CN105925454A - Imitation earthen jar ageing method of yellow rice wine - Google Patents

Imitation earthen jar ageing method of yellow rice wine Download PDF

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Publication number
CN105925454A
CN105925454A CN201610311011.0A CN201610311011A CN105925454A CN 105925454 A CN105925454 A CN 105925454A CN 201610311011 A CN201610311011 A CN 201610311011A CN 105925454 A CN105925454 A CN 105925454A
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China
Prior art keywords
oxygen
yellow wine
passed
aging
pithos
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Pending
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CN201610311011.0A
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Chinese (zh)
Inventor
李维新
何志刚
林晓姿
任香芸
林晓婕
梁璋成
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Institute of Agricultural Engineering Technology of Fujian Academy of Agricultural Sciences
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Institute of Agricultural Engineering Technology of Fujian Academy of Agricultural Sciences
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Application filed by Institute of Agricultural Engineering Technology of Fujian Academy of Agricultural Sciences filed Critical Institute of Agricultural Engineering Technology of Fujian Academy of Agricultural Sciences
Priority to CN201610311011.0A priority Critical patent/CN105925454A/en
Publication of CN105925454A publication Critical patent/CN105925454A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/22Ageing or ripening by storing, e.g. lagering of beer

Abstract

The invention provides an imitation earthen jar ageing method of yellow rice wine. According to the imitation earthen jar ageing method, yellow rice wine is stored in a stainless steel container, ceramic particles containing Ni<2+>, Cu<2+> and Fe<2+> are added into the container, and oxygen is introduced into the yellow rice for ageing. With the adoption of the ageing method provided by the invention, on one hand, the ester fragrance can be increased, the pungency and bitterness can be reduced, and the quality obtained by the ageing method is superior to that obtained by the traditional earthen jar ageing method; on the other hand, compared with the traditional ageing method, the ageing method provided by the invention has the advantages that the ageing period is short, the production efficiency is high, and the industrial production is facilitated.

Description

Yellow wine imitates pithos aging method
Technical field
The invention belongs to food processing field, be specifically related to a kind of yellow wine and imitate cylinder aging method.
Background technology
Yellow wine is one of the most ancient drinks, comes from China, and only in state-owned it, with medicated beer, wine claim the world three great Gu wine.Yellow wine contains the physiologically active ingredients such as polyphenol, melanoidin, glutathion, has removing free radical, prevents cardiovascular diseases, physiological function of waiting for a long time anticancer, anti-ageing.The fresh processed pungent excitement of yellow wine ethanol is strong, coarse mouthfeel, need to be the most drinkable after aging in 3 to 5 years.
Traditionally, yellow wine aging many employings pithos is preserved, and because the breathability of pithos can make yellow wine slowly aoxidize when there being oxygen, itself there is Ni in pithos simultaneously2+、Cu2+、Fe2+Plasma has catalytic action to esterification, aldol condensation, accelerates the aging ageing of yellow wine.But traditional yellow wine aging method, in traditional aging process, be pithos, be difficult to mechanized operation, the defects such as floor space is big, and cost is high, quality is unstable, be unfavorable for industrialized production.The process that yellow wine traditional aging process, actually yellow wine slowly aoxidize, namely yellow wine Ni in pithos2+、Cu2+、Fe2+Be esterified under isoionic catalysis, the process of aldol condensation because oxygen is at finite concentration in traditional aging process yellow wine to be maintained system, can not be the highest, can not be the lowest;But traditional yellow wine traditional aging process, the main breathability by pithos is to aging system oxygen supply, but this offering oxygen way is affected by many-sides such as pithos hole, air pressure, air humiditys, and then in yellow wine aging system, oxygen fluctuation is relatively big, and then affects the quality of yellow wine.The tradition aging cycle is 3 to 5 years, and the cycle is longer, causes production efficiency low.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of production efficiency height, the yellow wine aging method of stay in grade, beneficially industrialized production.
For solving above-mentioned technical problem, the technical solution used in the present invention is:
A kind of yellow wine imitates pithos aging method, it is characterised in that is preserved by yellow wine rustless steel container, adds containing Ni in container2+、Cu2+、Fe2+The ceramic granule of ion, is passed through oxygen aging in yellow wine.
The present invention can carry out aging according to the present invention to the not requirement of yellow wine kind, every fresh processed yellow wine (such as malt yeast yellow wine, Monas cuspurpureus Went yellow wine etc.).
Rustless steel container of the present invention storage yellow wine, because rustless steel has a voltage endurance, easy mechanized operation, floor space are little, low cost, beneficially industrialized production.
The ceramic granule of the present invention, is usually with containing Ni2+、Cu2+、Fe2+Isoionic potter's clay sintering forms;Industrially, this potter's clay is generally used for manufacturing pithos.In traditional aging process, this kind of metal ion has catalytic action to esterification, aldol condensation, can accelerate the aging ageing of yellow wine.In the present invention in " ceramic granule " " granule ", it is not limited to the fictile of " granule " shape, it is also possible to include other shapes of fictile.
Yellow wine traditional aging process is esterified, aldol reaction, be required for the participation of oxygen, the effect being passed through oxygen is to ensure that being smoothed out of yellow wine aging.
Using the aging method of the present invention, on the one hand can increase ester perfume, reduce pungent bitter taste, be better than the quality of pithos aging, on the other hand, use rustless steel container storage, mechanical strength is high, and floor space is little, it is simple to industrialized production.
Preferably, described yellow wine imitates pithos aging method, and with yellow wine stereometer, the amount adding ceramic granule is 0.5 to 1.0g/L.
Preferably, described yellow wine imitates pithos aging method, and ceramic particle diameter is 0.1 to 10.0mm, wraps up by 0.5 to 2.0kg/ bag, is evenly distributed in rustless steel container by the ceramic granule bandaged.
Preferably, described yellow wine imitates pithos aging method, before adding ceramic granule, by ceramic granule sterilizing 20 to 30min at 100 to 121 DEG C.
Preferably, described yellow wine imitates pithos aging method, is passed through oxygen aging, with yellow wine stereometer, maintains in the whole aging cycle in yellow wine the concentration of dissolved oxygen at 5 to 8mg/L.
Because yellow wine traditional aging process is esterified, aldol reaction, be required for the participation of oxygen;In whole traditional aging process yellow wine to be maintained system, oxygen is at finite concentration, the too high too low ageing quality that all can affect yellow wine of oxygen concentration.
Preferably, described yellow wine imitates pithos aging method, and the whole aging cycle is 8 to 12 months.
Because the present invention uses oxygen to be passed through system oxygen supply, being easily controlled oxygen concentration, relative to traditional handicraft, can shorten the aging cycle, production efficiency is high.The present invention uses oxygen to be passed through system oxygen supply so that aging system oxygen concentration is more stable, can guarantee that the stay in grade of aging yellow wine.
Preferably, described yellow wine imitates pithos aging method, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: be spaced 48 to 72h after being passed through oxygen every time, then be passed through the oxygen cycle next time;The purity being passed through oxygen is more than 99%, and with yellow wine stereometer, each oxygen ventilation amount is 0.1 to 0.3mL/L;The flow being every time passed through oxygen is 0.5 to 1.0L/min.
Use the aging method of the present invention, be easily controlled the concentration of oxygen so that yellow wine quality and mouthfeel relatively traditional handicraft improves a lot.
The present invention requiring, oxygen purity is more than 99%, because other gases not readily dissolved can be contained in the oxygen of low-purity, affects aging effect.
Preferably, described yellow wine imitates pithos aging method, and oxygen is passed through system and is made up of oxygen cylinder, air relief valve, effusion meter, pressure leather hose, air filter for removing bacteria, electrotimer, electromagnetic valve, gas conduit and dispersing head;The order of connection of this system is flowing through sequentially of oxygen, and oxygen flows through oxygen cylinder, air relief valve, effusion meter, pressure leather hose, air filter for removing bacteria, electrotimer, electromagnetic valve, gas conduit and dispersing head successively;There is a determining deviation bottom dispersing head placement location and rustless steel container, this is smaller than the 1/5 of rustless steel container height.
The present invention uses the effect of dispersing head to be to ensure that in aging system to be passed through oxygen and can slowly penetrate in yellow wine with micro-bubble shape;Dispersing head placement location and rustless steel container bottom space, less than the 1/5 of rustless steel container height, are so that the oxygen being passed through can be substantially dissolved in aging system.
Dispersing head material can be pottery, stainless, nanometer etc., dispersing head effect in the present invention is the oxygen that will flow out through gas conduit, oxygen disperses through dispersing head so that oxygen slowly penetrates in yellow wine with micro-bubble shape, accelerates the oxygen dissolving in yellow wine system.
Preferably, described yellow wine imitates pithos aging method, is passed through in oxygen process the flow being every time passed through oxygen with effusion meter and air relief valve control;Control be passed through oxygen gap periods and be passed through the oxygen time with electrotimer and electromagnetic valve.
Detailed description of the invention
By describing the technology contents of the present invention, structural feature in detail, being realized purpose and effect, it is explained in detail below in conjunction with detailed description of the invention.
Embodiment 1
The concrete technology method of the present embodiment is as follows:
Being preserved by yellow wine rustless steel container, with yellow wine stereometer, the amount adding ceramic granule is 0.5g/L, and ceramic particle diameter is 8.0 to 10.0mm, wraps up by 0.5kg/ bag, is evenly distributed in rustless steel container by the ceramic granule bandaged;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 8 months;It is spaced 72h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.1mL/L;The flow being every time passed through oxygen is 1.0L/min.
Embodiment 2
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 30min ceramic granule at 100 DEG C that is added on is 0.5g/L, and ceramic particle diameter is 8.0 to 10.0mm, wrap up by 0.5kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 8 months;It is spaced 72h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.1mL/L;The flow being every time passed through oxygen is 1.0L/min.
Embodiment 3
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 30min ceramic granule at 100 DEG C that is added on is 1.0g/L, and ceramic particle diameter is 0.1 to 2.0mm, wrap up by 2.0kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 12 months;It is spaced 48h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.3mL/L;The flow being every time passed through oxygen is 0.5L/min.
Embodiment 4
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 20min ceramic granule at 121 DEG C that is added on is 0.7g/L, and ceramic particle diameter is 6.0 to 8.0mm, wrap up by 1.0kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 10 months;It is spaced 60h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.2mL/L;The flow being every time passed through oxygen is 0.8L/min.
Embodiment 5
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 25min ceramic granule at 110 DEG C that is added on is 0.8g/L, and ceramic particle diameter is 4.0 to 6.0mm, wrap up by 1.5kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 11 months;It is spaced 66h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.15mL/L;The flow being every time passed through oxygen is 0.6L/min.
Embodiment 6
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 30min ceramic granule at 100 DEG C that is added on is 0.9g/L, and ceramic particle diameter is 2.0 to 4.0mm, wrap up by 1.5kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 9 months;It is spaced 54h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.25mL/L;The flow being every time passed through oxygen is 0.9L/min.
Embodiment 7
The concrete technology method of the present embodiment is as follows:
Yellow wine rustless steel container is preserved, with yellow wine stereometer, the amount of sterilizing 20min ceramic granule at 121 DEG C that is added on is 0.6g/L, and ceramic particle diameter is 3.0 to 6.0mm, wrap up by 1.0kg/ bag, the ceramic granule bandaged is evenly distributed in rustless steel container;It is passed through oxygen aging, maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine in the following way: the whole aging cycle is 10 months;It is spaced 60h after being passed through oxygen every time, then is passed through the oxygen cycle next time;With yellow wine stereometer, each oxygen ventilation amount is 0.2mL/L;The flow being every time passed through oxygen is 0.7L/min.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the present invention is limited; every equivalent structure utilizing description of the invention content to be made or equivalence flow process conversion; or directly or indirectly it is used in other relevant technical fields, the most in like manner it is included in the scope of patent protection of the present invention.

Claims (9)

1. a yellow wine imitates pithos aging method, it is characterised in that preserved by yellow wine rustless steel container, past Add containing Ni in container2+、Cu2+、Fe2+The ceramic granule of ion, is passed through oxygen aging in yellow wine.
2. yellow wine as claimed in claim 1 imitates pithos aging method, it is characterised in that with yellow wine stereometer, The amount adding ceramic granule is 0.5 to 1.0g/L.
3. yellow wine as claimed in claim 1 imitates pithos aging method, it is characterised in that described ceramic granule A diameter of 0.1 to 10.0mm, is wrapped up by 0.5 to 2.0kg/ bag, by uniform for the ceramic granule bandaged It is distributed in rustless steel container.
4. yellow wine as claimed in claim 1 imitates pithos aging method, it is characterised in that adding ceramic Before Li, by ceramic granule sterilizing 20 to 30min at 100 to 121 DEG C.
5. the yellow wine as described in Claims 1-4 is arbitrary imitates pithos aging method, it is characterised in that be passed through Oxygen aging, with yellow wine stereometer, maintains in the whole aging cycle in yellow wine the concentration of dissolved oxygen 5 to 8 mg/L。
6. yellow wine as claimed in claim 5 imitates pithos aging method, it is characterised in that the whole aging cycle It it is 8 to 12 months.
7. yellow wine as claimed in claim 6 imitates pithos aging method, it is characterised in that in the following way Maintain in the whole aging cycle concentration of dissolved oxygen in yellow wine: after being passed through oxygen, be spaced 48 to 72h every time, It is passed through the oxygen cycle the most next time;The purity being passed through oxygen is more than 99%, with yellow wine stereometer, every time Oxygen ventilation amount is 0.1 to 0.3mL/L;The flow being every time passed through oxygen is 0.5 to 1.0L/min.
8. the yellow wine as described in claim 1 to 7 is arbitrary imitates pithos aging method, it is characterised in that use Oxygen is passed through system and maintains in the whole aging cycle concentration of dissolved oxygen in yellow wine, and oxygen is passed through system by oxygen Gas cylinder, air relief valve, effusion meter, pressure leather hose, air filter for removing bacteria, electrotimer, electromagnetic valve, Gas conduit and dispersing head composition;The order of connection of this system is flowing through sequentially of oxygen, and oxygen flows successively Through oxygen cylinder, air relief valve, effusion meter, pressure leather hose, air filter for removing bacteria, electrotimer, electromagnetism Valve, gas conduit and dispersing head;A determining deviation is there is bottom dispersing head placement location and rustless steel container, This is smaller than the 1/5 of rustless steel container height.
9. yellow wine as claimed in claim 8 imitates pithos aging method, it is characterised in that with effusion meter and subtract Pressure valve controls to be passed through in oxygen process the flow being every time passed through oxygen;Control with electrotimer and electromagnetic valve It is passed through oxygen gap periods and is passed through the oxygen time.
CN201610311011.0A 2016-05-11 2016-05-11 Imitation earthen jar ageing method of yellow rice wine Pending CN105925454A (en)

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108504528A (en) * 2018-06-12 2018-09-07 枣阳市灵鹿酒业有限公司 A method of ageing improves yellow rice wine vinosity
CN108795679A (en) * 2018-06-12 2018-11-13 枣阳市灵鹿酒业有限公司 A kind of technique that X-ray urges old yellow rice wine
CN108795680A (en) * 2018-06-12 2018-11-13 枣阳市灵鹿酒业有限公司 A kind of technique that gamma-rays urges old yellow rice wine
CN108823053A (en) * 2018-06-12 2018-11-16 枣阳市灵鹿酒业有限公司 A kind of yellow wine aging method of acceleration
CN108841558A (en) * 2018-06-12 2018-11-20 枣阳市灵鹿酒业有限公司 A kind of method of accelerated ageing yellow rice wine
CN110923110A (en) * 2019-12-24 2020-03-27 山西紫林醋业股份有限公司 Mature vinegar aging device and aging method
CN111484916A (en) * 2020-05-29 2020-08-04 山西金科海生物制品有限公司 Aroma-producing filler, preparation method thereof and wine aging method
CN113583785A (en) * 2021-08-13 2021-11-02 唐山启森农业科技有限公司 Preparation method of high-quality mulberry wine
CN114032156A (en) * 2021-11-18 2022-02-11 中国长城葡萄酒有限公司 Aging method for distilled liquor

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108504528A (en) * 2018-06-12 2018-09-07 枣阳市灵鹿酒业有限公司 A method of ageing improves yellow rice wine vinosity
CN108795679A (en) * 2018-06-12 2018-11-13 枣阳市灵鹿酒业有限公司 A kind of technique that X-ray urges old yellow rice wine
CN108795680A (en) * 2018-06-12 2018-11-13 枣阳市灵鹿酒业有限公司 A kind of technique that gamma-rays urges old yellow rice wine
CN108823053A (en) * 2018-06-12 2018-11-16 枣阳市灵鹿酒业有限公司 A kind of yellow wine aging method of acceleration
CN108841558A (en) * 2018-06-12 2018-11-20 枣阳市灵鹿酒业有限公司 A kind of method of accelerated ageing yellow rice wine
CN110923110A (en) * 2019-12-24 2020-03-27 山西紫林醋业股份有限公司 Mature vinegar aging device and aging method
CN111484916A (en) * 2020-05-29 2020-08-04 山西金科海生物制品有限公司 Aroma-producing filler, preparation method thereof and wine aging method
CN113583785A (en) * 2021-08-13 2021-11-02 唐山启森农业科技有限公司 Preparation method of high-quality mulberry wine
CN114032156A (en) * 2021-11-18 2022-02-11 中国长城葡萄酒有限公司 Aging method for distilled liquor

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