CN106000845A - Fluorescent powder coating process for glass tubes - Google Patents

Fluorescent powder coating process for glass tubes Download PDF

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Publication number
CN106000845A
CN106000845A CN201610409921.2A CN201610409921A CN106000845A CN 106000845 A CN106000845 A CN 106000845A CN 201610409921 A CN201610409921 A CN 201610409921A CN 106000845 A CN106000845 A CN 106000845A
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CN
China
Prior art keywords
dusting
coating
glass
tube
heating
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Granted
Application number
CN201610409921.2A
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Chinese (zh)
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CN106000845B (en
Inventor
桑永树
范学锋
刘军
吴百超
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Anhui Shilin Lighting Co Ltd
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Anhui Shilin Lighting Co Ltd
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Priority to CN201610409921.2A priority Critical patent/CN106000845B/en
Publication of CN106000845A publication Critical patent/CN106000845A/en
Application granted granted Critical
Publication of CN106000845B publication Critical patent/CN106000845B/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/22Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to internal surfaces, e.g. of tubes
    • B05D7/222Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to internal surfaces, e.g. of tubes of pipes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/02Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by baking
    • B05D3/0218Pretreatment, e.g. heating the substrate
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J9/00Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
    • H01J9/20Manufacture of screens on or from which an image or pattern is formed, picked up, converted or stored; Applying coatings to the vessel
    • H01J9/22Applying luminescent coatings

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Manufacturing & Machinery (AREA)
  • Formation Of Various Coating Films On Cathode Ray Tubes And Lamps (AREA)
  • Surface Treatment Of Glass (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

The invention aims to provide a fluorescent powder coating process for glass tubes. The fluorescent powder coating process comprises the steps that step one, materials are selected, specifically, the twenty glass tubes in different specifications and a proper amount of fluorescent powder syrup are selected for standby application; step two, heating is conducted before power coating; step three, coating processing is conducted, specifically, the glass tubes are evenly coated with the fluorescent powder by use of a coating method, four heating zones are set for the coating temperature in the powder coating process, and the heating zones can be properly turned on or off according to seasonal variation in the heating process; and step four, layered weighing and verifying are conducted. The evenness of powder coating is improved by adoption of the circulating reflowing type coating method and a multi-zone segmented controllable heating method as part of improvement for the powder coating process; and multiple times of layer-by-layer powder coating improves control over the thickness of coated powder as well as improving the quality of a coating.

Description

A kind of coating process of glass-tube fluorescent material
Technical field
The present invention relates to the field in terms of glass-tube coating process, particularly to the improvement in terms of the powder-coating method of led fluorescent material, refer more particularly to the coating process of a kind of glass-tube fluorescent material.
Background technology
Along with growth in the living standard, people are the most of a relatively high to the requirement of normal lighting, while illumination, it is also required to the structure to illuminating lamp carry out improving improvement, wherein fluorescent material status especially important in illumination, especially require higher on the coating process of the fluorescent material of illuminating lamp glass-tube, the dusting quality of glass-tube directly influences illuminating effect, owing to stirring and heating abundant not and reasonable in conventional coating process, often when dusting, coating produces substantial amounts of eyebrow print, the substantially flaw such as bright bubble and flake, and it is in uneven thickness, blocked up or the thinnest, and fall flat, therefore substantial amounts of defect ware is produced, increase production cost.
Therefore, the compound method of a kind of fluorescence grinding is provided, to can be by the improvement to coating process, use painting method and the controlled heating of multi-region segmentation looping back streaming, improve the uniformity of dusting, the most successively dusting, improve the control of coating layer thickness, by bisque weight check, reduce substandard product and flow out, just become the problem that those skilled in the art need solution badly.
Summary of the invention
It is an object of the invention to provide the compound method of a kind of fluorescence grinding, to can be by the improvement to coating process, use painting method and the controlled heating of multi-region segmentation looping back streaming, improve the uniformity of dusting, the most successively dusting, improve the control of coating layer thickness, by bisque weight check, reduce substandard product and flow out.
For solving technical problem described in background technology, the present invention by the following technical solutions:
A kind of coating process of glass-tube fluorescent material, the processing step of its dusting is:
Step 1, material select: select the glass-tube 20 of different size and appropriate phosphor slurry, in case using, the specification that its glass-tube is corresponding is:
Diameter includes specification: T8, diameter: 26 ± 0.5;Specification: T9, diameter: 29 ± 0.5;Specification: T10, diameter: 32 ± 0.5, and wall thickness is all between 0.7 0.8, length includes specification: 18/20W, length: 660 ± 1;Specification: 25W, length: 813 ± 1;Specification: 36/40W, length: 1270 ± 1;
Heat before step 2, dusting: before dusting, first once open electric switch, blower fan and heater to heat up, the predetermined temperature of dusting is 80 120 DEG C, when temperature is heated up to predetermined production temperature, open pulp absorbing pump, by carrying out heat treated in advance, it is possible to enable slurry to reach the dusting temperature of requirement at short notice, avoid because local heating's inequality produces the situation of powder and pump housing bonding simultaneously.
Step 3, coating processing: after opening pulp absorbing pump, under the effect of pulp absorbing pump, slurry is evacuated to cone through the pump housing, is coated with in cylinder, flow out when slurry reaches to be coated with cylinder spillwag chute, then in being back to agitator, and constituted circulation with this, then begin through cladding process and glass-tube is carried out uniform dusting, dusting temperature during dusting is divided into four thermals treatment zone, and is respectively as follows:
I district: 70 90;II district: 80 100;III district: 60 80;IV district: 80 100.
Suitably can be turned on and off heating warm area, by looping back painting method and the controlled heating of multi-region segmentation of streaming according to seasonal variations when heating operation, make dusting more uniform, the thermal treatment zone can open and close at any time simultaneously, to reduce the control difficulty of bringing-up section, makes temperature the most various easily-controllable.
Step 4, the inspection of laminated weighting school: after having coated, mark the bright glass-tube of weighing of 3 different sizes, fluorescent material weight is weighed after fully drying, and every 2 hours, it is weighed once, then whether technological requirement is met according to fluorescent material weight, by weighing to the sample timing fluorescent material that carries out the most repeatedly, to judge qualification rate, and produce in enormous quantities.
The invention has the beneficial effects as follows:
1), by the improvement to coating process, use painting method and the controlled heating of multi-region segmentation looping back streaming, improve the uniformity of dusting, the most successively dusting, improve the control of coating layer thickness.
2), by bisque weight check, reduce substandard product and flow out.
Detailed description of the invention
In order to make those skilled in the art be more fully understood that technical scheme, the present invention will be further detailed below.
Embodiment 1:
A kind of coating process of glass-tube fluorescent material, the processing step of its dusting is:
Step 1, material select: select the glass-tube 20 of different size and appropriate phosphor slurry, in case using, the specification that its glass-tube is corresponding is:
Diameter includes specification: T8, diameter: 26 ± 0.5;Specification: T9, diameter: 29 ± 0.5;Specification: T10, diameter: 32 ± 0.5, and wall thickness is all between 0.7 0.8, length includes specification: 18/20W, length: 660 ± 1;Specification: 25W, length: 813 ± 1;Specification: 36/40W, length: 1270 ± 1;
Heat before step 2, dusting: before dusting, first once open electric switch, blower fan and heater to heat up, the predetermined temperature of dusting is 90 DEG C, when temperature is heated up to predetermined production temperature, open pulp absorbing pump, by carrying out heat treated in advance, it is possible to enable slurry to reach the dusting temperature of requirement at short notice, avoid because local heating's inequality produces the situation of powder and pump housing bonding simultaneously.
Step 3, coating processing: after opening pulp absorbing pump, under the effect of pulp absorbing pump, slurry is evacuated to cone through the pump housing, is coated with in cylinder, flow out when slurry reaches to be coated with cylinder spillwag chute, then in being back to agitator, and constituted circulation with this, then begin through cladding process and glass-tube is carried out uniform dusting, dusting temperature during dusting is divided into four thermals treatment zone, and is respectively as follows:
I district: 70;II district: 80;III district: 70;IV district: 90.
Suitably can be turned on and off heating warm area, by looping back painting method and the controlled heating of multi-region segmentation of streaming according to seasonal variations when heating operation, make dusting more uniform, the thermal treatment zone can open and close at any time simultaneously, to reduce the control difficulty of bringing-up section, makes temperature the most various easily-controllable.
Step 4, the inspection of laminated weighting school: after having coated, mark the bright glass-tube of weighing of 3 different sizes, fluorescent material weight is weighed after fully drying, and every 2 hours, it is weighed once, then whether technological requirement is met according to fluorescent material weight, by weighing to the sample timing fluorescent material that carries out the most repeatedly, to judge qualification rate, and produce in enormous quantities.
Implement to prove, use this data, use low-temperature prewarming and heat treated, improve to a certain extent in the uniformity improving dusting, but temperature during dusting heating is slightly lower, can bond when dusting, except water abundant not, increase heat time heating time.
Embodiment 2:
A kind of coating process of glass-tube fluorescent material, the processing step of its dusting is:
Step 1, material select: select the glass-tube 20 of different size and appropriate phosphor slurry, in case using, the specification that its glass-tube is corresponding is:
Diameter includes specification: T8, diameter: 26 ± 0.5;Specification: T9, diameter: 29 ± 0.5;Specification: T10, diameter: 32 ± 0.5, and wall thickness is all between 0.7 0.8, length includes specification: 18/20W, length: 660 ± 1;Specification: 25W, length: 813 ± 1;Specification: 36/40W, length: 1270 ± 1;
Heat before step 2, dusting: before dusting, first once open electric switch, blower fan and heater to heat up, the predetermined temperature of dusting is 120 DEG C, when temperature is heated up to predetermined production temperature, open pulp absorbing pump, by carrying out heat treated in advance, it is possible to enable slurry to reach the dusting temperature of requirement at short notice, avoid because local heating's inequality produces the situation of powder and pump housing bonding simultaneously.
Step 3, coating processing: after opening pulp absorbing pump, under the effect of pulp absorbing pump, slurry is evacuated to cone through the pump housing, is coated with in cylinder, flow out when slurry reaches to be coated with cylinder spillwag chute, then in being back to agitator, and constituted circulation with this, then begin through cladding process and glass-tube is carried out uniform dusting, dusting temperature during dusting is divided into four thermals treatment zone, and is respectively as follows:
I district: 90;II district: 100;III district: 80;IV district: 100.
Suitably can be turned on and off heating warm area, by looping back painting method and the controlled heating of multi-region segmentation of streaming according to seasonal variations when heating operation, make dusting more uniform, the thermal treatment zone can open and close at any time simultaneously, to reduce the control difficulty of bringing-up section, makes temperature the most various easily-controllable.
Step 4, the inspection of laminated weighting school: after having coated, mark the bright glass-tube of weighing of 3 different sizes, fluorescent material weight is weighed after fully drying, and every 2 hours, it is weighed once, then whether technological requirement is met according to fluorescent material weight, by weighing to the sample timing fluorescent material that carries out the most repeatedly, to judge qualification rate, and produce in enormous quantities.
Implement to prove, use this data, use and carry out preheating and heat treated under hot conditions, improving to the full extent in the uniformity improving dusting, when smearing, temperature is of a relatively high simultaneously, and it is stronger that molecule enlivens power, advantageously in the bonding of phosphor slurry, also substantially reduce heat time heating time simultaneously.
Therefore, the present embodiment is most preferred embodiment.
By the way of explanation, only describe some one exemplary embodiment of the present invention above, undoubtedly, for those of ordinary skill in the art, in the case of without departing from the spirit and scope of the present invention, by various different modes, described embodiment can be modified.Therefore, foregoing description is the most illustrative, should not be construed as the restriction to the claims in the present invention protection domain.

Claims (1)

1. the coating process of a glass-tube fluorescent material, it is characterised in that the processing step of its dusting is:
Step 1, material select: select the glass-tube 20 of different size and appropriate phosphor slurry, in case making With, the specification that its glass-tube is corresponding is:
Diameter includes specification: T8, diameter: 26 ± 0.5;Specification: T9, diameter: 29 ± 0.5;Specification: T10, diameter: 32 ± 0.5, and wall thickness is all between 0.7 0.8, length includes specification: 18/20W, length Degree: 660 ± 1;Specification: 25W, length: 813 ± 1;Specification: 36/40W, length: 1270 ± 1;
Heat before step 2, dusting: before dusting, first once open electric switch, blower fan and heater and enter Row heats up, and the predetermined temperature of dusting is 80 120 DEG C, when temperature is heated up to predetermined production temperature, opens Pulp absorbing pump.
Step 3, coating processing: after opening pulp absorbing pump, under the effect of pulp absorbing pump, slurry is evacuated to loudspeaker through the pump housing In cylinder, painting cylinder, flow out when slurry reaches to be coated with cylinder spillwag chute, then in being back to agitator, and with This constitutes circulation, then begins through cladding process and glass-tube is carried out uniform dusting, and dusting temperature during dusting is divided It is four thermals treatment zone, and is respectively as follows:
I district: 70 90;II district: 80 100;III district: 60 80;IV district: 80 100.
Suitably can be turned on and off heating warm area according to seasonal variations when heating operation.
Step 4, the inspection of laminated weighting school: mark the bright glass-tube of weighing of 3 different sizes after having coated, carry out Weigh fluorescent material weight after fully drying, and every 2 hours, it is weighed once, then according to fluorescence grain weight Whether amount meets technological requirement.
CN201610409921.2A 2016-06-03 2016-06-03 Powder coating process of glass tube fluorescent powder Active CN106000845B (en)

Priority Applications (1)

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CN201610409921.2A CN106000845B (en) 2016-06-03 2016-06-03 Powder coating process of glass tube fluorescent powder

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Application Number Priority Date Filing Date Title
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CN106000845B CN106000845B (en) 2020-02-18

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107088511A (en) * 2017-04-17 2017-08-25 安徽路明光电科技有限公司 A kind of fluorescent material application process of LED filament

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5344667A (en) * 1993-02-23 1994-09-06 Rockwell International Corporation Method and apparatus for manufacturing serpentine avionics fluorescent tubes with enhanced uniformity of luminance and chromaticity
CN2243123Y (en) * 1996-02-09 1996-12-18 李建龙 Compacted fluorescent-lamp powder-coating machine
CN202263695U (en) * 2011-09-20 2012-06-06 浙江金陵光源电器有限公司 Constant temperature retaining device
CN102683138A (en) * 2012-05-11 2012-09-19 广东电力士照明科技有限公司 Technique for manufacturing glass tube case of electrodeless lamp

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5344667A (en) * 1993-02-23 1994-09-06 Rockwell International Corporation Method and apparatus for manufacturing serpentine avionics fluorescent tubes with enhanced uniformity of luminance and chromaticity
CN2243123Y (en) * 1996-02-09 1996-12-18 李建龙 Compacted fluorescent-lamp powder-coating machine
CN202263695U (en) * 2011-09-20 2012-06-06 浙江金陵光源电器有限公司 Constant temperature retaining device
CN102683138A (en) * 2012-05-11 2012-09-19 广东电力士照明科技有限公司 Technique for manufacturing glass tube case of electrodeless lamp

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
吴祖塏: "《荧光灯制造基础》", 30 June 1962, 上海科学技术出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107088511A (en) * 2017-04-17 2017-08-25 安徽路明光电科技有限公司 A kind of fluorescent material application process of LED filament

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