CN105907567A - Preparation method of red pitaya icewine - Google Patents

Preparation method of red pitaya icewine Download PDF

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Publication number
CN105907567A
CN105907567A CN201610506698.3A CN201610506698A CN105907567A CN 105907567 A CN105907567 A CN 105907567A CN 201610506698 A CN201610506698 A CN 201610506698A CN 105907567 A CN105907567 A CN 105907567A
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red heart
wine
preparation
huolong
ice wine
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CN105907567B (en
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龚霄
方蕾
王晓芳
刘洋洋
林丽静
李积华
殷俊伟
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Agricultural Products Processing Research Institute of CATAS
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation

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  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
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  • Life Sciences & Earth Sciences (AREA)
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  • Alcoholic Beverages (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

The invention relates to the field of fruit wind preparation, and in particular relates to a preparation method of red pitaya icewine. The method comprises the following steps: (1) freezing and squeezing red pitaya to prepare red pitaya juice; (2) adding a clarifying agent to the red pitaya juice, carrying out freezing preservation for 2-4 days, filtering the juice and adding potassium metabisulfite; (3) adjusting the sugar content and the acidity of the red pitaya juice, adding saccharomyces cerevisiae and pectinase for carrying out temperature-controlled fermentation, cooling and freezing the product and adding the potassium metabisulfite for terminating fermentation; (4) filtering and separating wine lees to obtain raw wine; and (5) carrying out low-temperature ageing, and filtering, sterilizing and filling the raw wine. The prepared red pitaya icewine has a unique sweet fragrance of the pitaya, mellow in bouquet and smooth and refreshing in mouthfeel; the wine body is full and coordinated; and the red pitaya icewine is long in aftertaste, and has a good health function.

Description

A kind of preparation method of red heart HUOLONG fruit ice wine
Technical field
The present invention relates to fruit wine preparation field, in particular to the system of a kind of red heart HUOLONG fruit ice wine Preparation Method.
Background technology
Hylocereus undatus, also known as Hylocereus undatus, Herba Passiflorae Foetidae, is that Cactaceae triangular prism belongs to (Hylocereus) or Serpentis Whip post belongs to (Selenicereus) fruit, presents ellipse, diameter 10cm~12cm, and outward appearance is Redness or yellow, have the thallus of green rounded triangle, white, red or yellow sarcocarp, have Melanospermous fruit.Red heart Hylocereus undatus is because of disease-resistant, high yield, rich in nutrition, enjoys plantation in recent years The favor of person.
Hylocereus undatus Fruit anatomy speed is than very fast, and the Hylocereus undatus fruit of after-ripening can not be preserved, time fresh-keeping Between short, easily rot, the sale so the Hylocereus undatus of maturation should not be transfered to other localities, ripe Hylocereus undatus city Field the most just receives limitation.Along with the development in epoch, various fruit wine progress into the life of people, close More and more deep in the nutrient research of fruit wine.If Hylocereus undatus can be carried out deep processing to make red pitaya wine, Hylocereus undatus can not only be solved and be difficult to storage and the problem of transport, moreover it is possible to preferably promote answering of Hylocereus undatus By scope and sales value.
In view of this, the special proposition present invention.
Summary of the invention
It is an object of the invention to provide the preparation method of a kind of red heart HUOLONG fruit ice wine, described method with Red heart Hylocereus undatus is raw material, by limiting the reaction condition of each step, improves and with red heart Hylocereus undatus is The mouthfeel of the red heart HUOLONG fruit ice wine that raw material brews and quality.
In order to realize the above-mentioned purpose of the present invention, spy by the following technical solutions:
The preparation method of a kind of red heart HUOLONG fruit ice wine, comprises the following steps:
1), by the freezing of red heart Hylocereus undatus, squeezing, red heart dragon fruit juice is prepared;
2), in described red heart dragon fruit juice, clarifier, freezing 3~filter also after 4 days are added Add potassium metabisulfite;
3), adjust the sugar content of red heart dragon fruit juice and acidity, add saccharomyces cerevisiae and pectase enters Row temperature controlled fermentation, after having fermented, cooling is freezing and adds potassium metabisulfite termination fermentation;
4), filter separation wine mud, obtain wine base;
5), by fill after described wine base low temperature aging, filtration, sterilizing.
Ice wine has long history, it brewage be before 200 years after Europe is found unintentionally Start to spread so far.The frostbite that the vineyard of Germany is overtaken at that time, in order to save loss, Winemaker presses traditional method ferment wine brewing after the Fructus Vitis viniferae squeezing of frost, surprisingly it has been found that result is acid Sweet proportional balancing method, sweet good wine as Mel, and by named ice wine.
Hylocereus undatus is the torrid zone, subtropical fruit, when preparing ice wine, if being also adopted by tree body the coldest Freeze until plucking the most unrealistic.The present invention all uses cryogenic system in main technique, preparation Ice wine total phenols and tannin content are low, give off a strong fragrance, and taste is coordinated.
It is known that Hylocereus undatus have red in vain point.Red heart Hylocereus undatus selected by the present invention is ripe new Fresh red heart Hylocereus undatus, hardness is high, scale is green, and epidermis is without piebaldism or white macula.General red heart fire Dragon fruit is higher than white heart Hylocereus undatus sugariness, and its sugar reaches more than 15 degree, and taste is the most agreeably sweet.Except Icing Sugar Outward, red heart Hylocereus undatus is in addition to even better in mouthfeel, and its nutritive value is also far above white heart-fire Long Guo.Red heart Hylocereus undatus color is deep, and carotene carotene content is higher.Carotene is to free radical resisting One of effective antioxidant, is favorably improved immunity, the fiber part of protection eyes crystal.
The ice wine brewageed with red heart Hylocereus undatus, the smell of fruits is very sweet, beautiful in colour, nutritious, and has The good health cares such as toxin expelling nourishing the stomach, antioxidation, blood sugar lowering, blood fat reducing, radioprotective.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, step 1) specifically include:
Fresh mature red heart Hylocereus undatus harvesting obtained carries out gradient with 1 DEG C~3 DEG C of speed hourly Cooling, is incubated 12~16h, squeezes extracting juice, prepare red heart dragon fruit juice after being down to-8 DEG C~-4 DEG C.
The present invention uses the mode of gradient cooling Hylocereus undatus to be carried out frost process, in whole production technology To Hylocereus undatus safekeeping in case violent variations in temperature.This frost mode condition milder, ice crystal Produce lacks, and can increase subsequent step further and squeeze out the sugariness of fruit juice, it is often more important that the fruit squeezed out In juice, tannin and total phenol content are lower, and then make red heart HUOLONG fruit ice wine color, fragrance and taste more Good.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 2) in, described Clarifier is PVPP or bentonite, and addition is 800~1200mg/L.
PVPP (Polyvinylpyrrolidone) i.e. crospovidone.PVPP itself will not cause Cancer, has good food safety, can form complex with specific polyphenolic substance (such as tannin), Mainly as food clarifier and stabilizers such as medicated beer, fruit juice, wines in terms of food processing.
Bentonite is a kind of colloidal clay, can adsorb itself weight 8~the moisture of 10 times, forms pasty state Mucilage.Owing to it has powerful absorbability, water can be fixed and substantially increase its volume, in electrolysis Adsorbable protein and pigment in matter solution and produce the cohesion of colloid.Clarifier is made with bentonite There is advantage inexpensive, that muddiness will not be produced because adding excess.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 2) in, described The temperature of freezing is-9 DEG C~-4 DEG C.
The application freezing 2~fruit juice can be clarified during 4 days.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 2) and step 3) In, the addition of described potassium metabisulfite is 70~110g/t.
Potassium metabisulfite can produce sulfur dioxide, and the application is in red heart dragon fruit juice per ton or fermentation After product in add 70~110g potassium metabisulfites, beneficially pigment, winestone, inorganic salt etc. become The dissolving divided, can increase the content of extractum and the colourity of wine, also have the work of sterilization and anticorrosion and clarification With, prevent wine liquid aging while the natural fruit characteristic of wine liquid more as antioxidant, can be protected.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 3) in, adjust The sugar content of red heart dragon fruit juice with the concrete mode of acidity is:
The sugar content adding white sugar adjustment red heart dragon fruit juice is 285~300g/L;Add tartaric acid to adjust Whole acid content is 8~9g/L.
The computational methods of sugaring amount are: sugaring amount (g)=(sugar content-reality of fruit juice target is sugary Amount) × fruit juice volume;
Acid adding amount (g)=(acid content of fruit juice target-actual sugar content) × fruit juice volume.
Generally before sugaring, total sugar is about 50g/L, and total acid is about 1.5g/L (in terms of tartaric acid).
Wherein, adjust sugariness and be mainly used for improving the mouthfeel of products obtained therefrom, and adjust acidity on the one hand It is to consider from mouthfeel, on the other hand, is the pH value in order to regulate fermentation system.
In the present invention, the pH value of red heart HUOLONG fruit ice wine depends primarily on tartaric content, but also By other materials, such as malic acid and the impact of citric acid;Adding tartaric acid regulation total acid is 8~9g/L can The breeding of suppression microorganism.Owing to pH value can affect natural pigment, so it is to red heart HUOLONG fruit ice wine Color also have a great impact, add tartaric acid the ice wine color prepared can be made scarlet limpid.With Time suitable pH value also be beneficial to low temperature aging time red heart HUOLONG fruit ice wine low-temperature stability, beneficially winestone The precipitation of potassium hydrogen phthalate.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 3) in, described The addition of saccharomyces cerevisiae is 230~270g/L, and the addition of pectase is 30~35mg/L.
Pectase uses as clarifier.
The inoculum concentration of yeast is particularly important to fermentation system.In the present invention, in conjunction with the bar that specifically ferments Part, along with the increase fermenting speed of yeast-inoculated amount can be gradually increased, liquor output is consequently increased, wine Taste and color and luster the best, subjective appreciation score also can uprise;If but inoculum concentration is excessive, then owing to sending out Nutrient substance in ferment system consumes too much consuming on the growth and breeding of somatic cells so that be used for The amount of substrate changing into wine reduces, and consuming rapidly and the product of more metabolite along with nutrient substance Raw, somatic cells ecological deterioration, cross presenility and be concurrently conigenous molten, cause yielding poorly of wine, impact sense Official's quality.Thus, the yeast-inoculated amount of the application be comprehensive mouthfeel, color and luster, fermentation duration etc. in many ways Scope the most out after the factor of face.
It is further preferred that in step 3) in, the condition of described temperature controlled fermentation is
18 DEG C~20 DEG C ferment 30~40 days.
During ice liquor brewing, it is a crucial process procedure that temperature control slowly ferments.Fermentation temperature Degree affects fermentation time and ice wine quality.
Preferably, the preparation method of red heart HUOLONG fruit ice wine as above, in step 5) in,
Described aging is specially 0 DEG C~the storage aging 6 of 5 DEG C of tanks~12 months.
Yeast autolysis phenomenon can occur during aging, directly affect the organoleptic attribute of ice wine so that it is The most harmonious mellow and full;Traditional aging process also can improve the clarity of ice wine in addition further.
Red heart HUOLONG fruit ice wine prepared by preparation method as above.
Red heart HUOLONG fruit ice wine prepared by the application, the physical and chemical index recording product by GB is: ethanol Degree 11% ± 1% (V/V), total sugar content >=125.0g/L (with glucose meter), total acid content is 8.0~9.2g/L (in terms of tartaric acid), total SO2Content≤200mg/L, sugar-free extract >=15g/L, volatile acid≤1.5g/l.
Compared with prior art, the invention have the benefit that
1), the present invention with red heart Hylocereus undatus as raw material, the red heart HUOLONG fruit ice wine of preparation has Hylocereus undatus Distinctive fresh and sweet fragrance, aroma is mellow, and mouthfeel is smooth, tasty and refreshing, the plentiful coordination of wine body, long times of aftertaste. It is rich in the several amino acids of needed by human body, organic acid, vitamin, mineral and useful to human body The nutritional labelings such as betanin, phenols, cellulose, have good health care, belong to high-grade variety Red heart HUOLONG fruit ice wine.
2), by the operation of two step clarifications, improve the red heart brewed with red heart Hylocereus undatus for raw material The mouthfeel of HUOLONG fruit ice wine and organoleptic quality, the red heart HUOLONG fruit ice wine of preparation is bright aubergine, Wine body is beautiful, and mouthfeel is sweet and returns acid, and quality is superior.
3), use the mode of unique gradient cooling that Hylocereus undatus carries out frost process, whole production work To Hylocereus undatus safekeeping in case violent variations in temperature in skill.This frost mode condition milder, What ice crystal produced lacks, and can increase subsequent step further and squeeze out the sugariness of fruit juice, it is often more important that squeeze out Fruit juice in tannin and total phenol content lower, and then make red heart HUOLONG fruit ice wine color, fragrance and mouth Taste is more preferably.
Accompanying drawing explanation
In order to be illustrated more clearly that the specific embodiment of the invention or technical scheme of the prior art, under The accompanying drawing used required in detailed description of the invention or description of the prior art will be briefly described by face, It should be evident that the accompanying drawing in describing below is some embodiments of the present invention, general for this area From the point of view of logical technical staff, on the premise of not paying creative work, it is also possible to obtain according to these accompanying drawings Obtain other accompanying drawing.
Fig. 1 is that different cooling processing modes is on tannin and the impact of total phenol content;
Fig. 2 is the impact on red heart HUOLONG fruit ice wine quality of the yeast-inoculated amount.
Detailed description of the invention
Below in conjunction with embodiment, embodiment of the present invention are described in detail, but this area skill Art personnel are it will be appreciated that the following example is merely to illustrate the present invention, and are not construed as limiting the present invention Scope.Unreceipted actual conditions person in embodiment, the condition advised according to normal condition or manufacturer Carry out.Agents useful for same or instrument unreceipted production firm person, being can be by commercially available purchase acquisition Conventional products.
Embodiment 1
The preparation method of a kind of red heart HUOLONG fruit ice wine, comprises the following steps:
1), selecting ripe fresh red heart Hylocereus undatus, hardness is high, scale is green, and epidermis is without piebaldism Or white macula, raw material is manually removed the peel, cutting;
2), carrying out gradient cooling with 1 DEG C of speed hourly, be incubated 12h after being down to-8 DEG C, squeezing takes Juice, prepares red heart dragon fruit juice.
3), adding PVPP in described red heart dragon fruit juice, addition is 800mg/L;-9℃ ~-4 DEG C of freezings filter after 2 days and add potassium metabisulfite 70g/t;
4) sugar content, adding white sugar adjustment red heart dragon fruit juice is 285g/L;Add tartaric acid to adjust Whole acid content is 8g/L;
Adding saccharomyces cerevisiae and pectase, 18 DEG C~20 DEG C ferment 30 days, the addition of described saccharomyces cerevisiae Amount is 270g/L, and the addition of pectase is 30mg/L;After having fermented, cooling is freezing and addition is laid particular stress on Potassium sulfite 70g/t, terminates fermentation;
4), filter separation wine mud, obtain wine base;
5), by fill after described wine base 0 DEG C~5 DEG C tanks storage aging 6 months, filtration, sterilizings, bottle stores up List marketing in more than 3 months.
Embodiment 2
The preparation method of a kind of red heart HUOLONG fruit ice wine, comprises the following steps:
1), selecting ripe fresh red heart Hylocereus undatus, hardness is high, scale is green, and epidermis is without piebaldism Or white macula, raw material is manually removed the peel, cutting;
2), carrying out gradient cooling with 3 DEG C of speed hourly, be incubated 16h after being down to 4 DEG C, squeezing takes Juice, prepares red heart dragon fruit juice.
3), adding bentonite in described red heart dragon fruit juice, addition is 1200mg/L;-9℃ ~-4 DEG C of freezings filter after 4 days and add potassium metabisulfite 110g/t;
4) sugar content, adding white sugar adjustment red heart dragon fruit juice is 300g/L;Add tartaric acid to adjust Whole acid content is 9g/L;
Adding saccharomyces cerevisiae and pectase, 18 DEG C~20 DEG C ferment 40 days, the addition of described saccharomyces cerevisiae Amount is 230g/L, and the addition of pectase is 35mg/L;After having fermented, cooling is freezing and addition is laid particular stress on Potassium sulfite 110g/t, terminates fermentation;
4), filter separation wine mud, obtain wine base;
5), by fill after described wine base 0 DEG C~5 DEG C tanks storage aging 12 months, filtration, sterilizings, bottle stores up List marketing in more than 3 months.
Embodiment 3
The preparation method of a kind of red heart HUOLONG fruit ice wine, comprises the following steps:
1), selecting ripe fresh red heart Hylocereus undatus, hardness is high, scale is green, and epidermis is without piebaldism Or white macula, raw material is manually removed the peel, cutting;
2), carrying out gradient cooling with 2 DEG C of speed hourly, be incubated 14h after being down to-6 DEG C, squeezing takes Juice, prepares red heart dragon fruit juice.
3), adding bentonite in described red heart dragon fruit juice, addition is 1000mg/L;-9℃ ~-4 DEG C of freezings filter after 3 days and add potassium metabisulfite 85g/t;
4) sugar content, adding white sugar adjustment red heart dragon fruit juice is 290g/L;Add tartaric acid to adjust Whole acid content is 8g/L;
Adding saccharomyces cerevisiae and pectase, 18 DEG C~20 DEG C ferment 35 days, the addition of described saccharomyces cerevisiae Amount is 250g/L, and the addition of pectase is 32mg/L;After having fermented, cooling is freezing and addition is laid particular stress on Potassium sulfite 90g/t, terminates fermentation;
4), filter separation wine mud, obtain wine base;
5), by fill after described wine base 0 DEG C~5 DEG C tanks storage aging 9 months, filtration, sterilizings, bottle stores up List marketing in more than 3 months.
Experimental example 1
With experimental example 3 to basic engineering comparative example 1.In comparative example 1, by the temperature-fall period of Hylocereus undatus Change into: directly the Hylocereus undatus after peeling, cutting is put into the refrigerator-freezer storage of-6 DEG C, storage time and enforcement Example 3 is identical, and in addition remaining production technology is the most same as in Example 3.
Prepared red heart dragon fruit juice is squeezed and the finished product ice finally given after measuring different freezing mode Tannin and total phenol content in wine, its result is as shown in Figure 1.
It will be seen from figure 1 that use the red heart Hylocereus undatus of directly cooling, either in fruit juice still In finished wine, its tannin and total phenol content are all more than gradient cooling group doubles.
Understanding from the hereinafter organoleptic test of the experimental example 2 of the present invention, different freezing modes are to ice wine Aesthetic quality's impact is relatively big, and this has much relations with its tannin and total phenol content.
Experimental example 2
The red heart HUOLONG fruit ice wine providing embodiment 1~3 carries out sensory evaluation, by Application No. CN104962424A, publication date is the fire provided in the embodiment 6 in the patent application of 2015.10.07 Dragon fruit wine as a comparison case 2, contrasts embodiment 1~3 with comparative example 1 and comparative example 2, evaluation Result test result is as shown in table 2.
Sensory evaluation method: evaluation group is by 20 member compositions, and they are according to the standards of grading of table 1 Color and luster, fragrance, mouthfeel and the quality of composite beverage is carried out independent marking, average with accumulative total score It is worth the sensory evaluation scores as product.
Sensory evaluation scores standard: refer to table 1.
Table 1 red heart HUOLONG fruit ice wine evaluation test sensory evaluation scores standard
Table 2 embodiment 1~6 sensory evaluation score
It is demonstrated experimentally that use the present invention provide method produce red heart HUOLONG fruit ice wine, its mouthfeel and The sensory evaluation scores of purity (referring mainly to color and luster, quality, abnormal smells from the patient) will be higher than comparative example.
Experimental example 3
Be the benchmark that experiment adjusts with embodiment 3, be separately added into 140,170,200,230,260, 290, the yeast of 320g/L, ferments according to the method described in embodiment 3, the red heart that will obtain HUOLONG fruit ice wine carries out sensory evaluation respectively.As shown in Figure 2, along with yeast-inoculated amount increases, fermentation Speed is accelerated, and ice wine quality strengthens, and when inoculum concentration reaches 230~270g/L, sensory evaluation is the highest. And if strengthen yeast-inoculated amount, then the index of quality such as wine body mouthfeel and color and luster can be caused to decline, cause commenting Divide and reduce.
Last it is noted that various embodiments above is only in order to illustrate technical scheme, rather than It is limited;Although the present invention being described in detail with reference to foregoing embodiments, but this area Those of ordinary skill it is understood that it still can be to the technical scheme described in foregoing embodiments Modify, or the most some or all of technical characteristic is carried out equivalent;And these amendments Or replace, do not make the essence of appropriate technical solution depart from the model of various embodiments of the present invention technical scheme Enclose.

Claims (10)

1. the preparation method of a red heart HUOLONG fruit ice wine, it is characterised in that comprise the following steps:
1), by the freezing of red heart Hylocereus undatus, squeezing, red heart dragon fruit juice is prepared;
2), in described red heart dragon fruit juice, clarifier, freezing 2~filter also after 4 days are added Add potassium metabisulfite;
3), adjust the sugar content of red heart dragon fruit juice and acidity, add saccharomyces cerevisiae and pectase enters Row temperature controlled fermentation, after having fermented, cooling is freezing and adds potassium metabisulfite termination fermentation;
4), filter separation wine mud, obtain wine base;
5), by fill after described wine base low temperature aging, filtration, sterilizing.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that Step 1) specifically include:
Fresh mature red heart Hylocereus undatus harvesting obtained carries out gradient with 1 DEG C~3 DEG C of speed hourly Cooling, is incubated 12~16h, squeezes extracting juice, prepare red heart dragon fruit juice after being down to-8 DEG C~-4 DEG C.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that In step 2) in, described clarifier is PVPP or bentonite, and addition is 800~1200mg/L.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that In step 2) in, the temperature of described freezing is-9 DEG C~-4 DEG C.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that In step 2) and step 3) in, the addition of described potassium metabisulfite is 70~110g/t.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that In step 3) in, the concrete mode of the sugar content and acidity that adjust red heart dragon fruit juice is:
The sugar content adding white sugar adjustment red heart dragon fruit juice is 285~300g/L;Add tartaric acid to adjust Whole acid content is 8~9g/L.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 1, it is characterised in that In step 3) in, the addition of described saccharomyces cerevisiae is 230~270g/L, and the addition of pectase is 30~35mg/L.
The preparation method of red heart HUOLONG fruit ice wine the most according to claim 7, it is characterised in that In step 3) in, the condition of described temperature controlled fermentation is
18 DEG C~20 DEG C ferment 30~40 days.
9., according to the preparation method of the red heart HUOLONG fruit ice wine described in any one of claim 1~8, it is special Levy and be, in step 5) in,
Described aging is specially 0 DEG C~5 DEG C of tanks storage 6~12 months.
10. the red heart HUOLONG fruit ice wine that prepared by the preparation method described in any one of claim 1~9.
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