneven, influence the reaction of liquid.
The content of the invention
Simple in structure the object of the present invention is to provide a kind of reaction kettle, easily manufactured, work efficiency is high, what is used
It stirs in the process more fully, evenly, the product obtained after reaction is purer for fluid temperature, and when cleaning is more convenient effectively.
The present invention above-mentioned technical purpose technical scheme is that:A kind of reaction kettle, including reaction
Autoclave body, be located on the reaction kettle body for the negative-pressure cyclic filter device of filtered fluid raw material, for stirring the reaction
The rotation and lifting agitating device of liquid is with main agitating device and for installing the rotation and lifting agitating device and master in autoclave body
Mounting bracket needed for agitating device.
The reaction kettle body includes upper reaction kettle body, is connected with the upper reaction kettle body lower reaction kettle body, for sealing
The first sealing ring and the second sealing ring.
Preferably, first sealing ring includes the first sealing ring cylindrical ring body, is located at the first sealing ring cylinder
The elastic tiltedly protrusion of multiple bar shapeds in ring body, the protruded connecting members for connecting the oblique protrusion of adjacent bar elasticity, described first
Tiltedly protrusion and the protruded connecting members are integrally formed for sealing ring cylindrical ring body, bar shaped elasticity, the adjacent bar shaped elasticity
The first cavity is tiltedly formed between protrusion and the protruded connecting members three, first cavity is equipped with the first of elastically deformable
Auxiliary seal body, bar shaped elasticity are tiltedly equipped with the oblique elastic cavity along the oblique protrusion extending direction of bar shaped elasticity in protrusion.
Preferably, first filter device includes being located at the rotation that the motor above autoclave body is connected with the motor
Whipping filter screen, the impurity collecting box for being located at the rotation whipping filtering sieve bottom, be fixedly connected on autoclave body for storing
The outlet at bottom that the rotation whipping filter screen throws away the liquid holding tank of liquid and is located at the liquid holding tank bottom, institute
Rotation whipping filter screen is stated to be arranged on inside the liquid holding tank and can take out from the liquid holding tank.
Preferably, the adjacent bar shaped elasticity tiltedly protrusion projection section overlapping in the horizontal direction.
Preferably, the first auxiliary seal body includes the elastic thin-wall of elastically deformable and the elastic thin-wall encloses
Into annular seal space, the oblique elastic cavity communicates with the annular seal space, full of working fluid in the annular seal space, is set in working fluid
There are microspheres, plastic grain.
Preferably, second sealing ring includes sealing ring main body, the multiple arches being arranged in the sealing ring main body
Shape seal protuberance, the elastic sealing element being coated in the arch seal protuberance, the arch seal protuberance and the elasticity are close
Elastic cavity is formed between sealing, the elastic cavity is equipped with multiple elastic pearls, forms cavity between the adjacent elastic sealing element, institute
It states and prolongs the cavity wall in cavity equipped with auxiliary sealing member.
Preferably, the elastic sealing element includes the first lower seals for being connected with sealing ring main body and described the
One lower seals connection First Transition sealing element and the First Transition sealing element connection and contacted with reaction kettle body
Squeeze sealing member and squeeze sealing member connection the second transition seal and by second transition seal and institute
State the second lower seals that sealing ring main body connects, first lower seals, the First Transition sealing element, institute
Squeeze sealing member, second transition seal and second lower seals are stated to be integrally formed.
Preferably, the First Transition sealing element is equipped with multiple sealing latches, the First Transition sealing element is equipped with
Multiple sealing card slots with the sealing latch cooperation.
Preferably, the cavity wall of the cavity is inwardly collapsed with away from sealing ring kernel of section.
The negative-pressure cyclic filter device includes the first filter device being connected with motor and is filled with the described first filtering
Put the second filter device of connection;What the motor that first filter device includes being located above autoclave body was connected with the motor
Rotation whipping filter screen, the impurity collecting box for being located at the rotation whipping filtering sieve bottom are fixedly connected on autoclave body and are used for
The rotation whipping filter screen is stored to throw away the liquid holding tank of liquid and be located at the bottom of the liquid holding tank bottom
Mouthful, the rotation whipping filter screen is arranged on inside the liquid holding tank and can be taken out from the liquid holding tank.
Preferably, the liquid holding tank is provided with autoclave body junction facilitates the rotation whipping filter screen from described
The hole taken out in liquid holding tank.
Preferably, the rotation whipping filter screen includes the connecting shaft connected with the motor, is fixedly connected on the company
Cylinder type filter net in spindle and be set in outside the connecting shaft and with the raw material that the cylinder type filter net communicates into
Enter passage, the cylinder type filter net is evenly distributed with filter hole, and the cylinder type filter net does not have adhesiveness.
Preferably, the liquid holding tank lower end is in funnel-form.
Preferably, the impurity collecting box includes a collection entrance collapsed downwards.
Preferably, second filter device includes liquid inlet tee joint pipe, goes out liquid threeway pipe, filtration members, negative pressure device, described
Liquid inlet tee joint pipe include input end a, input end b and port of export a, the goes out liquid threeway pipe include input end c, port of export b with
And port of export c, the input end a are connected with the outlet at bottom, the filtration members be located at the port of export a and input end c it
Between, the negative pressure device is located between the port of export b and the input end b, the outlet at bottom, the input end a, described
Port of export a, the filtration members, the input end c and the port of export c form passage by pipeline and note the raw material after filtering
Enter in the reaction kettle body, the input end b, the port of export a, the filtration members, the input end c, the port of export b with
And the negative pressure device forms negative-pressure cyclic filtration channel by pipeline.
Preferably, the filtration members include filtering body, the filter chamber being located inside the filtering body, are located at the filter chamber
In filter screen and the impurity discharging device for being used for the impurity for being filtered down the filter screen and discharging that is communicated with the filter chamber.
Preferably, the negative pressure device includes negative pressure body, the negative pressure cavity being located inside the negative pressure body, is located at the negative pressure
Aspiration pump on body.
The rotation and lifting agitating device is stirred including the first lifting agitating device, the second lifting agitating device, the 3rd lifting
Mix device and the 4th lifting agitating device.
Preferably, the first lifting agitating device, the second lifting agitating device, the 3rd lifting stirring dress
It puts and the 4th lifting agitating device has identical structure, the first lifting agitating device is stirred with the described 3rd lifting
Mix device synchronization lifting, the second lifting agitating device and the described 4th lifting agitating device synchronization lifting, described first liter
Agitating device and the described second lifting asynchronous lifting of agitating device drop.
Preferably, the main agitating device includes the main agitating shaft connected with motor, is located on the main agitating shaft
Paddle and the drive bevel gear being located on main agitating shaft.
Preferably, the first lifting agitating device includes be sequentially connected with drive bevel gear first from mantle tooth
Wheel, for fixing the first driven wheel of differential rotating shaft of the first driven wheel of differential, be fixedly connected on first driven wheel of differential
The first driving pulley on rotating shaft, by the first driven pulley that the first driving pulley drives, to be hinged on described first driven
Among hinged the first intermediate active connecting rod and described first of the first pivoted link and first pivoted link on belt wheel
The first hinged elevating mechanism of movable rod and the first driven pulley rotating shaft being fixedly connected with first driven pulley.
Preferably, first elevating mechanism is equipped with successively from inside to outside and the first intermediate active connecting rod is hinged
First screw rod, the first spiral lifting stirring axle sleeve and the first guideway being fixedly connected with reaction kettle.
Preferably, first screw rod, the first spiral lifting stirring axle sleeve and the first guideway three are coaxial
The heart, the first spiral rod outer surface are equipped with external screw thread a, and first guideway is equipped with internal thread a, the first spiral liter
Drop stirring axle sleeve inner surface is equipped with and the first screw rod external screw thread matched lifting stirring axle sleeve internal thread b, and described the
The lifting stirring axle sleeve external screw thread that one spiral lifting stirring sleeve outer surface is equipped with and the first guideway internal thread is spirally connected
b。
In conclusion the invention has the advantages that:
Its is simple in structure, easily manufactured, and work efficiency is high, is stirred during use more fully, fluid temperature is more equal
Even, the product obtained after reaction is purer, and when cleaning is more convenient effectively.
Description of the drawings
Fig. 1 is the structure diagram of the present invention-while Figure of abstract;
Fig. 2 is rotation and lifting agitating device and main agitating device position relationship schematic diagram;
Fig. 3 is the structure diagram of the first lifting agitating device of the present invention;
Fig. 4 is the structure diagram of the first elevating mechanism of the present invention;
Fig. 5 is sectional view at A-A in Fig. 4;
Fig. 6 is the schematic cross-sectional view of reaction kettle body;
Fig. 7 is the sectional view of the first sealing ring of the present invention;
Fig. 8 is sectional view at B-B in Fig. 7;
Fig. 9 is the oblique protrusion of bar shaped elasticity perspective view in the horizontal direction;
Figure 10 is the schematic cross-sectional view of the first auxiliary seal body;
Figure 11 is the schematic cross-sectional view of the sealing ring cross section of the second sealing ring
Figure 12 is part-structure schematic diagram in Fig. 1;
Figure 13 is the structure diagram of the negative-pressure cyclic filter device of the present invention;
Figure 14 is the first filter apparatus configuration schematic diagram of the present invention;
Figure 15 is the schematic cross-sectional view of filtration members;
Figure 16 is the schematic cross-sectional view of negative pressure device;
Figure 17 is the partial schematic diagram at D in Figure 11;
Figure 18 is the partial schematic diagram at E in Figure 11.
Specific embodiment
The present invention is described in further detail below in conjunction with attached drawing.
This specific embodiment is only explanation of the invention, is not limitation of the present invention, people in the art
Member can as needed make the present embodiment the modification of no creative contribution after this specification is read, but as long as at this
It is all protected in the right of invention be subject to Patent Law.
Embodiment 1:As shown in Figure 1, Figure 2, Fig. 3, Fig. 4, Fig. 5, Fig. 6, Fig. 7, Fig. 8, Fig. 9, Figure 10, Figure 11, Figure 12, Figure 13, figure
14th, shown in Figure 15, Figure 16, Figure 17, Figure 18, a kind of reaction kettle including reaction kettle body 1, is located on the reaction kettle body 1 and is used for
The negative-pressure cyclic filter device 2 of filtered fluid raw material, the rotation and lifting agitating device for stirring liquid in the reaction kettle body 1
3 with main agitating device 5 and for installing the rotation and lifting agitating device 3 and the mounting bracket 4 needed for main agitating device 5.
The reaction kettle body 1 includes upper reaction kettle body 1a, the lower reaction kettle body 2a being connected with the upper reaction kettle body 1a, use
In the first sealing ring 3a and the second sealing ring 4a of sealing, lower reaction kettle body 2a tops are equipped with the step biased to central shaft,
Step is socketed in by rotation on upper reaction kettle body 1a, and socket place is equipped with the first sealing ring 3a and the second sealing ring 4a.
The first sealing ring 3a includes the first sealing ring cylindrical ring body 301a, is located at the first sealing ring cylindrical ring body
The elastic tiltedly protrusion 302a of multiple bar shapeds on 301a, the protruded connecting members for connecting the oblique protrusion 302a of adjacent bar elasticity
303a, the first sealing ring cylindrical ring body 301a, the oblique protrusion 302a and protruded connecting members 303a of bar shaped elasticity
It is integrally formed, the adjacent bar shaped elasticity tiltedly forms the first cavity between protrusion 302a and the protruded connecting members 303a three
304a, the first cavity 304a are equipped with the first auxiliary seal body 305a of elastically deformable, the oblique protrusion of the bar shaped elasticity
302a is internally provided with the oblique elastic cavity 306a along the oblique protrusion 302a extending directions of bar shaped elasticity;The oblique protrusion of the adjacent bar shaped elasticity
302a projection section overlappings in the horizontal direction so that no matter upper reaction kettle body 1a occurs which kind of with lower reaction kettle body 2a junctions
Small notch or protrusion, tiltedly protrusion 302a can cover the notch or protrusion, the first auxiliary seal body to bar shaped elasticity
The annular seal space 3052a that the elastic thin-wall 3051a and the elastic thin-wall 3051a of 305a including elastically deformable is surrounded, it is described
Oblique elastic cavity 306a is communicated with the annular seal space 3052a, full of flowing in the oblique elastic cavity 306a and annular seal space 3052a
Liquid is equipped with microspheres, plastic grain in working fluid;The setting of working fluid, make bar shaped elasticity tiltedly protrusion 302a with
The elastic deformation of first auxiliary seal body 305a is mutually adjusted, and is finally reached optimal sealing effect.
In this example, the mass percent of the working fluid of the annular seal space 3052a, microspheres and plastic grain
For 98.1%, 0.33%, 1.66%, the working fluid is toluene.
The setting of multiple oblique protrusion 302a of bar shaped elasticity and the setting for being internally provided with oblique elastic cavity 306a, bar shaped bullet
Property oblique protrusion 302a deformed upon to oblique elastic cavity 306a directions, oblique elastic cavity 306a becomes the bullet of the oblique protrusion 302a of bar shaped elasticity
Property buffer zone, and tiltedly protrusion 302a is leaned on into not deforming upon substantially at the first sealing ring cylindrical ring body 301a bar shaped elasticity.
Further, the second sealing ring 4a includes sealing ring main body 401a, is arranged on the sealing ring main body 401a
On multiple arch seal protuberance 402a, the elastic sealing element 403a that is coated on the arch seal protuberance 402a, the arch
Elastic cavity 404a, the elastic cavity 404a are formed between shape seal protuberance 402a and the elastic sealing element 403a and is equipped with multiple bullets
Property pearl 405a, elastic sealing element 403a acts on down by external force and deformed upon, so as to elastic pearl 405a applied forces, elastic pearl 405a
Between interact mutually to adjust and form optimal seal effect, cavity 406a is formed between the adjacent elastic sealing element 403a,
Prolonging the cavity 406a walls in the cavity 406a includes and seals equipped with auxiliary sealing member 407a, the elastic sealing element 403a
The First Transition that first lower seals 403a1 of circle main body 401a connections is connected with the first lower seals 403a1 is close
Sealing 403a2 and the First Transition sealing element 403a2 connections and the squeeze sealing member that is contacted with reaction kettle body 1
The second transition seal 403a4 that 403a3 is connected with the squeeze sealing member 403a3 and by second transition seal
The second lower seals 403a5 that the 403a4 and sealing ring main body 401a is connected, first lower seals
403a1 is consistent and symmetrical compared with squeeze sealing member 403a3 with the second lower seals 403a5 shapes, first mistake
It is consistent and symmetrical compared with squeeze sealing member 403a3 with the second transition seal 403a4 shapes to cross sealing element 403a2, institute
State the first lower seals 403a1, the First Transition sealing element 403a2, the squeeze sealing member 403a3, second mistake
It crosses sealing element 403a4 and the second lower seals 403a5 to be integrally formed, be set on the First Transition sealing element 403a2
There are multiple sealing latch 408a, the second transition seal 403a4 to be equipped with multiple close with the sealing latch 408a cooperations
Card slot 409a is sealed, the sealing latch 408a and sealing card slot 409a is taper.
Further, the cavity wall of the cavity 406a is inwardly collapsed with away from sealing ring kernel of section, first bottom
Profile of the profile of portion sealing element 403a1 and the second lower seals 403a5 with the cavity wall of the cavity 406a
Unanimously, the profile of the First Transition sealing element 403a2 and the second transition seal 403a4 is compared with the cavity 406a
Cavity wall expand outwardly.
Further, the negative-pressure cyclic filter device 2 includes the first filter device 201 and is filled with the described first filtering
Put the second filter device 202 of 201 connections;First filter device 201 includes the motor for being located at 1 top of reaction kettle body
2011 and the motor 2011 connect rotation whipping filter screen 2012, be located at whipping filter screen 2012 bottom of rotating
Impurity collecting box 2013 is fixedly connected on being thrown away for storing the rotation whipping filter screen 2012 on the reaction kettle body 1
The liquid holding tank 2014 of liquid and the outlet at bottom 2015 for being located at 2014 bottom of liquid holding tank, the rotation whipping
Filter screen 2012 is arranged on 2014 inside of liquid holding tank and can be taken out from the liquid holding tank 2014.
Second filter device 202 is located at the left side of the reaction kettle body 1 and is fixedly mounted on institute by profile piece
State on reaction kettle body 1, the motor 2011 is fixedly connected on mounting bracket 4, mounting bracket 4 be profile piece, 2011 He of motor
The rotation whipping filter screen 2012 is connected by shaft coupling.
Further, the liquid holding tank 2014 is provided with 1 junction of reaction kettle body and facilitates the rotation
The hole 20141 that whipping filter screen 2012 takes out from the liquid holding tank 2014, the rotation whipping filter screen 2012 include
The connecting shaft 20121 connected with the motor 2011, the cylinder type filter net 20122 being fixedly connected in the connecting shaft 20121
And it is set in raw material that is outside the connecting shaft 20121 and being communicated with the cylinder type filter net 20122 and enters passage
20123, the cylinder type filter net 20122 is evenly distributed with filter hole, and the cylinder type filter net 20122 does not have adhesiveness.
Further, 2014 lower end of liquid holding tank is in funnel-form, facilitates and is got rid of in the cylinder type filter net 20122
The raw material gone out is more preferably into the second filter device 202.
Further, the impurity collecting box 2013 includes a collection entrance collapsed downwards, the rotation whipping mistake
For strainer 2012 in rotation, impurity enters impurity collecting box 2013 along the collection entrance collapsed downwards, and impurity is into impurity
After collecting box 2013, due to collect entrance collapse downwards, impurity be not easy from impurity collecting box 2013 return to once again it is described rotation get rid of
In dynamic filter screen 2012.
Further, second filter device 202 includes liquid inlet tee joint pipe 2021, goes out liquid threeway pipe 2022, filtration members
2023rd, negative pressure device 2024, the liquid inlet tee joint pipe 2021 include input end a2021a, input end b2021b and the port of export
A2021c, the goes out liquid threeway pipe 2022 include input end c2022a, port of export b2022b and port of export c2022c, it is described into
Mouth end a2021a is connected with the outlet at bottom 2015, and the filtration members 2023 are located at the port of export a2021c and input end
Between c2022a, the negative pressure device 2024 is located between the port of export b2022b and the input end b2021b, the bottom
Portion outlet 2015, the input end a2021a, the port of export a2021c, the filtration members 2023, the input end c2022a
And the port of export c2022c forms passage by pipeline and injects the raw material after filtering in the reaction kettle body 1, it is described into
Mouth end b2021b, the port of export a2021c, the filtration members 2023, the input end c2022a, the port of export b2022b
And the negative pressure device 2024 forms negative-pressure cyclic filtration channel by pipeline.
It is equipped with to adjust the flow control valve of flow, institute at the port of export b2022b and port of export c2022c
It states and check valve is equipped at input end b2021b, check valve control raw material can only flow into the port of export from the negative pressure device 2024
A2021c will not generate adverse current.
Further, the filtration members 2023 include filtering body 20231, the filtering being located inside the filtering body 20231
Chamber 20232, the filter screen 20233 being located in the filter chamber 20232 and and being used for institute of communicating of the filter chamber 20232
State the impurity discharging device 20234 for the impurity discharge that filter screen 20233 is filtered down.
Further, the negative pressure device 2024 includes negative pressure body 20241, is located at bearing inside the negative pressure body 20241
Pressure chamber 20242, the aspiration pump 20243 being located in the negative pressure body 20241, the bottom of negative pressure cavity 20242 are equipped with negative pressure cavity liquid
Import, 20242 side wall of negative pressure cavity be equipped with negative pressure cavity liquid outlet, the height of negative pressure cavity liquid outlet in the vertical direction be higher than into
The height of mouthful end b2021b in the vertical direction, and pipeline between negative pressure cavity liquid outlet and input end b2021b it is arc-shaped to
Under, the entire downward pipeline of arc is not at the pipeline in horizontal direction, further ensure that liquid from negative pressure cavity 20242
It will not be detained after into the downward pipeline of arc in the downward pipeline of arc.
The operation principle of negative-pressure cyclic filter device 2 of the present invention is:By at the port of export b2022b flow control valve,
The closed check valve at flow control valve and the input end b2021b at the port of export c2022c, with the aspiration pump
Air in the negative pressure cavity 20242 is detached to form negative pressure state by 20243, opens motor 2011, is added the raw material into described
Raw material enters in passage 20123, and raw material enters the second filter device after the rotation whipping filter screen 2012 tentatively filtering
202, the flow control valve at the port of export b2022b is opened, raw material enters in the negative pressure cavity 20242 under negative pressure state,
After raw material covers negative pressure cavity liquid outlet, continue to detach the air in negative pressure cavity 20242 with aspiration pump 20243, open simultaneously
Check valve at input end b2021b, until raw material can be along the input end b2021b, port of export a2021c, described
Filtration members 2023, the input end c2022a, the port of export b2022b and the negative pressure device 2024 are formed by pipeline
Negative-pressure cyclic filtration channel circulate after, close aspiration pump 20243, pressure in negative pressure device 2024 keeps permanent at this time
It is fixed, after the completion of band filtering, the flow control valve at port of export b2022b and the check valve at input end b2021b are closed, is opened
Flow control valve at port of export c2022c, the raw material after filtering enter in reaction kettle body 1.
Mounting bracket 4 is profile piece, and mounting bracket 4 is equipped with stirring motor, and main agitating device 5 is connected with stirring motor, stirs
Motor drives the main agitating device 5 to rotate, and the rotation and lifting agitating device 3 includes the first lifting agitating device 301, second
It lifts agitating device the 302, the 3rd and lifts the lifting agitating device 304 of agitating device 303 and the 4th, the first lifting stirring dress
It puts the 301, second lifting agitating device the 302, the 3rd and lifts the lifting agitating device 304 of agitating device the 303, the 4th and main stirring dress
Putting 5 position distribution relations is:Main agitating device 5 is located at center, and the first lifting agitating device 301, second lifts agitating device
302nd, the 3rd lifting agitating device the 303, the 4th lifts the surrounding that agitating device 304 is distributed in main agitating device 5, main agitating device
5 include horizontal centre section in the horizontal direction and vertically on vertical central cross-section, and described first liter
It drops agitating device 301 and the described second lifting agitating device 302 is symmetrical compared with vertical central cross-section, the first lifting stirring
Device 301 and the described 4th lifting agitating device 304 are symmetrical compared with horizontal centre section, the second lifting agitating device
302 with the described 3rd lifting agitating device 303 it is symmetrical compared with horizontal centre section, it is described 3rd lifting agitating device 303 with
The 4th lifting agitating device 304 is symmetrical compared with vertical central cross-section.
Further, the first lifting agitating device 301, the second lifting agitating device 302, the 3rd lifting
Agitating device 303 and the 4th lifting agitating device 304 have identical structure, the first lifting agitating device 301
With the described 3rd lifting 303 synchronization lifting of agitating device, i.e., the first lifting agitating device 301 and the 3rd lifts agitating device 303
With rising with drop, the second lifting agitating device 302 and the described 4th lifting agitating device 304 also synchronization lifting, described first
Agitating device 301 and the described second lifting 302 asynchronous lifting of agitating device are lifted, i.e., when the first lifting agitating device 301 rises
Second lifting agitating device 302 declines, and the second lifting agitating device 302 rises when the first lifting agitating device 301 declines, described
First lifting agitating device 301, the second lifting agitating device 302, the 3rd lifting agitating device 303, the described 4th
The synchronization lifting in agitating device 304 between any two and asynchronous lifting are lifted, the liquid in reaction kettle body is made to form sinuous flow, is mixed
It closes more uniformly, quickly.
Further, the main agitating device 5 includes the main agitating shaft 501 connected with stirring motor, is located at the master and stirs
Mix the paddle 502 on axis 501 and the drive bevel gear 503 being located on main agitating shaft 501.
Further, the first lifting agitating device 301 includes and that drive bevel gear 503 is sequentially connected is first driven
Bevel gear 3011, for fixing the first driven wheel of differential rotating shaft 3012 of the first driven wheel of differential 3011, be fixedly connected on institute
First for stating the first driving pulley 3013 on the first driven wheel of differential rotating shaft 3012, being driven by the first driving pulley 3013
Driven pulley 3014, the first pivoted link 3015 being hinged on first driven pulley 3014 and first revolution connect
The first hinged intermediate active connecting rod 3016 of bar 3015 and hinged the first elevating mechanism of the first intermediate active connecting rod 3016
3017 and the first driven pulley rotating shaft 3018 for being fixedly connected with first driven pulley 3014.
First driven wheel of differential rotating shaft 3012 and the first driven pulley rotating shaft 3018 are horizontal positioned, and logical
It crosses 2 vertical racks to be fixed on rotation and lifting agitating device mounting bracket, vertical rack is equipped with rolling bearing, and first from mantle
3012 and first driven pulley rotating shaft 3018 of gear rotating shaft is connected by rolling bearing with vertical rack, and first from mantle
Gear 3011 is connected with the first driven wheel of differential rotating shaft 3012 by spline, 503 and first driven wheel of differential of drive bevel gear
3011 drive connection realizes and 3011 vertical side of the first driven wheel of differential is rotated to from 503 horizontal direction of drive bevel gear
The transformation rotated up, the rotation of the first driven pulley 3014 drive the first pivoted link 3015 and the first intermediate active to connect
Bar 3016 does periodic motion, and the periodic motion of final first intermediate active connecting rod 3016 drives the first elevating mechanism 3017 to realize
Cycle elevating movement;It is located at the first lifting agitating device 301, the second lifting agitating device 302, the 3rd lifting respectively
Agitating device 303 and it is described 4th lifting agitating device 304 on 4 as the first driven wheel of differential 3011 respectively with master
Dynamic bevel gear 503 is sequentially connected, wherein the first lifting agitating device 301 is lifted with the described 3rd on agitating device 303
First driven wheel of differential, 3011 direction of rotation is consistent, is stirred so as to fulfill the first lifting agitating device 301 and the described 3rd lifting
The synchronization lifting of device 303, it is described second lifting agitating device 302 with the described 4th lifting agitating device 304 on first from
3011 direction of rotation of dynamic bevel gear is consistent, is stirred so as to fulfill the synchronous second lifting agitating device 302 with the described 4th lifting
Mix the lifting of device 304.
Further, first elevating mechanism 3017 is equipped with and the first intermediate active connecting rod successively from inside to outside
It 3016 the first hinged screw rods 30171, the first spiral lifting stirring axle sleeve 30172 and is fixedly connected with reaction kettle body 1
First guideway 30173, first screw rod 30171, the first spiral lifting stirring axle sleeve 30172 and first are oriented to
30173 three of axle sleeve is concentric, and 30171 outer surface of the first screw rod is equipped with external screw thread a, first guideway
30173 are equipped with internal thread a, and 30172 inner surface of the first spiral lifting stirring axle sleeve is equipped with and first screw rod 30171
The matched lifting stirring axle sleeve internal thread b of external screw thread, 30172 outer surface of the first spiral lifting stirring axle sleeve is equipped with and institute
The lifting stirring axle sleeve external screw thread b that 30173 internal thread of the first guideway is spirally connected is stated, first guideway 30173 is vertical
It sets on reaction kettle body 1, makes to be located at the first spiral lifting agitating shaft being spirally connected therewith inside first guideway 30173
Set 30172 and the first screw rod 30171 being spirally connected with the first spiral lifting stirring axle sleeve 30172 can only prolong vertical direction fortune
It is dynamic.
The periodic motion of first intermediate active connecting rod 3016 drives 3017 performance period of the elevating movement of the first elevating mechanism,
Substantially the first intermediate active connecting rod 3016 drives hinged with the first intermediate active connecting rod 3016 in the first elevating mechanism 3017
The first screw rod 30171 do cycle elevating movement, the cycle elevating movement of the first screw rod 30171 drives thread fitting therewith
The first spiral lifting stirring axle sleeve 30172 do the movement of periodic spiral lifting in the vertical direction.
Claims (4)
1. a kind of reaction kettle, including reaction kettle body(1), be located at the reaction kettle body(1)On for the negative of filtered fluid raw material
Pressure circulation filter (2), for stirring the reaction kettle body(1)The rotation and lifting agitating device of middle liquid(3)With main stirring
Device(5)And for installing the rotation and lifting agitating device(3)With main agitating device(5)Required mounting bracket(4);
The rotation and lifting agitating device (3) includes the first lifting agitating device(301), second lifting agitating device(302),
Three lifting agitating devices(303)And the 4th lifting agitating device(304);
The main agitating device(5)Including main agitating shaft(501), be located at the main agitating shaft(501)On paddle(502)With
And it is located at main agitating shaft(501)On drive bevel gear(503);
It is characterized in that, the first lifting agitating device(301)Including and drive bevel gear(503)Be sequentially connected first from
Dynamic bevel gear(3011), for fixing the first driven wheel of differential(3011)The first driven wheel of differential rotating shaft(3012), it is fixed
It is connected to the first driven wheel of differential rotating shaft(3012)On the first driving pulley(3013), be the first driving pulley
(3013)The first driven pulley driven(3014), be hinged on first driven pulley(3014)On the first pivoted link
(3015)And first pivoted link(3015)The first hinged intermediate active connecting rod(3016)It is and living among described first
Dynamic connecting rod(3016)The first hinged elevating mechanism(3017)And with first driven pulley(3014)Be fixedly connected
One driven pulley rotating shaft(3018);First elevating mechanism(3017)It is equipped with successively from inside to outside and the described first centre is living
Dynamic connecting rod(3016)The first hinged screw rod(30171), the first spiral lifting stirring axle sleeve(30172)And and reaction kettle body
(1)The first guideway being fixedly connected(30173);
The first lifting agitating device(301), it is described second lifting agitating device(302), it is described 3rd lifting agitating device
(303)And the 4th lifting agitating device(304)With identical structure, the first lifting agitating device(301)With
The 3rd lifting agitating device(303)Synchronization lifting, the second lifting agitating device(302)It is stirred with the described 4th lifting
Device(304)Synchronization lifting, the first lifting agitating device(301)With the described second lifting agitating device(302)Asynchronous liter
Drop;
The negative-pressure cyclic filter device(2)Including the first filter device(201)And with first filter device(201)Even
The second filter device connect(202);First filter device(201)Including being located at the reaction kettle body(1)The motor of top
(2011)And the motor(2011)The rotation whipping filter screen of connection(2012), be located at it is described rotation whipping filter screen
(2012)The impurity collecting box of bottom(2013), be fixedly connected on reaction kettle body(1)On for store it is described rotation whipping mistake
Strainer(2012)Throw away the liquid holding tank of liquid(2014)And it is located at the liquid holding tank(2014)The bottom of bottom goes out
Mouthful(2015), the rotation whipping filter screen(2012)It is arranged on the liquid holding tank(2014)It is internal and can be from described
Liquid holding tank(2014)Middle taking-up;
Second filter device(202)Including liquid inlet tee joint pipe(2021), goes out liquid threeway pipe(2022), filtration members(2023)、
Negative pressure device(2024), the liquid inlet tee joint pipe(2021)Including input end a(2021a), input end b(2021b)And outlet
Hold a(2021c), the goes out liquid threeway pipe(2022)Including input end c(2022a), port of export b(2022b)And port of export c
(2022c), the input end a(2021a)With the outlet at bottom(2015)Connection, the filtration members(2023)Go out described in being located at
Mouth end a(2021c)With input end c(2022a)Between, the negative pressure device(2024)It is located at the port of export b(2022b)With institute
State input end b(2021b)Between, the outlet at bottom(2015), the input end a(2021a), the port of export a
(2021c), the filtration members(2023), the input end c(2022a)And the port of export c(2022c)It is formed by pipeline
Raw material after filtering is injected the reaction kettle body by passage(1)In, the input end b(2021b), the port of export a
(2021c), the filtration members(2023), the input end c(2022a), the port of export b(2022b)And the negative pressure dress
It puts(2024)Negative-pressure cyclic filtration channel is formed by pipeline;
The negative pressure device(2024)Including negative pressure body(20241), be located at the negative pressure body(20241)Internal negative pressure cavity
(20242), be located at the negative pressure body(20241)On aspiration pump(20243).
A kind of 2. reaction kettle according to claim 1, which is characterized in that the reaction kettle body(1)Including upper reaction kettle body
(1a), with the upper reaction kettle body(1a) the lower reaction kettle body of connection(2a), for the first sealing ring of sealing(3a) with second
Sealing ring(4a).
A kind of 3. reaction kettle according to claim 2, which is characterized in that first sealing ring(3a) include the first sealing
Enclose cylindrical ring body(301a), it is located at the first sealing ring cylindrical ring body(The oblique protrusion of multiple bar shapeds elasticity on 301a)
(302a), by the oblique protrusion of adjacent bar elasticity(Protruded connecting members 302a) connected(303a), the first sealing ring circle
Band of column body(301a), the oblique protrusion of the bar shaped elasticity(302a) and the protruded connecting members(It 303a) is integrally formed, adjacent institute
State the oblique protrusion of bar shaped elasticity(302a) and the protruded connecting members(The first cavity 303a) is formed between three(304a), it is described
First cavity(304a) it is equipped with the first auxiliary seal body of elastically deformable(305a), the oblique protrusion of the bar shaped elasticity(In 302a)
Equipped with along the oblique protrusion of bar shaped elasticity(302a) the oblique elastic cavity of extending direction(306a).
A kind of 4. reaction kettle according to claim 2, which is characterized in that second sealing ring(4a) include sealing ring master
Body(401a), it is arranged on the sealing ring main body(Multiple seal protuberances on 401a)(402a), it is coated on the seal protuberance
(Elastic sealing element on 402a)(403a), the seal protuberance(402a) with the elastic sealing element(Bullet is formed between 403a)
Property chamber(404a), the elastic cavity(404a) it is equipped with multiple elastic pearls(405a), the adjacent elastic sealing element(Between 403a)
Form cavity(406a), the cavity(Prolong the cavity in 406a)(406a) wall is equipped with auxiliary sealing member(407a).
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CN201610491215.7A CN106040139B (en) | 2016-06-29 | 2016-06-29 | A kind of reaction kettle |
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CN201610491215.7A CN106040139B (en) | 2016-06-29 | 2016-06-29 | A kind of reaction kettle |
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CN106040139B true CN106040139B (en) | 2018-05-22 |
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CN107099662B (en) * | 2017-05-16 | 2018-09-18 | 嘉兴市迅程信息技术有限公司 | A kind of Rare Earth Mine precipitation type settler easy to clean |
CN107998992B (en) * | 2017-12-05 | 2020-04-28 | 浙江天奇新材料科技股份有限公司 | Hot-curing furan resin fixed-ratio production system and process |
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CN201337902Y (en) * | 2008-11-04 | 2009-11-04 | 无锡市张华医药设备有限公司 | Filtering, washing and drying three-in-one device |
CN202921308U (en) * | 2012-10-25 | 2013-05-08 | 河南银城科技股份有限公司 | Extremely-toxic substance reaction device |
CN204134623U (en) * | 2014-07-22 | 2015-02-04 | 江山市艺康化学有限公司 | The filtering type reactor that agitating roller height charging aperture direction is adjustable |
CN204412257U (en) * | 2015-01-16 | 2015-06-24 | 云南润杰农业科技股份有限公司 | One seed amino acid retort |
CN204485860U (en) * | 2015-03-18 | 2015-07-22 | 袁加平 | A kind of auxiliary agitation cycle reactor |
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2016
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Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN201337902Y (en) * | 2008-11-04 | 2009-11-04 | 无锡市张华医药设备有限公司 | Filtering, washing and drying three-in-one device |
CN202921308U (en) * | 2012-10-25 | 2013-05-08 | 河南银城科技股份有限公司 | Extremely-toxic substance reaction device |
CN204134623U (en) * | 2014-07-22 | 2015-02-04 | 江山市艺康化学有限公司 | The filtering type reactor that agitating roller height charging aperture direction is adjustable |
CN204412257U (en) * | 2015-01-16 | 2015-06-24 | 云南润杰农业科技股份有限公司 | One seed amino acid retort |
CN204485860U (en) * | 2015-03-18 | 2015-07-22 | 袁加平 | A kind of auxiliary agitation cycle reactor |
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