CN105911229A - High-temperature and high-confining-pressure fluid-solid mutual effect testing device and testing method - Google Patents
High-temperature and high-confining-pressure fluid-solid mutual effect testing device and testing method Download PDFInfo
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- CN105911229A CN105911229A CN201610496411.3A CN201610496411A CN105911229A CN 105911229 A CN105911229 A CN 105911229A CN 201610496411 A CN201610496411 A CN 201610496411A CN 105911229 A CN105911229 A CN 105911229A
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- G—PHYSICS
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/65—Raman scattering
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- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D27/00—Simultaneous control of variables covered by two or more of main groups G05D1/00 - G05D25/00
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Abstract
The invention discloses a high-temperature and high-confining-pressure fluid-solid mutual effect testing device and a testing method. The high-temperature and high-confining-pressure fluid-solid mutual effect testing device comprises a pressure container, wherein two axial pressing rods, which are symmetrically sealed, are arranged in the pressure container in the horizontal direction; a test sample is arranged between the two pressing rods; a heating device for heating the test sample sleeves the outer side of the pressure container; a liquid pressing hole and an optical window are arranged on the surface of the pressure container; the heating device is arranged in a groove of a base; a temperature sensor is arranged on a contact surface between the heating device and the pressure container; theliquidpressing hole is communicated to a test sample placement part; and the optical window is aligned to the center of the test sample and is provided with an optical measurement system for observing a test sample light spectrum. According to the testing device and testing method, by carrying out chemical reaction and light spectrum measurementon the test sample under high-confining-pressure and high-temperature conditions, the micro morphology characteristics and spectrum collection of solid samples can be observed in situ under high-temperature high-pressure fluid condition, the interaction product of the solid and fluid can be measured in situ, measured data is closer to actual data, the measured data is more accurate and reliable and the accurate practice, and utilization and analysis of the test sample can be more easily guided.
Description
Technical field
The present invention relates to a kind of high temperature high confining pressure fluid-solid interaction assay device and test method, belong to high temperature
High-Voltage Experimentation device technique field.
Background technology
High temperature and pressure experiment is many scientific domains, such as planet and geoscience, condensed state physics, chemistry, material supply section
The important research means of etc. research fields, and have been achieved for many important research achievements.In geoscience, High Temperature High Pressure
Experiment provides substantial amounts of experimental data for the material composition within people's ball epistemically and state and Petrogenesis And Metallogenesis etc..
Such as, by studying the high temperature and pressure experiment of mantle rocks, people recognize that the seismic wave discontinuity surface of earth mantle about 650km is
Caused by the phase in version of olivine/pyroxene-perovskite structure.At physics and chemical field, supertension can make between atom
Distance Shortened and there is the interaction between electronic shell, and make electron structure change and formed and be totally different from often
The chemical bond of pressure material.Such as, have realized that so far the most any material all can occur nonmetal with
Transformation between metallic state.Wherein, the most not only there is the metallic state transformation to insulator in sodium and lithium, and in room temperature and
The phenomenon that fusing occurs under 1000000 atmospheric pressure the most still cannot understand and explain.In material science, High-Voltage Experimentation research makes
People recognize have superconducting property for the material of non-superconducting under high pressure low temperature under atmospheric low-temperature.Such as, except known 23 kinds
Element has outside superconducting property under atmospheric low-temperature, it was found that have 29 kinds of elements under high pressure to have superconducting property.Except pure material
Outward, the Hg-Ba-Ca cuprate obtained under elevated pressure conditions is that the material so far with the highest superconducting temperature is (under 30Pa pressure
Superconducting transition temperature reach 164K).This has guided a new approach for finding and synthesizing superconducting material.It addition, High Temperature High Pressure
Element can also be synthesized many there is the important or new material of advantageous property, as the superhard materials such as boron nitride, magnetic material,
Thermoelectric material, hydrogen storage material and solar energy materials etc..In recent years, high pressure (high temperature) was tested the most at Oil-gas origin and biology
Be applied in field.
Nature (such as earth interior, seabed and water body), engineering (as machinery, geology, ocean, thermoelectricity, nuclear power,
Boiler, building, digging, hydrometallurgy, chemical industry, material Hydrothermal Synthesis with modified etc.), scientific exploration is (such as ultrasonic probing and sea
Ocean detection) and scientific experiments in, be widely present the high temp/high pressure (hydrostatic pressing/differential stress) interaction between fluid and solid.
Mechanical-chemical coupling effect in interaction process then makes interaction process become complicated various.On the one hand, at high temperature
Under high pressure, fluid matasomatism can make the composition (including chemical composition and thing phase composition) of solid sample, structure (bag when solid sample
Include microcosmic, be situated between and see and macroscopic view) and character (include the physical propertys such as macroscopic property, mechanics, acoustics, electricity, calorifics, spectroscopy,
And Adsorption and desorption, dissolve, crystallize, the chemical property such as alteration and electrochemistry) significantly change；And on the other hand, it is in height
The composition (include chemical composition, compose and deposit kind and phase composition) of the solid sample convection cell the most again of temperature high pressure, microcosmic knot
Structure and character (include macroscopic property, various physical propertys, and hydrogen fugacity/activity, oxygen fugacity/activity, water fugacity/activity,
The chemical property such as Eh value and pH value) produce material impact.Therefore, the experimentation that high-temperature, high pressure fluid-solid interacts is i.e.
Become the research work that many science and technology field are particularly important.But, it is currently used for high-temperature, high pressure fluid-solid and interacts
The experimental facilities of experimentation generally exists that operating temperature pressure is relatively low, function limitation is single, integrated level is the highest and body weight is excessive
And lack the defects such as motility, seriously hinder each field progress in this aspect.
At present, according to pressure method, high temperature and pressure test device can be divided into Static pressure device and dynamic high-pressure device.Static pressure
Pressue device can realize high-temperature and high-pressure conditions or environment by following several approach: 1. autoclave device, it is possible to achieve temperature
Degree and limited pressure, generally below 800 DEG C and 200MPa；The biggest forcing press, mainly has multiaspect top formula forcing press and piston-cylinder
Two kinds of devices of formula forcing press, multiface upsetting machine can produce the isobaric hydrostatic pressing of three axles and three axial anisobaric pressure fields, can
Maximum temperature and pressure to realize respectively may be about 2000 DEG C and 10GPa, can carry out relatively large sample under high-temperature and high-pressure conditions
The experimentatioies such as the synthesis of material phase transformation, melted, mineral or material, piston cylinder formula forcing press can form the standard of 0～5GPa
Hydrostatic pressing, operating temperature is up to 1600 DEG C；3. Diamond primary ore, it is possible to achieve the high temperature more than 6000 DEG C and 500GPa
The experiment of pressure, almost can carry out the high temperature and pressure experiment research of earth interior all substances.The mainly impact of dynamic high-pressure device
Ripple and laser pressue device.Pressure can be carried out and reach the high temperature and pressure experiment research of 1000GPa.
The problem that above-mentioned high tension unit exists mainly has:
(1) under the conditions of the hydrostatic pressing of High Temperature High Pressure, it is difficult to accurately independent control temperature and pressure；(2) existing autoclave system
System volume bigger, it is difficult to dock with microscope and various spectrogrph, it is impossible to the surface appearance feature of in-situ observation solid sample with
Cannot be by means in site measurement product such as spectrum.
Summary of the invention
The technical problem to be solved in the present invention is: provide a kind of high temperature high confining pressure fluid-solid interaction assay device
And test method, it is achieved the surface microstructure feature of in-situ observation solid measure the surface of solids and solution under high temperature high confining pressure
In product, temperature reaches 700 DEG C, and confined pressure pressure reaches 200MPa, and test is more accurately reliable, the most domestic to solve
Above-mentioned variety of problems present in outer similar assay device.
The technical scheme that the present invention takes is: a kind of high temperature high confining pressure fluid-solid interaction assay device, including pressure
Force container, is provided with two axial depression bars of symmetrical sealing in described pressure vessel horizontal direction, place sample between described two depression bars,
Being socketed with the heater of heated solution and sample outside described pressure vessel, its surface configuration has hydraulic fluid mouth and optical window, institute
Stating heater to be placed in the groove of base, pressure vessel contact surface is provided with temperature sensor, described hydraulic fluid mouth is communicated to
Sample lay down location, described optical window is just to sample center, and is provided with observation sample micro-white light picture and the light of microspectrum
Learn measurement system.
Preferably, said temperature sensor, heater, optical measuring system are connected to controller, and controller is also connected with
There are hydrostatic sensor and hydraulic pump, and are wired to host computer.
Preferably, above-mentioned hydraulic fluid mouth is connected to hydraulic pump by pipeline, and described hydraulic pump is connected to reserving liquid tank by pipeline,
Hydraulic fluid mouth is connected on pipeline with hydraulic pump and is provided with cross valve and flow stop valve one, and the another two-port of cross valve connects liquid respectively
Pressure sensor and relief valve, the pipeline enclosure that hydraulic pump is connected with reserving liquid tank is provided with flow stop valve two.
Preferably, above-mentioned optical window includes just to communicating the first through hole, the second through hole, hyalomere and third through-hole, the
One through hole is arranged on pressure vessel, and the second through hole is arranged on the heating, and described third through-hole is arranged on base side wall,
Described hyalomere is arranged on the first through hole by briquetting, and it is arranged in briquetting groove, is provided with loophole in briquetting groove,
Its outer surface is close to the first through hole, is arranged in pressure vessel groove.
A kind of test method of high temperature high confining pressure fluid-solid interaction assay device, the method comprises the following steps:
(1) sample is loaded in pressure vessel, seal fixing sample by two symmetrical depression bars；
(2) calculate compactedness according to different temperatures, confined pressure condition and pressure vessel containment, led in pressure vessel by hydraulic fluid mouth
Enter a certain amount of fluid；
(3) sample and solution will be heated by heater by heated pressure container；
(4) at different temperatures, observe when sample interacts with the chemical solution of different pressures high by optical measuring system
Micro-white light picture under temperature high confining pressure and microphotogram.
Beneficial effects of the present invention: compared with prior art, effect of the present invention is as follows:
(1) present invention can independently and precise control of temperature and pressure, and the present invention is independent and accurately controls two kinds of ways of pressure, and one
Being the flexible change volume of depression bar, this method will not change the component of reaction system；Two is that hydraulic pump can pump fluid also
Fluid inside pressure vessel can be sucked out, this method can change the component of reaction system；
(2) present invention is provided with optical window, can be with the micro-image of in-situ observation specimen surface, thus can be high at high temperature
Under the conditions of confined pressure, microscope is utilized directly to observe the microstructure (surface produced such as corrosion) of specimen surface；
(3) present invention uses and carries out chemical reaction and spectral measurement under the conditions of high temperature and high confining pressure for sample, it is possible at height
Product in site measurement solid sample surface and fluid under the fluid condition of temperature high confining pressure, measurement data is more nearly reality
Border, data measured is more accurately reliable, is more beneficial for instructing the correct practice of sample to use and analyzes；
(4) present invention is provided with optical window, and the microspectrum of energy in-situ observation sample, and as various in measurement have Raman active
The Raman spectrum of material, Raman spectrum can accurately measure the lattice vibration energy of material.When material is by different temperatures and confined pressure
During effect, its lattice structure will produce change, and lattice vibration energy also will change, and Raman frequency shift also will change,
Can accurately calculate the stress of crystals according to the relation between stress with relative Raman frequency shift, micro Raman spectra method is used for
Mechanical meaurement, has noncontact, lossless, spatial resolution is high and can be with features such as deep focus, can be in different temperatures and pressure
Under the conditions of power, the ess-strain measuring solid sample of system and Raman spectrum, and set up the theoretical pass of Raman frequency shift and stress
It is model, provides basic data support for research work and engineering；
(5) present configuration is simple, and has that volume is little, lightweight, the feature of low cost.
Accompanying drawing explanation
Fig. 1 is the layout drawing of the structural representation of the present invention；
Fig. 2 is the forward sight structural representation of Fig. 1；
Fig. 3 is the close-up schematic view A in Fig. 1；
Fig. 4 is the hydraulic system structure schematic diagram of the present invention.
Detailed description of the invention
Below in conjunction with the accompanying drawings and the present invention is described further by specific embodiment.
Embodiment 1: as Figure 1-Figure 4, a kind of high temperature high confining pressure fluid-solid interaction assay device, including pressure
Force container 2, is provided with two axial left side depression bar 3 and right side depression bars 4 of symmetrical sealing in pressure vessel 2 horizontal direction, left side is pressed
Place sample 5 between bar 3 and right side depression bar 4, outside pressure vessel 2, be socketed with the heater 6 of heated solution and sample 5, its surface
Being provided with hydraulic fluid mouth 9 and optical window 10, described heater 6 is placed in the groove 26 of base 1, with pressure vessel 2 contact surface
Being provided with temperature sensor 29, hydraulic fluid mouth 9 is communicated to sample 5 lay down location, and optical window 10 is just to sample 5 center, and is provided with
Observe the optical measuring system 30 of the micro-white light picture of sample 5 and microspectrum (Raman, infrared etc.).
Raman spectrum can accurately measure the lattice vibration energy of material.When material is stressed effect, its lattice structure
Will produce change, lattice vibration energy also will change, and Raman frequency shift also will change.According to stress and relative Raman
Relation between frequency displacement can accurately calculate the stress of crystals.Under the conditions of different temperatures difference confined pressure and axial stress,
Systematically measure ess-strain and the Raman spectrum of solid sample, the theoretic relationmodel of Raman frequency shift and stress can be set up.
Preferably, depression bar 3 outer end, above-mentioned left side connects charger 7, and charger 7 is fixedly attached on base 1.
Preferably, above-mentioned charger 7 includes that afterburning screw 18 and adaptor 19, afterburning screw 18 can connect by spiral movably
Being connected on base 1 sidewall, its thread head center connects has adaptor 19, adaptor 19 end to be provided with universal ball end 20, and ten thousand
Transferring force to left side depression bar 3 to bulb 20, the adjustment screw 25 on right side is connected on base 1, depression bar 4 one end on the right side of its connection
It is provided with bulb 43, combines above-mentioned afterburning screw 18 by adjusting screw 25, it is achieved the movement of left and right sides depression bar, thus ensure
Sample can occupy center position just to optical window, it is simple to the data that optic testing system gathers more accurately and more may be used
Lean on, and by adjusting turning of screw and afterburning screw, easy to adjust fast.
Preferably, said temperature sensor 29, heater 6, optical measuring system 30 are connected to controller, and controller is also
Connect and have hydrostatic sensor and hydraulic pump, and be wired to host computer.
Preferably, above-mentioned hydraulic fluid mouth 9 is connected to hydraulic pump 37 by pipeline, and hydraulic pump 37 is connected to reserving liquid tank by pipeline
36, hydraulic fluid mouth 9 is connected on pipeline with hydraulic pump 37 and is provided with cross valve 38 and flow stop valve 1, the another two ends of cross valve 38
Mouth connects hydrostatic sensor 39 and relief valve 40 respectively, and the pipeline enclosure that hydraulic pump 37 is connected with reserving liquid tank 36 is provided with flow cutoff
Valve 2 42.
Preferably, above-mentioned optical window 10 includes just to communicating first through hole the 14, second through hole 15, hyalomere 13 and the 3rd
Through hole 16, the first through hole 14 is arranged on pressure vessel 2, and the second through hole 15 is arranged on heater 6, described third through-hole 16
Being arranged on base 1 sidewall, hyalomere 13 is arranged at the first through hole 14 by briquetting 12, and it is arranged in briquetting 12 groove,
Being provided with loophole in briquetting 12 groove, its outer surface is close at the first through hole 14, is fixedly connected in pressure by screw 17
In force container 2 groove.
Embodiment 2: the test method of a kind of high temperature high confining pressure fluid-solid interaction assay device, the method includes
Following steps:
(1) sample is loaded in pressure vessel, seal fixing sample by two symmetrical depression bars；
(2) calculate compactedness according to different temperatures, confined pressure condition and pressure vessel containment, led in pressure vessel by hydraulic fluid mouth
Enter a certain amount of fluid；
(3) sample and solution will be heated by heater by heated pressure container；
(4) high temperature when being observed the chemical solution interaction of sample and different pressures at different temperatures by optical measuring system
Micro-white light picture under high confining pressure and microphotogram.
The above, the only detailed description of the invention of the present invention, but protection scope of the present invention is not limited thereto, and any
Those familiar with the art, in the technical scope that the invention discloses, can readily occur in change or replace, should contain
Covering within protection scope of the present invention, therefore, protection scope of the present invention should be as the criterion with described scope of the claims.
Claims (5)
1. a high temperature high confining pressure fluid-solid interaction assay device, it is characterised in that: include pressure vessel (2), described
It is provided with two axial depression bars (3,4) of symmetrical sealing in pressure vessel (2) horizontal direction, between described two depression bars (3,4), places examination
Sample (5), is socketed with the heater (6) of heated solution and sample (5) outside described pressure vessel (2), its surface configuration has hydraulic fluid
Mouth (9) and optical window (10), described heater (6) is placed in the groove (26) of base (1), contacts with pressure vessel (2)
Face is provided with temperature sensor (29), and described hydraulic fluid mouth (9) is communicated to sample (5) lay down location, and described optical window (10) is the most right
Sample (5) center, and the optical measuring system (30) observing sample (5) spectrum is installed.
A kind of high temperature high confining pressure fluid-solid interaction assay device the most according to claim 1, it is characterised in that:
Described temperature sensor (29), heater (6), optical measuring system (30) are connected to controller, and controller is also associated with liquid
Pressure sensor and hydraulic pump, and it is wired to host computer.
A kind of high temperature high confining pressure fluid-solid interaction assay device the most according to claim 1, it is characterised in that:
Hydraulic fluid mouth (9) is connected to hydraulic pump (37) by pipeline, and described hydraulic pump (37) is connected to reserving liquid tank (36), hydraulic fluid by pipeline
Mouthful (9) are connected on pipeline with hydraulic pump (37) and are provided with cross valve (38) and flow stop valve one (41), and cross valve (38) is separately
Two-port connects hydrostatic sensor (39) and relief valve (40) respectively, the pipeline enclosure peace that hydraulic pump (37) is connected with reserving liquid tank (36)
Equipped with flow stop valve two (42).
A kind of high temperature high confining pressure fluid-solid interaction assay device the most according to claim 1, it is characterised in that:
Optical window (10) includes just to communicating the first through hole (14), the second through hole (15), hyalomere (13) and third through-hole (16), institute
Stating the first through hole (14) to be arranged on pressure vessel (2), described second through hole (15) is arranged on heater (6), and described
Three through holes (16) are arranged on base (1) sidewall, and described hyalomere (13) is arranged on the first through hole (14) place by briquetting (12),
It is arranged in briquetting (12) groove, is provided with loophole in briquetting (12) groove, and its outer surface is close to the first through hole (14)
Place, is arranged in pressure vessel (2) groove.
5. according to the test of the arbitrary described a kind of high temperature high confining pressure fluid-solid interaction assay device of claim 1-4
Method, it is characterised in that: the method comprises the following steps:
(1) sample is loaded in pressure vessel, seal fixing sample by two symmetrical depression bars；
(2) calculate compactedness according to different temperatures, confined pressure condition and pressure vessel containment, led in pressure vessel by hydraulic fluid mouth
Enter a certain amount of fluid；
(3) sample and solution will be heated by heater by heated pressure container；
(4) at different temperatures, observe when sample interacts with the chemical solution of different pressures high by optical measuring system
Micro-white light picture under temperature high confining pressure and microphotogram.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106908170A (en) * | 2017-03-14 | 2017-06-30 | 吉首大学 | A kind of Raman frequency shift temp measuring method and system |
| CN107796959A (en) * | 2017-10-13 | 2018-03-13 | 中国科学院地球化学研究所 | Different oxygen fugacity in-situ control methods in a kind of diamond anvil cell electrical measurement |
| CN109682937A (en) * | 2019-03-04 | 2019-04-26 | 中国科学院地球化学研究所 | A kind of large cavity high temperature and pressure gas liquid two-phase flow experimental provision and experimental method |
| CN109731531A (en) * | 2019-03-04 | 2019-05-10 | 中国科学院地球化学研究所 | A kind of hydro-thermal large cavity high temperature and high voltage experimental device and experimental method |
| CN109738594A (en) * | 2019-03-04 | 2019-05-10 | 中国科学院地球化学研究所 | A kind of hydro-thermal large cavity high temperature and pressure flowing experimental provision and experimental method |
| CN112403393A (en) * | 2020-12-17 | 2021-02-26 | 吉林大学 | High-temperature and high-pressure resistant in-situ optical observation reaction kettle shell |
| CN112403392A (en) * | 2020-12-17 | 2021-02-26 | 吉林大学 | High-temperature high-pressure reaction kettle for in-situ optical measurement of large-capacity liquid environment |
| CN113848171A (en) * | 2021-05-26 | 2021-12-28 | 国家电投集团科学技术研究院有限公司 | In-situ optical measuring device for simulating pressurized water reactor loop water environment |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6401523B1 (en) * | 1998-11-09 | 2002-06-11 | Institut Francais Du Petrole | Device for testing rock samples at relatively high pressure and temperature |
| CN101718725A (en) * | 2009-12-08 | 2010-06-02 | 中国科学院广州能源研究所 | Device for measuring sample thermo-physical property in situ |
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
| CN104596907A (en) * | 2015-01-28 | 2015-05-06 | 太原理工大学 | Measurement method for large-displacement shear-flow of rock under high temperature and high pressure |
| CN105181930A (en) * | 2015-09-07 | 2015-12-23 | 中国地质大学（北京） | Method and device for measuring chemical reaction and physical change of oil rock and water rock |
| CN205786560U (en) * | 2016-06-30 | 2016-12-07 | 中国科学院地球化学研究所 | A kind of high temperature high confining pressure fluid-solid interaction assay device |
-
2016
- 2016-06-30 CN CN201610496411.3A patent/CN105911229B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6401523B1 (en) * | 1998-11-09 | 2002-06-11 | Institut Francais Du Petrole | Device for testing rock samples at relatively high pressure and temperature |
| CN101718725A (en) * | 2009-12-08 | 2010-06-02 | 中国科学院广州能源研究所 | Device for measuring sample thermo-physical property in situ |
| CN103406070A (en) * | 2013-08-26 | 2013-11-27 | 中国科学院地球化学研究所 | Multifunctional high-temperature and high-pressure reaction kettle |
| CN104596907A (en) * | 2015-01-28 | 2015-05-06 | 太原理工大学 | Measurement method for large-displacement shear-flow of rock under high temperature and high pressure |
| CN105181930A (en) * | 2015-09-07 | 2015-12-23 | 中国地质大学（北京） | Method and device for measuring chemical reaction and physical change of oil rock and water rock |
| CN205786560U (en) * | 2016-06-30 | 2016-12-07 | 中国科学院地球化学研究所 | A kind of high temperature high confining pressure fluid-solid interaction assay device |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106908170A (en) * | 2017-03-14 | 2017-06-30 | 吉首大学 | A kind of Raman frequency shift temp measuring method and system |
| CN107796959A (en) * | 2017-10-13 | 2018-03-13 | 中国科学院地球化学研究所 | Different oxygen fugacity in-situ control methods in a kind of diamond anvil cell electrical measurement |
| CN109682937A (en) * | 2019-03-04 | 2019-04-26 | 中国科学院地球化学研究所 | A kind of large cavity high temperature and pressure gas liquid two-phase flow experimental provision and experimental method |
| CN109731531A (en) * | 2019-03-04 | 2019-05-10 | 中国科学院地球化学研究所 | A kind of hydro-thermal large cavity high temperature and high voltage experimental device and experimental method |
| CN109738594A (en) * | 2019-03-04 | 2019-05-10 | 中国科学院地球化学研究所 | A kind of hydro-thermal large cavity high temperature and pressure flowing experimental provision and experimental method |
| CN109738594B (en) * | 2019-03-04 | 2023-09-01 | 中国科学院地球化学研究所 | Hydrothermal large-cavity high-temperature high-pressure flow experimental device and experimental method |
| CN109731531B (en) * | 2019-03-04 | 2024-01-23 | 中国科学院地球化学研究所 | Hydrothermal large-cavity high-temperature high-pressure experimental device and experimental method |
| CN109682937B (en) * | 2019-03-04 | 2024-02-06 | 中国科学院地球化学研究所 | Large-cavity high-temperature high-pressure gas-liquid two-phase flow experimental device and experimental method |
| CN112403393A (en) * | 2020-12-17 | 2021-02-26 | 吉林大学 | High-temperature and high-pressure resistant in-situ optical observation reaction kettle shell |
| CN112403392A (en) * | 2020-12-17 | 2021-02-26 | 吉林大学 | High-temperature high-pressure reaction kettle for in-situ optical measurement of large-capacity liquid environment |
| CN112403392B (en) * | 2020-12-17 | 2021-10-08 | 吉林大学 | High-temperature high-pressure reaction kettle for in-situ optical measurement of large-capacity liquid environment |
| CN113848171A (en) * | 2021-05-26 | 2021-12-28 | 国家电投集团科学技术研究院有限公司 | In-situ optical measuring device for simulating pressurized water reactor loop water environment |
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