CN105926269A - Preparation method for recombined finishing agent - Google Patents

Preparation method for recombined finishing agent Download PDF

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Publication number
CN105926269A
CN105926269A CN201610362144.0A CN201610362144A CN105926269A CN 105926269 A CN105926269 A CN 105926269A CN 201610362144 A CN201610362144 A CN 201610362144A CN 105926269 A CN105926269 A CN 105926269A
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China
Prior art keywords
parts
preparation
finishing agent
composite finishing
mixed liquor
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610362144.0A
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Chinese (zh)
Inventor
史卫红
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JIANGSU DESHENGTE TEXTILE Co Ltd
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JIANGSU DESHENGTE TEXTILE Co Ltd
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Priority to CN201610362144.0A priority Critical patent/CN105926269A/en
Publication of CN105926269A publication Critical patent/CN105926269A/en
Pending legal-status Critical Current

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
    • D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
    • D06M13/268—Sulfones
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/39—Aldehyde resins; Ketone resins; Polyacetals
    • D06M15/423—Amino-aldehyde resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30—Flame or heat resistance, fire retardancy properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a preparation method for a recombined finishing agent. The preparation method comprises the following steps that firstly, 44-55 parts of fire retardant is taken and heated to a certain temperature, and 15-25 parts of etherifled hexamethylolmelamine resin is taken and shocked in a constant-temperature shocking pot for 20 minutes to be mixed fully; secondly, 3-7 parts of diamino diphenyl sulfone and 5-15 parts of an antibacterial agent are added into the mixed liquid to be heated to a certain temperature, a certain stirring speed is controlled, and stirring is carried out for 30 min; thirdly, 10-20 parts of phosphoric acid is added into the mixed liquid in the second step, and PH of the mixed liquid is adjusted to be 4-5; fourthly, 2-3 parts of a softening agent and 8-9 parts of octylphenyl salicylate are added into the mixed liquid in the third step, a certain stirring speed is controlled, and stirring is carried out for 30 min. The preparation method for the recombined finishing agent can prepare the recombined finishing agent with multiple good functions of preventing ultraviolet, resisting inflaming and bacteria and the like.

Description

The preparation method of composite finishing agent
Technical field
The disclosure relates generally to field of textiles, is specifically related to weaving additive preparation field, especially It relates to the preparation method of a kind of composite finishing agent.
Background technology
Textile finishing is to apply a kind of finishing agent on fabric, and it can change the surface property of fabric, Thus give the function that fabric is special.Such as hydrophobic and oil repellent arranges to have low surface tension Finishing agent processes fabric, changes the surface characteristic of fiber, makes fabric face be difficult to by water or glossy Wet and sprawl, thus reach the purpose of hydrophobic and oil repellent.Soil resistant finish and soil-releasing finiss are to pass through Change surface property or the apparent condition of fiber, make fabric be difficult to be stained with under the conditions of dress, use Attached dirt, or the dirt attached is prone to wash the processing technique of not recontamination.
Current finishing agent function is more single, prepares more complicated.
Summary of the invention
In view of drawbacks described above of the prior art or deficiency, it is desirable to provide one to prepare simple, many The preparation method of the composite finishing agent of function.
First aspect, the preparation method of a kind of composite finishing agent, preparation method is by following steps group Become:
Step one, takes fire retardant 45～55 parts, is heated to uniform temperature, takes etherificate hexamethylol Melmac 15～25 parts, shake 20 minutes so that it is be sufficiently mixed in isothermal vibration pot；
Step 2, adds DADPS 3～7 parts, antibacterial 5～15 in above-mentioned mixed liquor Part, it is heated to uniform temperature, controls certain mixing speed, stir 30min；
Step 3, adds phosphatase 11 0～20 parts, adjusts mixed liquor in the mixed liquor in step 2 PH to 4～5；
Step 4, adds softening agent 2～3 parts and salicylic acid to pungent in the mixed liquor of step 3 kind Base phenylester 8～9 parts, control certain mixing speed, stirs 30min.
The technical scheme provided according to the embodiment of the present application, the preparation of the composite finishing agent of the application Method can prepare have preferable anti-ultraviolet, the several functions such as fire-retardant, antibacterial compound Finishing agent.
Detailed description of the invention
Below in conjunction with embodiment, the application is described in further detail.It is understood that Specific embodiment described herein is used only for explaining related invention, rather than the limit to this invention Fixed.
It should be noted that in the case of not conflicting, the embodiment in the application and embodiment In feature can be mutually combined.The application is described in detail below with reference to embodiment.
Embodiment one
A kind of preparation method of composite finishing agent, preparation method is made up of following steps:
Step one, takes fire-retardant N TF-9045L45 part, is heated to 40 DEG C, takes etherificate six hydroxyl first Base melmac 15 parts, shakes 20 minutes so that it is be sufficiently mixed in isothermal vibration pot；
Step 2, adds DADPS 3 parts, magnesium oxide, oxidation in above-mentioned mixed liquor 5 parts of the mixture of calcium, is heated to 30 DEG C, and controlling mixing speed is 100 revs/min, stirring 30min；
Step 3, adds phosphatase 11 0 part, adjusts mixed liquor in the mixed liquor in step 2 PH to 4；
Step 4, adds softening agent 2 parts and salicylic acid to octyl group in the mixed liquor of step 3 kind Phenylester 8 parts, controlling mixing speed is 100 revs/min, stirs 30min.
Softening agent according to the mass fraction, comprises following components:
Organosilicon quaternary ammonium salt: 65 parts,
Amido silicon oil: 45 parts.
Embodiment two
A kind of preparation method of composite finishing agent, preparation method is made up of following steps:
Step one, takes fire-retardant N TF-9045L55 part, is heated to 60 DEG C, takes etherificate six hydroxyl first Base melmac 25 parts, shakes 20 minutes so that it is be sufficiently mixed in isothermal vibration pot；
Step 2, adds DADPS 7 parts, zinc oxide, oxidation in above-mentioned mixed liquor 15 parts of the mixture of calcium, is heated to 50 DEG C, and controlling mixing speed is 200 revs/min, stirring 30min；
Step 3, adds phosphoric acid 20 parts, adjusts mixed liquor in the mixed liquor in step 2 PH to 5；
Step 4, adds softening agent 3 parts and salicylic acid to octyl group in the mixed liquor of step 3 kind Phenylester 9 parts, controlling mixing speed is 200 revs/min, stirs 30min.
Softening agent according to the mass fraction, comprises following components:
Organosilicon quaternary ammonium salt: 85 parts,
Amido silicon oil: 55 parts.
Embodiment three
A kind of preparation method of composite finishing agent, preparation method is made up of following steps:
Step one, takes fire-retardant N TF-9045L50 part, is heated to 60 DEG C, takes etherificate six hydroxyl first Base melmac 20 parts, shakes 20 minutes so that it is be sufficiently mixed in isothermal vibration pot；
Step 2, adds DADPS 5 parts, zinc oxide, oxidation in above-mentioned mixed liquor 10 parts of the mixture of calcium, is heated to 40 DEG C, and controlling mixing speed is 150 revs/min, stirring 30min；
Step 3, adds phosphatase 11 5 parts, adjusts mixed liquor in the mixed liquor in step 2 PH to 5；
Step 4, adds softening agent 3 parts and salicylic acid to octyl group in the mixed liquor of step 3 kind Phenylester 9 parts, controlling mixing speed is 150 revs/min, stirs 30min.
Softening agent according to the mass fraction, comprises following components:
Organosilicon quaternary ammonium salt: 75 parts,
Amido silicon oil: 50 parts.
The composite finishing agent that the preparation method of the composite finishing agent of the present invention prepares has anti-purple The features such as outside line, antibacterial, anti-flammability, and corresponding various aspects of performance is than single Use Limitation Fruit is better, and preparation method is fairly simple.
Above description is only the preferred embodiment of the application and saying institute's application technology principle Bright.It will be appreciated by those skilled in the art that invention scope involved in the application, do not limit In the technical scheme of the particular combination of above-mentioned technical characteristic, also should contain simultaneously without departing from In the case of described inventive concept, above-mentioned technical characteristic or its equivalent feature carry out combination in any And other technical scheme formed.Such as features described above and (but not limited to) disclosed herein The technical characteristic with similar functions is replaced mutually and the technical scheme that formed.

Claims (8)

1. the preparation method of a composite finishing agent, it is characterised in that described preparation method is by such as Lower step forms:
Step one, takes fire retardant 45～55 parts, is heated to uniform temperature, takes etherificate hexamethylol Melmac 15～25 parts, shake 20 minutes so that it is be sufficiently mixed in isothermal vibration pot；
Step 2, adds DADPS 3～7 parts, antibacterial 5～15 in above-mentioned mixed liquor Part, it is heated to uniform temperature, controls certain mixing speed, stir 30min；
Step 3, adds phosphatase 11 0～20 parts, adjusts mixed liquor in the mixed liquor in step 2 PH to 4～5；
Step 4, adds softening agent 2～3 parts and salicylic acid to pungent in the mixed liquor of step 3 kind Base phenylester 8～9 parts, control certain mixing speed, stirs 30min.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that The heating-up temperature of described step one is 40-60 DEG C.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that Heating-up temperature in described step 2 is 30-50 DEG C.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that The concussion speed of described step one is 100-200 rev/min.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that Mixing speed in described step 2 is 100-200 rev/min.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that Described antibacterial is one or more the combination in magnesium oxide, calcium oxide, zinc oxide.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that Described fire retardant is NTF-9045L.
The preparation method of composite finishing agent the most according to claim 1, it is characterised in that Described softening agent according to the mass fraction, comprises following components:
Organosilicon quaternary ammonium salt: 65～85 parts,
Amido silicon oil: 45～55 parts.
CN201610362144.0A 2016-05-26 2016-05-26 Preparation method for recombined finishing agent Pending CN105926269A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610362144.0A CN105926269A (en) 2016-05-26 2016-05-26 Preparation method for recombined finishing agent

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Application Number Priority Date Filing Date Title
CN201610362144.0A CN105926269A (en) 2016-05-26 2016-05-26 Preparation method for recombined finishing agent

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CN105926269A true CN105926269A (en) 2016-09-07

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102337669A (en) * 2010-07-19 2012-02-01 苏州市统业化工有限公司 Method for processing antibacterial wool fiber
CN102505481A (en) * 2011-10-11 2012-06-20 南通市田园装饰布有限公司 Environmental-friendly yarn soil release decorative fabric
CN103146054A (en) * 2013-02-21 2013-06-12 合肥杰事杰新材料股份有限公司 Modified jute fiber reinforced polypropylene and its preparation method
CN104594030A (en) * 2015-01-26 2015-05-06 江苏文凤化纤集团有限公司 Preparation method for spinning composite finishing agent

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102337669A (en) * 2010-07-19 2012-02-01 苏州市统业化工有限公司 Method for processing antibacterial wool fiber
CN102505481A (en) * 2011-10-11 2012-06-20 南通市田园装饰布有限公司 Environmental-friendly yarn soil release decorative fabric
CN103146054A (en) * 2013-02-21 2013-06-12 合肥杰事杰新材料股份有限公司 Modified jute fiber reinforced polypropylene and its preparation method
CN104594030A (en) * 2015-01-26 2015-05-06 江苏文凤化纤集团有限公司 Preparation method for spinning composite finishing agent

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘瑞云: ""亲水抗菌有机硅柔软剂整理剂的制备"", 《铜牛杯第九届功能性纺织品及纳米技术研讨会论文集》 *

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