CN106001395A - Coating for hub forming mold and preparation method thereof - Google Patents
Coating for hub forming mold and preparation method thereof Download PDFInfo
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- CN106001395A CN106001395A CN201610465900.2A CN201610465900A CN106001395A CN 106001395 A CN106001395 A CN 106001395A CN 201610465900 A CN201610465900 A CN 201610465900A CN 106001395 A CN106001395 A CN 106001395A
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- consumption
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- weight portion
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- mixed liquor
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22C—FOUNDRY MOULDING
- B22C3/00—Selection of compositions for coating the surfaces of moulds, cores, or patterns
Abstract
The invention discloses coating for a hub forming mold and a preparation method thereof. The preparation method of the coating comprises the steps that sodium alginate, sodium carboxymethyl cellulose, aluminum phosphate, soluble silicate, phenol formaldehyde resin and water are stirred and mixed, so that mixed liquor M is formed; after being subjected to still standing for 2-4 hours, the mixed liquor M is added with refractory powder and stirred, and then mixed liquor N is obtained; and the mixed liquor N is put in a sealed environment to be subjected to aging treatment, and the coating for the hub forming mold is obtained. The problems that the defects of pores, sand holes and the like of a casting occur due to the fact that the volatility of traditional coating is high, meanwhile, the strength of the traditional coating is low, and a formed coating layer is prone to being cracked are solved.
Description
Technical field
The present invention relates to coating preparation field, in particular it relates to wheel hub mould coating and preparation side thereof
Method.
Background technology
Along with the development in epoch, require day by day to improve to the matter of the product of casting quality, traditional sand casting
Can not meet Production requirement, new special casts, high with its precision, resistant to damage is good, low cost
Etc. advantage, being increasingly widely used, representative therein is exactly permanent mold casting, its because processing performance is high,
Technological process is easy, surface finish of casting advantages of higher gains great popularity, but the one of permanent mold casting is big
A difficult problem is how to improve its metal type dies life-span, and therefore, the research and development of metal mold heat-resisting paint have weight
Want meaning.Traditional coating volatility is high, will result in foundry goods and produces the defect such as pore, sand holes, is coated with meanwhile
The intensity of material is relatively low, and the coating of formation is easy to crack.
Summary of the invention
It is an object of the invention to provide a kind of wheel hub mould coating and preparation method thereof, solve tradition
Coating volatility is high, will result in foundry goods and produces the defect such as pore, sand holes, and meanwhile, the intensity of coating is relatively low,
The coating problem easy to crack formed.
To achieve these goals, the invention provides the preparation method of a kind of wheel hub mould coating,
Wherein, described preparation method includes:
(1) by sodium alginate, sodium carboxymethyl cellulose, aluminum phosphate, waterglass, phenolic resin and water
Stirring mixing, forms mixed liquor M;
(2) add refractory powder after described mixed liquor M being stood 2-4h, after stirring, obtain mixed liquor N;
(3) mixed liquor N is placed in sealed environment carries out ripening, obtain wheel hub mould and be coated with
Material;Wherein, relative to the water of 100 weight portions, the consumption of described sodium alginate is 5-15 weight portion,
The consumption of described sodium carboxymethyl cellulose is 2-7 weight portion, and the consumption of described aluminum phosphate is 3-10 weight portion,
The consumption of described waterglass is 4-12 weight portion, and the consumption of described phenolic resin is 10-20 weight portion, institute
The consumption stating refractory powder is 1-5 weight portion.
Present invention also offers a kind of wheel hub mould coating, described wheel hub mould coating is by above-mentioned
Preparation method prepare.
By technique scheme, the invention provides a kind of wheel hub mould coating and preparation side thereof
Method, wherein, described preparation method includes: by sodium alginate, sodium carboxymethyl cellulose, aluminum phosphate, water
Glass, phenolic resin and water stirring mixing, form mixed liquor M;Described mixed liquor M is stood 2-4h
Rear addition refractory powder, obtains mixed liquor N after stirring;Mixed liquor N is placed in sealed environment carry out old
Change processes, and obtains wheel hub mould coating, by the synergism between each raw material so that prepared
Coating possesses relatively low volatility, and the coating of formation is the most easy to crack to come off, and the intensity of coating is high.
Other features and advantages of the present invention will be described in detail in detailed description of the invention part subsequently.
Detailed description of the invention
Hereinafter the detailed description of the invention of the present invention is described in detail.It should be appreciated that this place is retouched
The detailed description of the invention stated is merely to illustrate and explains the present invention, is not limited to the present invention.
The invention provides the preparation method of a kind of wheel hub mould coating, wherein, described preparation method
Including: sodium alginate, sodium carboxymethyl cellulose, aluminum phosphate, waterglass, phenolic resin and water are stirred
Mixing, forms mixed liquor M;Refractory powder is added, after stirring after described mixed liquor M is stood 2-4h
Obtain mixed liquor N;Mixed liquor N is placed in sealed environment and carries out ripening, obtain wheel hub shaping mould
Tool coating, wherein, relative to the water of 100 weight portions, the consumption of described sodium alginate is 5-15 weight
Part, the consumption of described sodium carboxymethyl cellulose is 2-7 weight portion, and the consumption of described aluminum phosphate is 3-10 weight
Amount part, the consumption of described waterglass is 4-12 weight portion, and the consumption of described phenolic resin is 10-20 weight
Part, the consumption of described refractory powder is 1-5 weight portion.
So that the coating prepared possesses relatively low volatility and higher intensity, in the one of the present invention
In preferred embodiment, relative to the water of 100 weight portions, the consumption of described sodium alginate is 8-12
Weight portion, the consumption of described sodium carboxymethyl cellulose is 3-5 weight portion, and the consumption of described aluminum phosphate is 5-7
Weight portion, the consumption of described waterglass is 6-10 weight portion, and the consumption of described phenolic resin is 14-16 weight
Amount part, the consumption of described refractory powder is 2-3 weight portion.
The present invention one preferred embodiment in, in order to improve the refractory ability of coating further,
Described refractory powder is one or more in clay, silicon oxide and aluminium oxide, it is preferred that described fire-resistant
The particle diameter of powder is 2-8mm.
In order to improve the performance of sodium alginate further, the present invention one preferred embodiment in,
The time stating ripening is 24-36h.
The present invention one preferred embodiment in, in order to improve the intensity of coating further, described
The viscosity of epoxy resin is 1500-2500mPa s.
Present invention also offers a kind of wheel hub mould coating, described wheel hub mould coating is by above-mentioned
Preparation method prepare.
Hereinafter will be described the present invention by embodiment.In following example, sodium alginate is
The commercially available product that Qingdao excellent rope chemistry Science and Technology Ltd. provides, epoxy resin is that money wide industrial chemicals in Wuxi has
The commercially available product that limit company provides.
Embodiment 1
By 8g sodium alginate, 3g sodium carboxymethyl cellulose, 5g aluminum phosphate, 6g waterglass, 14g phenolic aldehyde
Resin and the stirring mixing of 100g water, form mixed liquor M;Add after described mixed liquor M is stood 2h
2g refractory powder (particle diameter is 2mm), obtains mixed liquor N after stirring;Mixed liquor N is placed in sealing ring
Border carries out ripening (time is 24h), obtains wheel hub mould coating A1.
Embodiment 2
By 12g sodium alginate, 5g sodium carboxymethyl cellulose, 7g aluminum phosphate, 10g waterglass, 16g phenol
Urea formaldehyde and the stirring mixing of 100g water, form mixed liquor M;Add after described mixed liquor M is stood 4h
Enter refractory powder (particle diameter is 8mm), after stirring, obtain mixed liquor N;Mixed liquor N is placed in sealing ring
Border carries out ripening (time is 36h), obtains wheel hub mould coating A2.
Embodiment 3
By 10g sodium alginate, 4g sodium carboxymethyl cellulose, 6g aluminum phosphate, 8g waterglass, 15g phenol
Urea formaldehyde and the stirring mixing of 100g water, form mixed liquor M;Add after described mixed liquor M is stood 3h
Enter refractory powder (particle diameter is 5mm), after stirring, obtain mixed liquor N;Mixed liquor N is placed in sealing ring
Border carries out ripening (time is 30h), obtains wheel hub mould coating A3.
Embodiment 4
Being prepared according to the method for embodiment 1, except for the difference that, the consumption of water is 100g, described Sargassum
The consumption of acid sodium is 5g, and the consumption of described sodium carboxymethyl cellulose is 2g, and the consumption of described aluminum phosphate is
3g, the consumption of described waterglass is 4g, and the consumption of described phenolic resin is 10g, described refractory powder
Consumption is 1g, obtains wheel hub mould coating A4.
Embodiment 5
Being prepared according to the method for embodiment 1, except for the difference that, the consumption of water is 100g, described Sargassum
The consumption of acid sodium is 15g, and the consumption of described sodium carboxymethyl cellulose is 7g, and the consumption of described aluminum phosphate is
10g, the consumption of described waterglass is 12g, and the consumption of described phenolic resin is 20g, described refractory powder
Consumption be 5g, obtain wheel hub mould coating A5.
Comparative example 1
Being prepared according to the method for embodiment 1, except for the difference that, the consumption of water is 100g, described Sargassum
The consumption of acid sodium is 3g, and the consumption of described sodium carboxymethyl cellulose is 1g, and the consumption of described aluminum phosphate is
2g, the consumption of described waterglass is 2g, and the consumption of described phenolic resin is 6g, described refractory powder
Consumption is 0.5g, obtains wheel hub mould coating D1.
Comparative example 2
Being prepared according to the method for embodiment 1, except for the difference that, the consumption of water is 100g, described Sargassum
The consumption of acid sodium is 20g, and the consumption of described sodium carboxymethyl cellulose is 10g, the consumption of described aluminum phosphate
For 12g, the consumption of described waterglass is 15g, and the consumption of described phenolic resin is 22g, described refractory powder
The consumption of material is 7g, obtains wheel hub mould coating D2.
Test case 1
Hub mold is heated to 200 DEG C, then the coating A1-A5, D1 and the D2 that stir is divided
It is not sprayed on mould (THICKNESS CONTROL is between 0.25mm~0.30mm), mould is placed on instrument,
Setting the number of turns (10 circle) rotated, start instrument and measure, the quality passing through scraped coating is many
Few, it is judged that the power of coating intensity.
Table 1
Embodiment is numbered | The amount of gas evolution from the coating (ml/g) | Scrape the quality (g) of coating |
A1 | 1.2 | 0.4 |
A2 | 1.1 | 0.5 |
A3 | 0.9 | 0.3 |
A4 | 1.5 | 1.1 |
A5 | 1.8 | 0.9 |
D1 | 3.5 | 1.9 |
D2 | 3.6 | 1.8 |
By above table data it can be seen that the coating A1-A5's prepared within the scope of the present invention sends out
Less than coating D1 and D2 prepared outside the scope of the invention, tolerance to illustrate that the volatility of A1-A5 is low,
Not easily causing foundry goods and produce the defect such as pore, sand holes, after strength test, A1-A5 scrapes the matter of coating
Amount D1 and D2 to be less than, illustrates that the intensity of A1-A5 is higher than D1 and D2, meanwhile, in the present invention
The coating A1-A3 prepared in the range of You Xuan possesses the most excellent performance.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited to above-mentioned reality
Execute the detail in mode, in the technology concept of the present invention, can be to the technical side of the present invention
Case carries out multiple simple variant, and these simple variant belong to protection scope of the present invention.
It is further to note that each the concrete technology described in above-mentioned detailed description of the invention is special
Levy, in the case of reconcilable, can be combined by any suitable means, in order to avoid need not
The repetition wanted, various possible compound modes are illustrated by the present invention the most separately.
Additionally, combination in any can also be carried out between the various different embodiment of the present invention, as long as its
Without prejudice to the thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (7)
1. the preparation method of a wheel hub mould coating, it is characterised in that described preparation method bag
Include:
(1) by sodium alginate, sodium carboxymethyl cellulose, aluminum phosphate, waterglass, phenolic resin and water
Stirring mixing, forms mixed liquor M;
(2) add refractory powder after described mixed liquor M being stood 2-4h, after stirring, obtain mixed liquor N;
(3) mixed liquor N is placed in sealed environment carries out ripening, obtain wheel hub mould and be coated with
Material;Wherein, relative to the water of 100 weight portions, the consumption of described sodium alginate is 5-15 weight portion,
The consumption of described sodium carboxymethyl cellulose is 2-7 weight portion, and the consumption of described aluminum phosphate is 3-10 weight portion,
The consumption of described waterglass is 4-12 weight portion, and the consumption of described phenolic resin is 10-20 weight portion, institute
The consumption stating refractory powder is 1-5 weight portion.
Preparation method the most according to claim 1, wherein, relative to the water of 100 weight portions,
The consumption of described sodium alginate is 8-12 weight portion, and the consumption of described sodium carboxymethyl cellulose is 3-5 weight
Part, the consumption of described aluminum phosphate is 5-7 weight portion, and the consumption of described waterglass is 6-10 weight portion, institute
The consumption stating phenolic resin is 14-16 weight portion, and the consumption of described refractory powder is 2-3 weight portion.
Preparation method the most according to claim 1, wherein, described refractory powder is clay, oxygen
One or more in SiClx and aluminium oxide.
Preparation method the most according to claim 1, wherein, the particle diameter of described refractory powder is
2-8mm。
Preparation method the most according to claim 1, wherein, the time of described ripening is
24-36h。
Preparation method the most according to claim 1, wherein, the viscosity of described epoxy resin is
1500-2500mPa·s。
7. a wheel hub mould coating, it is characterised in that described wheel hub mould coating is by weighing
Profit requires in 1-6 that the preparation method described in any one prepares.
Priority Applications (1)
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CN201610465900.2A CN106001395A (en) | 2016-06-24 | 2016-06-24 | Coating for hub forming mold and preparation method thereof |
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CN105001783A (en) * | 2015-08-12 | 2015-10-28 | 江苏绿科生物技术有限公司 | Preparation method of high-temperature-resistant coating |
CN105033169A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Anti-sedimentation release agent and preparation method thereof |
CN105033172A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy part die-casting die and preparation method thereof |
CN105033170A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy part die-casting die and preparation method thereof |
CN105033171A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy hub die-casting die and preparation method thereof |
CN105110755A (en) * | 2015-08-12 | 2015-12-02 | 江苏绿科生物技术有限公司 | High-temperature-resistant coating |
CN105170882A (en) * | 2015-07-27 | 2015-12-23 | 芜湖黄燕实业有限公司 | High-storability release agent and preparation method thereof |
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2016
- 2016-06-24 CN CN201610465900.2A patent/CN106001395A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105033169A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Anti-sedimentation release agent and preparation method thereof |
CN105033172A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy part die-casting die and preparation method thereof |
CN105033170A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy part die-casting die and preparation method thereof |
CN105033171A (en) * | 2015-07-27 | 2015-11-11 | 芜湖黄燕实业有限公司 | Release agent used for aluminum alloy hub die-casting die and preparation method thereof |
CN105170882A (en) * | 2015-07-27 | 2015-12-23 | 芜湖黄燕实业有限公司 | High-storability release agent and preparation method thereof |
CN105001783A (en) * | 2015-08-12 | 2015-10-28 | 江苏绿科生物技术有限公司 | Preparation method of high-temperature-resistant coating |
CN105110755A (en) * | 2015-08-12 | 2015-12-02 | 江苏绿科生物技术有限公司 | High-temperature-resistant coating |
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