CN105970352A - Ultraviolet aging resistant artificial wig fibers containing peacock feathers - Google Patents
Ultraviolet aging resistant artificial wig fibers containing peacock feathers Download PDFInfo
- Publication number
- CN105970352A CN105970352A CN201610343103.7A CN201610343103A CN105970352A CN 105970352 A CN105970352 A CN 105970352A CN 201610343103 A CN201610343103 A CN 201610343103A CN 105970352 A CN105970352 A CN 105970352A
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- CN
- China
- Prior art keywords
- hair
- peafowl hair
- peafowl
- fibers
- ultraviolet aging
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/08—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyacrylonitrile as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses ultraviolet aging resistant artificial wig fibers containing peacock feathers. The wig fibers have the advantages that (1) a polyacrylonitrile and polycaprolactone mixture is taken as a fiber base material, so the fibers have good biocompatibility, better experience of use on hair and moist and smooth hand feelings, are more oil-moist and are not like to dry up; (2) the peacock feathers are processed into nanoscale fillers, thus not destroying the natural biological structures and colors of the peacock feathers and improving the natural feelings of the fibers; nano zinc oxide is added and mixed with the nanoscale peacock feathers and then nano zinc oxide and the nanoscale peacock feathers are uniformly combined and dispersed in a spinning solution, thus stably improving the comprehensive properties of the fibers; (3) the prepared wig fibers are antibacterial, lightfast, breathable, moist, comfortable, submissive, economical and durable, have affinity with skin and have the effect of greatly increasing the quality and grades of synthetic fiber wigs.
Description
Technical field
The present invention relates to synthetic wig fiber technical field, particularly relate to a kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair.
Background technology
Peafowl whole body is precious, the especially feather of its gorgeous uniqueness, make us looking over so as to check unforgettable, the scale of peafowl cultivation in recent years gradually expands, also it is expanded about peafowl hair application industry, multiplex in conventional industries being used for making ornament and artware by tail feathers, and the feather of major part is taken as offal treatment, and utilization rate is extremely low.
Wig is a kind of common ornament, feather application in wig product at present mainly has two aspects: one is to extract the keratin in feather, again it is mixed to prepare with macromolecular material, but the product for preparing of this method does not the most possess breathability and the comfortableness of natural feather, and destroy the natural color and luster of feather and texture；Two is directly to connect with wig fiber, the product general moulding exaggeration so obtained, and lacks natural sense, and range of application is narrower.The current application about peafowl hair on wig also rarely has report, it is contemplated that peafowl hair is introduced in wig, the defect of the tradition wig containing feather fiber is improved, it is thus achieved that there is the novel wig product of practicality, aesthetic property, safety while retaining the color that peafowl hair is unique.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair.
The present invention is achieved by the following technical solutions:
A kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair, this wig fiber is prepared by the raw material of following weight portion: modified Nano peafowl hair 6-10, polycaprolactone 10-15, polyacrylonitrile 30-40, antistatic additive 0.1-0.2, pigment 1-10, nano zine oxide, silane coupler 0.5-0.8, spin solvent 180-220, quaternary ammonium salt ionic liquid 15-25, coagulating bath are appropriate.
Described modified peafowl hair is processed by following methods and obtains: by the peafowl hair of collection through sterilization, defat, cleaning, crushed after being dried, cross 80-100 mesh sieve, put into immersion treatment 1.5-2h in modification liquid subsequently, immersion is filtered after terminating, in gained material input air flow pulverizer the most cleaned, dried, be 0-60 DEG C in temperature, speed be 120-200 meter per second air stream in be processed into nano level modified peafowl hair.
Described modification liquid is mixed compounding making by the raw material of following weight portion: solid content is the nano titanic oxide sol 20-30 of 20-25%, chitosan quaternary ammonium salt 0.1-0.2, tannic acid 1-2, deionized water 40-50.
The preparation method of described a kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair is:
(1) polyacrylonitrile, polycaprolactone are put in spin solvent, it is heated to 60-80 DEG C, high-speed stirred mixing makes high polymer be completely dissolved, filtering and impurity removing subsequently, gained filtrate adds pigment, antistatic additive, grinding distribution 40-50min, makes spinning solution standby, and described spin solvent is the one in dimethylformamide, dimethyl acetylamide, dimethyl sulfoxide；
(2) modified Nano peafowl hair, nano zine oxide are put in quaternary ammonium salt ionic liquid after silane coupler mixed grinding 20-30min, mixing 2-3h is stirred with the speed of 400-500 rev/min, subsequently its spinning solution prepared with step (1) is mixed, after stirring, mixed serum is extruded by spinneret cap micropore, and immersion 2-5h makes tow in coagulating bath, described coagulating bath is formulated according to the weight ratio of 0.1:0.5-1 with deionized water by spin solvent；
(3) tow step (2) prepared stretches 3-5 time after 30-50 DEG C of warm water washing under 50-60 DEG C of hot blast, shrink process 20-30min in the hot-air of 60-65 DEG C the most again, finally after its surface uniformly coats silicone oil under the conditions of 50-60 DEG C wig fiber described in drying.
The wig fiber that the present invention prepares has the advantage that
(1) mixing as fiber base material using polyacrylonitrile and polycaprolactone so that fiber has good biocompatibility, hair is experienced more preferably, and feel lubrication, and fiber is more glossy, and it is withered short-tempered to be difficult to.
(2) peafowl hair is processed into the filler of nanometer scale, does not destroy the natural biological structure of peafowl hair and color, improve the natural sense of fiber；Add nano zine oxide in spinning liquid, be uniformly combined dispersion, the stable combination property improving fiber after the peafowl hair mixed processing of nanometer scale.
(3) to prepare wig fibre antibacterial fast light for the present invention, and pro-skin is breathed freely, and profit is refreshing docile, and economy and durability greatly improves quality and the class of synthetic fibers class wig.
Detailed description of the invention
This wig fiber is prepared by the raw material of following weight portion: modified Nano peafowl hair 6, polycaprolactone 10, polyacrylonitrile 30, antistatic additive 0.1, pigment 1, nano zine oxide, silane coupler 0.5, spin solvent 180, quaternary ammonium salt ionic liquid 15, coagulating bath are appropriate.
Wherein modified peafowl hair is processed by following methods and obtains: by the peafowl hair of collection through sterilization, defat, cleaning, crushed after being dried, cross 80 mesh sieves, put into immersion treatment 1.5h in modification liquid subsequently, immersion is filtered after terminating, in gained material input air flow pulverizer the most cleaned, dried, be 0 DEG C in temperature, speed be 120 meter per seconds air stream in be processed into nano level modified peafowl hair.
Wherein modification liquid is mixed compounding making by the raw material of following weight portion: solid content be 20% nano titanic oxide sol 20, chitosan quaternary ammonium salt 0.1, tannic acid 1, deionized water 40.
The preparation method of this synthetic wig fiber is:
(1) polyacrylonitrile, polycaprolactone are put in spin solvent, it is heated to 60 DEG C, high-speed stirred mixing makes high polymer be completely dissolved, filtering and impurity removing subsequently, gained filtrate adds pigment, antistatic additive, grinding distribution 40min, makes spinning solution standby, and described spin solvent is the one in dimethylformamide, dimethyl acetylamide, dimethyl sulfoxide；
(2) modified Nano peafowl hair, nano zine oxide are put in quaternary ammonium salt ionic liquid after silane coupler mixed grinding 20min, mixing 2h is stirred with the speed of 400 revs/min, subsequently its spinning solution prepared with step (1) is mixed, after stirring, mixed serum is extruded by spinneret cap micropore, and immersion 2h makes tow in coagulating bath, described coagulating bath is formulated according to the weight ratio of 0.1:0.5 with deionized water by spin solvent；
(3) tow step (2) prepared stretches 3 times after the washing of 30 DEG C of warm water under 50 DEG C of hot blasts, shrink process 20min in the hot-air of 60 DEG C the most again, finally after its surface uniformly coats silicone oil under the conditions of 50 DEG C wig fiber described in drying.
The performance indications that this wig fiber obtains after tested are as follows: filament number: 40.6dtex；Fracture strength: 4.6CN/dtex；Elongation at break: 15.2%.
Claims (4)
1. the ultraviolet aging resistance synthetic wig fiber containing peafowl hair, it is characterized in that, this wig fiber is prepared by the raw material of following weight portion: modified Nano peafowl hair 6-10, polycaprolactone 10-15, polyacrylonitrile 30-40, antistatic additive 0.1-0.2, pigment 1-10, nano zine oxide, silane coupler 0.5-0.8, spin solvent 180-220, quaternary ammonium salt ionic liquid 15-25, coagulating bath are appropriate.
A kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair, it is characterized in that, described modified peafowl hair is processed by following methods and obtains: by the peafowl hair of collection through sterilization, defat, cleaning, crushed after being dried, cross 80-100 mesh sieve, put into immersion treatment 1.5-2h in modification liquid subsequently, immersion is filtered after terminating, in gained material input air flow pulverizer the most cleaned, dried, be 0-60 DEG C in temperature, speed be 120-200 meter per second air stream in be processed into nano level modified peafowl hair.
A kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair, it is characterized in that, described modification liquid is mixed compounding making by the raw material of following weight portion: solid content is the nano titanic oxide sol 20-30 of 20-25%, chitosan quaternary ammonium salt 0.1-0.2, tannic acid 1-2, deionized water 40-50.
The preparation method of a kind of ultraviolet aging resistance synthetic wig fiber containing peafowl hair is:
(1) polyacrylonitrile, polycaprolactone are put in spin solvent, it is heated to 60-80 DEG C, high-speed stirred mixing makes high polymer be completely dissolved, filtering and impurity removing subsequently, gained filtrate adds pigment, antistatic additive, grinding distribution 40-50min, makes spinning solution standby, and described spin solvent is the one in dimethylformamide, dimethyl acetylamide, dimethyl sulfoxide；
(2) modified Nano peafowl hair, nano zine oxide are put in quaternary ammonium salt ionic liquid after silane coupler mixed grinding 20-30min, mixing 2-3h is stirred with the speed of 400-500 rev/min, subsequently its spinning solution prepared with step (1) is mixed, after stirring, mixed serum is extruded by spinneret cap micropore, and immersion 2-5h makes tow in coagulating bath, described coagulating bath is formulated according to the weight ratio of 0.1:0.5-1 with deionized water by spin solvent；
(3) tow step (2) prepared stretches 3-5 time after 30-50 DEG C of warm water washing under 50-60 DEG C of hot blast, shrink process 20-30min in the hot-air of 60-65 DEG C the most again, finally after its surface uniformly coats silicone oil under the conditions of 50-60 DEG C wig fiber described in drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610343103.7A CN105970352A (en) | 2016-05-23 | 2016-05-23 | Ultraviolet aging resistant artificial wig fibers containing peacock feathers |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610343103.7A CN105970352A (en) | 2016-05-23 | 2016-05-23 | Ultraviolet aging resistant artificial wig fibers containing peacock feathers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105970352A true CN105970352A (en) | 2016-09-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610343103.7A Pending CN105970352A (en) | 2016-05-23 | 2016-05-23 | Ultraviolet aging resistant artificial wig fibers containing peacock feathers |
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| CN (1) | CN105970352A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107268134A (en) * | 2017-08-09 | 2017-10-20 | 太仓市天茂化纤有限公司 | One kind has very good sunproof fibers material |
Citations (6)
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|---|---|---|---|---|
| CN101037813A (en) * | 2007-03-30 | 2007-09-19 | 东华大学 | Preparation method of spinning hairpiece by human hair and protein acrylic fibre |
| CN101096785A (en) * | 2007-06-27 | 2008-01-02 | 东华大学 | Process for producing fire retardant man-made protein hair |
| CN101250763A (en) * | 2008-03-11 | 2008-08-27 | 东华大学 | Long-acting medicine-loading orlon fibre capable of degrading partly, preparation and application thereof |
| CN101250764A (en) * | 2008-03-11 | 2008-08-27 | 东华大学 | Nanometer medicine-loading orlon fibre, preparation and application |
| CN101760803A (en) * | 2009-11-06 | 2010-06-30 | 苏州双轮化纤有限公司 | Superfine full-dull uvioresistant sheath-core fiber |
| CN102286800A (en) * | 2011-05-30 | 2011-12-21 | 上海瑞贝卡纤维材料科技有限公司 | Functional modified acrylic fiber for hair and preparation method thereof |
-
2016
- 2016-05-23 CN CN201610343103.7A patent/CN105970352A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101037813A (en) * | 2007-03-30 | 2007-09-19 | 东华大学 | Preparation method of spinning hairpiece by human hair and protein acrylic fibre |
| CN101096785A (en) * | 2007-06-27 | 2008-01-02 | 东华大学 | Process for producing fire retardant man-made protein hair |
| CN101250763A (en) * | 2008-03-11 | 2008-08-27 | 东华大学 | Long-acting medicine-loading orlon fibre capable of degrading partly, preparation and application thereof |
| CN101250764A (en) * | 2008-03-11 | 2008-08-27 | 东华大学 | Nanometer medicine-loading orlon fibre, preparation and application |
| CN101760803A (en) * | 2009-11-06 | 2010-06-30 | 苏州双轮化纤有限公司 | Superfine full-dull uvioresistant sheath-core fiber |
| CN102286800A (en) * | 2011-05-30 | 2011-12-21 | 上海瑞贝卡纤维材料科技有限公司 | Functional modified acrylic fiber for hair and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107268134A (en) * | 2017-08-09 | 2017-10-20 | 太仓市天茂化纤有限公司 | One kind has very good sunproof fibers material |
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Application publication date: 20160928 |
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| RJ01 | Rejection of invention patent application after publication |