CN105973020A - Sectional type condensation heat exchanger rich in volatile organic gas - Google Patents

Sectional type condensation heat exchanger rich in volatile organic gas Download PDF

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Publication number
CN105973020A
CN105973020A CN201610490341.0A CN201610490341A CN105973020A CN 105973020 A CN105973020 A CN 105973020A CN 201610490341 A CN201610490341 A CN 201610490341A CN 105973020 A CN105973020 A CN 105973020A
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CN
China
Prior art keywords
volatile organic
unit
organic gas
stagewise
applicable
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610490341.0A
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Chinese (zh)
Inventor
蔡祥军
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Shanghai Leader Catalyst Co Ltd
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Shanghai Leader Catalyst Co Ltd
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Application filed by Shanghai Leader Catalyst Co Ltd filed Critical Shanghai Leader Catalyst Co Ltd
Priority to CN201610490341.0A priority Critical patent/CN105973020A/en
Publication of CN105973020A publication Critical patent/CN105973020A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28BSTEAM OR VAPOUR CONDENSERS
    • F28B1/00Condensers in which the steam or vapour is separate from the cooling medium by walls, e.g. surface condenser
    • F28B1/02Condensers in which the steam or vapour is separate from the cooling medium by walls, e.g. surface condenser using water or other liquid as the cooling medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0003Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
    • B01D5/0012Vertical tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/0075Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with heat exchanging

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The invention relates to a sectional type condensation heat exchanger rich in volatile organic gas. The sectional type condensation heat exchanger comprises a tube bundle used for allowing gas to be condensed to flow and a barrel surrounding the tube bundle and allowing cold fluid to flow. The barrel is divided into a plurality of sections of barrel body units from top to bottom. Each barrel body unit is provided with an independent shell pass fluid inlet and an independent shell pass fluid outlet. Every two adjacent barrel body units are connected through an intermediate separation layer (5) in a sealed mode. Each intermediate separation layer (5) comprises connecting tubes and a heat insulation face layer. The connecting tubes penetrate through the heat insulation face layers and communicate with the tube bundles of every two adjacent barrel body units. Compared with the prior art, the sectional type condensation heat exchanger has the advantages that equipment is simple, heat exchange loss between the barrel body units is low, and the heat exchange efficiency is high.

Description

A kind of it is applicable to the stagewise condensing heat exchanger rich in volatile organic gas
Technical field
The present invention relates to a kind of condensing heat exchanger, especially relate to a kind of being applicable to rich in volatile organic gas Stagewise condensing heat exchanger.
Background technology
Organic substance produces in medium industry be often taken as solvent at chemical industry, medicine, and a part of organic solvent is in pole Gas just can be evaporated into, along with environmental requirement improves further, to rich in volatile organic gas also at a temperature of low There is tightened up discharge standard, waste gas produced in preparation process typically can first have been carried out condensation process, then Such as it is catalyzed oxidation or the purified treatment of multi-stage condensing recovery.And if condensation process can reach well to imitate Really, subsequent treatment amount can be just significantly reduced.
Condensation separation method is to utilize the low-boiling characteristic of volatile organic matter, and after temperature reduces, boiling point is higher Out, it is critical only that of this technique provides enough colds to make Organic substance condense to volatile organic matter condensation separation.Pass Equipment that the multiple stage heat exchanger of system exists and the problem such as pipeline is the compactest, SR is big.
Document CN 103028269 A first borrow the condenser of upstream divided by most water solublity volatile organic matter Separate out, then downstream water sprinkler be set utilize water sprinkler that the off-gas flows that passes through is sprayed water smoke, allow downstream Condenser condenses out more water droplet and absorbs water solublity volatile organic matter.This method is unsuitable for organic repetition profit With.
Cooling unit and mistake in CN 104390495 A, condensing heat exchanger primary structure includes condenser body, pipe Cold unit, is mainly interposed between the steam heat-exchanging in heat exchanger tube in two canister unit by dividing plate and is respectively divided into two journeys, Guarantee that each journey steam flow rate keeps uniform substantially.The condenser of this kind of device does not has condensate recovery device, application Extensive, VOC is reclaimed in the most inapplicable and condensation.
CN 103822510 A mainly describes muitishell tubular heat exchanger, mainly will by sealing dividing plate The shell side of heat transfer zone is divided into the plural separate sub-district of shell side heat exchange, and the independent sub-district of shell side heat exchange sets There are independent shell-side fluid import and shell side fluid outlet.The design of this kind of device is for equipment cooling or the intensification temperature difference not Time big the most applicable, but it seals the simple isolation of dividing plate, can not reduce the heat exchange energy of big temperature difference shell-side fluid Amount loss, and this kind of equipment do not has a lime set collection device, inapplicable with the gas converting heat having lime set.
Summary of the invention
Defect that the purpose of the present invention is contemplated to overcome above-mentioned prior art to exist and provide one be applicable to rich in The stagewise condensing heat exchanger of volatile organic gas.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of it is applicable to the stagewise condensing heat exchanger rich in volatile organic gas, flows including for gas to be condensed Tube bank and surround tube bank and cooling fluid flowing cylinder, this cylinder is divided into multistage canister unit from top to bottom, Every section of canister unit is equipped with independent shell side fluid inlet and shell side fluid outlet, between two adjacent canister unit Being tightly connected by middle insulating course, the tube bank between adjacent two canister unit through insulating course and is connected.
Described middle insulating course includes connecting tube and insulation surface layer, and described connecting tube is through insulation surface layer, and connects Tube bank between logical adjacent two canister unit.Connecting tube can also use the high-strength insulation equally with heat-insulating capability Material is made, and insulation surface layer can be multi-layer compound structure.
Described middle insulating course is connected with canister unit integral type.
Described cylinder is divided into top canister unit and lower cylinder unit two sections, wherein, the shell of top canister unit The temperature of Cheng Liuti is less than the temperature of the shell-side fluid of lower cylinder unit.
The shell-side fluid of described top canister unit is that room temperature cools down water, and the shell-side fluid of lower cylinder unit is low Temperature chilled water.
Described lower cylinder unit is provided with expansion joint.
In the gas access being arranged above and restraining connection of described cylinder, it is also equipped with collection in the bottom of cylinder Flow container, the sidepiece of liquid collecting tank is additionally provided with gas outlet, and bottom is provided with condensate outlet.
It is provided with far transmission level meter in described liquid collecting tank, at condensate outlet, is additionally provided with pneumatic operated valve, described teletransmission Liquidometer is all connected with automatic control system with pneumatic operated valve.
Described tube bank is straight tube structure.
The present invention by being divided into top canister unit and lower cylinder unit by shell side, and two independent canister unit divide Other and tube side forms heat exchange subregion cooling unit and condensing unit.Top canister unit is can be room temperature cooling heat transferring Canister unit, lower cylinder unit is can be condensation at low temperature heat exchanger tube body unit, it is also possible to set according to actual needs Put the heat transfer temperature difference of top cylinder and lower cylinder.So, the gas condensation process first passes through the normal of cooling unit Temperature cooling, portion gas condenses, and condenses further along with the gas of incoagulability enters condensing unit, the most permissible Being promoted by incoagulable gas makes lime set collect faster.In lower cylinder unit, shell-side fluid is freezing water, This section is provided with expansion joint, and what minimizing cold and hot liquids flowing caused can effectively reduce volatility to equipment injury simultaneously has The temperature of machine thing, reaches well to condense recovery purpose.
Compared with prior art, the invention have the advantages that
(1) by the setting of multistage shell side, it is possible to achieve utilize the space of a heat transmission equipment and heat exchange area to reach To the purpose of series connection heat transmission equipment, effectively save equipment cost, the connection between equipment and pipeline can be reduced, save Installation cost, can also reduce because multiple stage condenser is used in conjunction the fluid resistance caused simultaneously, increase the heat transfer system of condenser Number, improves heat exchange efficiency, and the condensation that can well improve volatile organic matter is reclaimed.
(2) fluid between each section of shell side all has individually import and export, and improve heat transmission equipment utilizes scope, This kind of heat transmission equipment can need to change the temperature difference of heat transferring medium according to different technique, reaches heat transfer effect.
(3) heat transfer coefficient of heat transmission equipment is improved: in the middle of the present invention, insulating course is to comprise tube bank and heat-preservation cotton layer, Wherein tube bank is connected with the tube bank of upper and lower canister unit, and insulating course and upper lower shell are the connected modes of integral type. The infiltration of middle insulating course different cold flow bodies in being possible to prevent upper and lower cylinder shell side and temperature shadow each other Ring, it is to avoid owing to the excessive generation of fluid temperature difference cold in upper and lower cylinder can cause the phenomenon of the cold fluid freeze of one of which. Insulation surface layer in middle insulating course can effectively reduce the heat transfer between the cold flow body in upper and lower cylinder, reduces cold The heat loss of fluid, effectively utilizes the cold of cold flow body, improves heat exchange efficiency.The expansion arranged on the cylinder of its underpart Joint is prevented from the impact for equipment barrel material of expanding with heat and contract with cold, and improves service life and the utilization rate of equipment.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention;
In figure, 1-gas access, 2-gas outlet, 3-condensate outlet, 4-bobbin carriage, insulating course in the middle of 5-, 6- Top cylinder shell side, 7-lower cylinder shell side, 8-top shell side inlet, 9-top shell-side outlet, 10-bottom shell side Entrance, 11-bottom shell-side outlet, 12-expansion joint, 13-top canister unit, 14-lower cylinder unit, 15-collection Flow container.
Detailed description of the invention
The present invention is described in detail with specific embodiment below in conjunction with the accompanying drawings.
Embodiment 1
A kind of being applicable to the stagewise condensing heat exchanger rich in volatile organic gas, its structure is as it is shown in figure 1, bag Include the tube bank in straight tube structure for gas to be condensed flowing and surround tube bank the cylinder of cooling fluid flowing, cylinder Body top is provided with bobbin carriage 4, and bobbin carriage 4 arranges gas access 1, and the bottom of cylinder is provided with liquid collecting tank 15, collection The sidepiece of flow container 15 is additionally provided with gas outlet 2, and bottom is provided with condensate outlet 3, is provided with teletransmission in liquid collecting tank 15 Liquidometer, is additionally provided with pneumatic operated valve at condensate outlet 3, and far transmission level meter and pneumatic operated valve are all and automatic control system Connect.
Cylinder is divided into top canister unit 13 and lower cylinder unit 14 two sections, top canister unit from top to bottom Walking room temperature cooling water in the top cylinder shell side 6 of 13, the lower cylinder shell side 7 of lower cylinder unit 14 walks low temperature Chilled water, lower cylinder unit 14 is additionally provided with expansion joint 12, top canister unit 13 and lower cylinder unit It is respectively equipped with independent shell-side fluid on 14 to import and export: the top shell side inlet 8 that is sequentially distributed from top to bottom, top Shell-side outlet 9, bottom shell side inlet 10 and bottom shell-side outlet 11.
It is tightly connected by middle insulating course 5 between top canister unit 13 and lower cylinder unit 14, middle interval Tomography 5 includes connecting tube and insulation surface layer, and connecting tube is through insulation surface layer, and connects between adjacent two canister unit Tube bank, middle insulating course 5 is connected with canister unit integral type.
The above-mentioned description to embodiment is to be understood that for ease of those skilled in the art and use to send out Bright.These embodiments obviously easily can be made various amendment by person skilled in the art, and at this The General Principle illustrated is applied in other embodiments without through performing creative labour.Therefore, the present invention does not limits In above-described embodiment, those skilled in the art are according to the announcement of the present invention, without departing from changing that scope is made Entering and revise all should be within protection scope of the present invention.

Claims (8)

1. it is applicable to the stagewise condensing heat exchanger rich in volatile organic gas, including for gas to be condensed The cylinder that the tube bank of flowing and encirclement tube bank cooling fluid are flowed, this cylinder is divided into multistage cylinder list from top to bottom Unit, every section of canister unit is equipped with independent shell side fluid inlet and shell side fluid outlet, it is characterised in that adjacent Two canister unit between be tightly connected by middle insulating course (5), described middle insulating course (5) includes company Adapter and insulation surface layer, described connecting tube is through insulation surface layer, and connects the tube bank between adjacent two canister unit.
The most according to claim 1 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that described middle insulating course (5) is connected with canister unit integral type.
The most according to claim 1 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that described cylinder is divided into top canister unit (13) and lower cylinder unit (14) two sections, Wherein, the temperature of the shell-side fluid of top canister unit (13) is less than the shell-side fluid of lower cylinder unit (14) Temperature.
The most according to claim 3 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that the shell-side fluid of described top canister unit (13) is that room temperature cools down water, lower cylinder The shell-side fluid of unit (14) is freezing water.
The most according to claim 3 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that described lower cylinder unit (14) is provided with expansion joint (12).
The most according to claim 1 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that in the gas access (1) being arranged above and restraining connection of described cylinder, at cylinder Bottom be also equipped with liquid collecting tank (15), the sidepiece of liquid collecting tank (15) is additionally provided with gas outlet (2), and bottom sets There is condensate outlet (3).
The most according to claim 6 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that be provided with far transmission level meter in described liquid collecting tank (15), at condensate outlet (3) place Being additionally provided with pneumatic operated valve, described far transmission level meter is all connected with automatic control system with pneumatic operated valve.
The most according to claim 1 a kind of it is applicable to the stagewise condensing heat-exchange rich in volatile organic gas Device, it is characterised in that described tube bank is straight tube structure.
CN201610490341.0A 2016-06-29 2016-06-29 Sectional type condensation heat exchanger rich in volatile organic gas Pending CN105973020A (en)

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CN201610490341.0A CN105973020A (en) 2016-06-29 2016-06-29 Sectional type condensation heat exchanger rich in volatile organic gas

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Application Number Priority Date Filing Date Title
CN201610490341.0A CN105973020A (en) 2016-06-29 2016-06-29 Sectional type condensation heat exchanger rich in volatile organic gas

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106440849A (en) * 2016-11-03 2017-02-22 江苏海云花新材料有限公司 Vertical condenser for spinning ultra-smooth silicone oil production

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2491798Y (en) * 2001-04-25 2002-05-15 中国华陆工程公司 Fixed bed shell-and-tube heat exchanging reactor
CN102022925A (en) * 2010-11-12 2011-04-20 中冶焦耐(大连)工程技术有限公司 Method and equipment for condensing and cooling flash oil
CN104390495A (en) * 2014-12-03 2015-03-04 北京交通大学 Undercooling type condensation heat exchanger and heat exchange method thereof
CN204337811U (en) * 2014-11-24 2015-05-20 宁波浙铁江宁化工有限公司 The equipment complex of a kind of overhead condenser and return tank
CN205860800U (en) * 2016-06-29 2017-01-04 上海立得催化剂有限公司 A kind of it is applicable to the stagewise condensing heat exchanger rich in volatile organic gas

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2491798Y (en) * 2001-04-25 2002-05-15 中国华陆工程公司 Fixed bed shell-and-tube heat exchanging reactor
CN102022925A (en) * 2010-11-12 2011-04-20 中冶焦耐(大连)工程技术有限公司 Method and equipment for condensing and cooling flash oil
CN204337811U (en) * 2014-11-24 2015-05-20 宁波浙铁江宁化工有限公司 The equipment complex of a kind of overhead condenser and return tank
CN104390495A (en) * 2014-12-03 2015-03-04 北京交通大学 Undercooling type condensation heat exchanger and heat exchange method thereof
CN205860800U (en) * 2016-06-29 2017-01-04 上海立得催化剂有限公司 A kind of it is applicable to the stagewise condensing heat exchanger rich in volatile organic gas

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106440849A (en) * 2016-11-03 2017-02-22 江苏海云花新材料有限公司 Vertical condenser for spinning ultra-smooth silicone oil production

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Application publication date: 20160928