CN106000624A - Multi-element recovery method for waste residues of gold tailings - Google Patents

Multi-element recovery method for waste residues of gold tailings Download PDF

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Publication number
CN106000624A
CN106000624A CN201610579070.6A CN201610579070A CN106000624A CN 106000624 A CN106000624 A CN 106000624A CN 201610579070 A CN201610579070 A CN 201610579070A CN 106000624 A CN106000624 A CN 106000624A
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China
Prior art keywords
flotation
tailings
mine tailing
gold
waste residues
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CN201610579070.6A
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Chinese (zh)
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CN106000624B (en
Inventor
王书岩
王洪波
丛玉韶
孙宝军
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SHANDONG JIUQU SHENGJI NEW BUILDING MATERIALS CO Ltd
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SHANDONG JIUQU SHENGJI NEW BUILDING MATERIALS CO Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B03SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
    • B03BSEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
    • B03B9/00General arrangement of separating plant, e.g. flow sheets
    • B03B9/06General arrangement of separating plant, e.g. flow sheets specially adapted for refuse
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/82Recycling of waste of electrical or electronic equipment [WEEE]

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  • Manufacture And Refinement Of Metals (AREA)

Abstract

The invention relates to a multi-element recovery method for waste residues of gold tailings. The method comprises the steps that the waste residues of the gold tailings enter a main bin after stone, garbage and the like are extracted through a vibration screen; then the waste residues enter a ball mill through a belt conveyor for ore grinding; then the waste residues pass through a stirring bucket, 24 g-26 g of xanthate and 19 g-20 g of flotation oil are added to per ton of the waste residues of the gold tailings, the waste residues enter a flotation machine for flotation after being fully stirred, products obtained through concentration are sulfur concentrates, and the tailings are discharged through scavenging; the tailings enter a cyclone through a tailing pump and return to the ball mill for regrinding through underflow; and after overflow enters a spiral chute, the enriched tailings enter the ball mill and the flotation machine for regrinding and re-flotation, the content of gold in the tailings is remarkably reduced, and the tailings of the spiral chute are subjected to three-grade magnetic separation to extract iron concentrates. The method has the beneficial effects that the process is adopted, and therefore the grinded ore fineness of the tailings is improved, the recovery rate is increased to 84% from original 58%, and the grade of the gold in the treated tailings is remarkably reduced.

Description

A kind of method that gold tailings waste residue multielement reclaims
Technical field
The present invention relates to the recovery method of a kind of mine tailing waste residue, particularly relate to a kind of gold tailings waste residue polynary The method that element reclaims, belongs to mine technology field.
Background technology
The waste residue amount that gold ores containing sulfur produces after cyaniding is extracted is very big, especially with people's environmental protection and joint The raising that can realize, the process of the waste residue that smeltery produces just becomes more and more important with recycling, root According to current environmental requirement, waste residue stacking to be built special Tailings Dam and be stacked, and outward transport requirement is compared Strictly.
Traditional mine tailing waste residue mineral processing circuit is: ore deposit is after Vibration Screen takes, and percutaneous band enters feed bin, Again by belt-conveying to ball mill ore grinding, agitated bucket adds xanthate, flotation oil, enters flotation device flotation, Choosing gold sulfur concentrate, mine tailing enters Tailings Dam.Do not have follow-up mine tailing to extract the technique of recovery again, make Having become a large amount of wastes of concentrate resource, the shortcoming of tradition ore-dressing technique is: 1, the ore grinding time is short, ore grinding Fineness is thick.2, the mine tailing after flotation does not has gold sulfur concentrate recycling equipment, slatterns wherein this part essence Ore deposit.
Summary of the invention
The present invention is directed to existing gold tailings waste residue and recycle the deficiency that technique exists, it is provided that a kind of gold The method that mine tailing waste residue multielement reclaims.
The technical scheme is that
A kind of method that gold tailings waste residue multielement reclaims, it is characterised in that comprise the steps:
1) remove impurity: stone, rubbish sieve are become owner of feed bin except laggard through vibrosieve by gold tailings waste residue;
2) ball milling: the waste residue in major ingredient storehouse is delivered to ball mill ore grinding;
3) flotation: step 2) in gained product enter agitator be sufficiently stirred for, be added thereto to xanthate simultaneously And flotation oil, mine tailing per ton adds xanthate 24~26 grams, flotation oil 19~20 grams, enters floating afterwards Selecting machine to carry out flotation, choose iron concentrate, mine tailing is discharged;
4) separate: step 3) in the tailings pump of gained deliver to centrifugal rotational flow device and separate, below gained 100 mesh Thick and the mine tailing waste residue of weight returns ball mill by underflow, gained overflow enters spiral chute gravity treatment, weight The mine tailing that choosing obtains enters magnetic separator and extracts iron ore concentrate, and gained enrichment ore deposit returns ball mill ore grinding again;
5) washed-out sand: the agitated bucket of mine tailing after magnetic separator extraction enters sand washer after being sufficiently stirred for adjusting concentration and washes Ore deposit desliming, the mine tailing after desliming enters flotation device;
6) secondary flotation: with sulfonated petroleum for collecting agent flotation iron containing compounds, adds sulfonation in mine tailing per ton Oil 3360g, chooses iron ore concentrate after being sufficiently stirred for;
7) Anhydrite, quartz are reclaimed: through step 6) after the agitated bucket of mine tailing after flotation is sufficiently stirred for adjusting concentration Enter Anhydrite flotation device, using amine as collecting agent, addition lauryl amine 480g in mine tailing per ton, flotation Anhydrite, Quartz is with the form output of mine tailing.
Further, step 2) in time of ore grinding be 8min.
Further, step 4) described in magnetic separator be three grades of magnetic separators.
The invention has the beneficial effects as follows: the technique mine tailing mog using the present invention to provide improves, and reclaims Rate is from 58% original raising to 84%, and in mine tailing, the grade of gold substantially reduces after treatment.
Accompanying drawing explanation
Fig. 1 is the process chart of the present invention;
Detailed description of the invention
Being described principle and the feature of the present invention below in conjunction with example, example is served only for explaining this Invention, is not intended to limit the scope of invention.
A kind of method that gold tailings waste residue multielement reclaims, comprises the steps:
1) remove impurity: stone, rubbish sieve are become owner of except laggard by the gold tailings waste residue in one-level feed bin through vibrosieve Feed bin;
2) ball milling: the waste residue in major ingredient storehouse is delivered to ball mill ore grinding 8min through belt conveyor;
3) flotation: step 2) in gained product enter agitator be sufficiently stirred for, be added thereto to xanthate simultaneously And flotation oil, mine tailing per ton adds xanthate 24~26 grams, flotation oil 19~20 grams, enters floating afterwards Selecting machine to carry out flotation, choose iron concentrate, mine tailing is discharged;
4) separate: step 3) in the tailings pump of gained deliver to centrifugal rotational flow device and separate, below gained 100 mesh Thick and the mine tailing waste residue of weight returns ball mill by underflow, gained overflow enters spiral chute gravity treatment, weight The mine tailing that choosing obtains enters three grades of magnetic separators and extracts iron ore concentrate, and gained enrichment ore deposit returns ball mill and again grinds Ore deposit;
5) washed-out sand: the agitated bucket of mine tailing after magnetic separator extraction enters sand washer after being sufficiently stirred for adjusting concentration and washes Ore deposit desliming, the mine tailing after desliming enters flotation device;
6) secondary flotation: with sulfonated petroleum for collecting agent flotation iron containing compounds, adds sulfonation in mine tailing per ton Oil 3360g, chooses iron ore concentrate after being sufficiently stirred for;
7) Anhydrite, quartz are reclaimed: through step 6) after the agitated bucket of mine tailing after flotation is sufficiently stirred for adjusting concentration Enter Anhydrite flotation device, using amine as collecting agent, addition lauryl amine 480g in mine tailing per ton, flotation Anhydrite, Quartz is with the form output of mine tailing.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all in the present invention Spirit and principle within, any modification, equivalent substitution and improvement etc. made, should be included in this Within bright protection domain.

Claims (3)

1. the method that a gold tailings waste residue multielement reclaims, it is characterised in that comprise the steps:
1) remove impurity: stone, rubbish sieve are become owner of feed bin except laggard through vibrosieve by gold tailings waste residue;
2) ball milling: the waste residue in major ingredient storehouse is delivered to ball mill ore grinding;
3) classification: by step 2) products therefrom is delivered to grader and is carried out classification after ball milling;
4) flotation: step 3) in gained product enter agitator be sufficiently stirred for, be added thereto to xanthate simultaneously And flotation oil, mine tailing per ton adds xanthate 24~26 grams, flotation oil 19~20 grams, enters floating afterwards Selecting machine to carry out flotation, choose iron concentrate, mine tailing is discharged;
5) separate: step 4) in the tailings pump of gained deliver to centrifugal rotational flow device and separate, below gained 100 mesh Thick and the mine tailing waste residue of weight returns ball mill by underflow, gained overflow enters spiral chute gravity treatment, weight The mine tailing that choosing obtains enters magnetic separator and extracts iron ore concentrate, and gained enrichment ore deposit returns ball mill ore grinding again;
6) washed-out sand: the agitated bucket of mine tailing after magnetic separator extraction enters sand washer after being sufficiently stirred for adjusting concentration and washes Ore deposit desliming, the mine tailing after desliming enters flotation device;
7) secondary flotation: with sulfonated petroleum for collecting agent flotation iron containing compounds, adds sulfonation in mine tailing per ton Oil 3360g, chooses iron ore concentrate after being sufficiently stirred for;
8) Anhydrite, quartz are reclaimed: through step) after the agitated bucket of mine tailing after flotation is sufficiently stirred for adjusting concentration Enter Anhydrite flotation device, using amine as collecting agent, addition lauryl amine 480g in mine tailing per ton, flotation Anhydrite, Quartz is with the form output of mine tailing.
The method that gold tailings waste residue multielement the most according to claim 1 reclaims, its feature exists In, step 2) in time of ore grinding be 8min.
The method that gold tailings waste residue multielement the most according to claim 1 reclaims, its feature exists In, step 4) described in magnetic separator be three grades of magnetic separators.
CN201610579070.6A 2016-07-21 2016-07-21 A kind of method of gold tailings waste residue multielement recovery Active CN106000624B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107876206A (en) * 2017-11-23 2018-04-06 山东九曲圣基新型建材有限公司 A kind of method that gold tailings are fully utilized
CN109894259A (en) * 2019-04-04 2019-06-18 山东华特磁电科技股份有限公司 Gold tailings method of comprehensive utilization containing gold, iron, feldspar
CN112295725A (en) * 2020-10-17 2021-02-02 云南天朗再生资源有限责任公司 Solid waste treatment method

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CN102327808A (en) * 2011-07-29 2012-01-25 中矿金业股份有限公司 Gold tailing treatment process
CN102553706A (en) * 2010-12-20 2012-07-11 北京有色金属研究总院 Process for recycling gold from high-arsenic and high-sulfur difficultly treated gold ore
CN103433124A (en) * 2013-09-18 2013-12-11 江西理工大学 Process for comprehensively recovering ferrum, molybdenum and sericite from gold concentrator tailings
CN103706464A (en) * 2013-12-29 2014-04-09 北票市金海矿业有限公司 Method for extracting gold from gold tailings
US20140112823A1 (en) * 2012-10-23 2014-04-24 Barrick Gold Corporation Recovery of gold from roaster calcine leach tailings
CN104148174A (en) * 2014-08-06 2014-11-19 哈巴河金坝矿业有限公司 Recycling method and device for quartz extracted from gold flotation tailings
CN104841565A (en) * 2015-05-26 2015-08-19 长安大学 Method for recycling gold from gold floatation tailings

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CN102553706A (en) * 2010-12-20 2012-07-11 北京有色金属研究总院 Process for recycling gold from high-arsenic and high-sulfur difficultly treated gold ore
CN102327808A (en) * 2011-07-29 2012-01-25 中矿金业股份有限公司 Gold tailing treatment process
US20140112823A1 (en) * 2012-10-23 2014-04-24 Barrick Gold Corporation Recovery of gold from roaster calcine leach tailings
CN103433124A (en) * 2013-09-18 2013-12-11 江西理工大学 Process for comprehensively recovering ferrum, molybdenum and sericite from gold concentrator tailings
CN103706464A (en) * 2013-12-29 2014-04-09 北票市金海矿业有限公司 Method for extracting gold from gold tailings
CN104148174A (en) * 2014-08-06 2014-11-19 哈巴河金坝矿业有限公司 Recycling method and device for quartz extracted from gold flotation tailings
CN104841565A (en) * 2015-05-26 2015-08-19 长安大学 Method for recycling gold from gold floatation tailings

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107876206A (en) * 2017-11-23 2018-04-06 山东九曲圣基新型建材有限公司 A kind of method that gold tailings are fully utilized
CN107876206B (en) * 2017-11-23 2019-08-16 山东九曲圣基新型建材有限公司 A method of full utilization gold tailings
CN109894259A (en) * 2019-04-04 2019-06-18 山东华特磁电科技股份有限公司 Gold tailings method of comprehensive utilization containing gold, iron, feldspar
CN112295725A (en) * 2020-10-17 2021-02-02 云南天朗再生资源有限责任公司 Solid waste treatment method

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Address after: 264000 comprehensive economic and Industrial Park in Fuhan Town, Zhaoyuan, Shandong

Patentee after: SHANDONG JIUQU SHENGJI NEW BUILDING MATERIAL CO.,LTD.

Address before: 264000 comprehensive economic and industrial park of Fuhan Town, Zhaoyuan City, Weifang, Shandong

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Denomination of invention: A method for multi-element recovery of gold tailings residue

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