CN105906726A - Manufacturing method for producing low-moisture starch through microwave method - Google Patents

Manufacturing method for producing low-moisture starch through microwave method Download PDF

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Publication number
CN105906726A
CN105906726A CN201610393600.8A CN201610393600A CN105906726A CN 105906726 A CN105906726 A CN 105906726A CN 201610393600 A CN201610393600 A CN 201610393600A CN 105906726 A CN105906726 A CN 105906726A
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China
Prior art keywords
microwave
starch
low moisture
microwave drying
moisture starch
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CN201610393600.8A
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Chinese (zh)
Inventor
王俭
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JIANGSU XINYU PHARMACY CO Ltd
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JIANGSU XINYU PHARMACY CO Ltd
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Priority to CN201610393600.8A priority Critical patent/CN105906726A/en
Publication of CN105906726A publication Critical patent/CN105906726A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B30/00Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
    • C08B30/06Drying; Forming

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Confectionery (AREA)

Abstract

The invention discloses a manufacturing method for producing low-moisture starch through a microwave method. The method comprises the steps that 1, corn starch is selected as a material; 2, the material of equal quantity in a raw material barrel is dug into a laying device through an automatic feeding system, and the material is laid on a conveying belt according to the certain thickness through the laying device; 3, the operation speed of the conveying belt is set according to the corresponding material thickness, the material is fed into multiple section microwave drying boxes to be heated, dried and sterilized, and the heating temperature in the multiple sections of microwave drying boxes are sequentially improved; 4, the material is fed into a stirrer for power loosening; 5, a vibration sieve with the hole diameter of 100 meshed is used for sieving the material; 6, the low-moisture starch is detected according to following indexes. The method for producing the low-moisture starch through the microwave method is an assembly line work way, and the material is automatically dried and sterilized through the microwave drying equipment; the intelligent technology is adopted in the production line, the temperature and moisture of the material are monitored in real time, and therefore whole-process precise control is achieved.

Description

Microwave method produces the manufacture method of low moisture starch
Technical field
The present invention relates to a kind of microwave method and produce the manufacture method of low moisture starch, belong to low moisture The manufacture method technical field of starch.
Background technology
At present, produce low moisture starch and mainly have 3 kinds of methods: one is pneumatic conveying drying method, and two are Constant-pressure and high-temperature roasts method, and three is that vacuum roasts method.In pneumatic conveying drying method, owing to material is at height In speed air current flow, unavoidable phase mutual friction produces electrostatic, there is certain potential safety hazard.And show Two kinds had roast the method producing low moisture starch, due to the limitation of reaction pot volume, make Become the moisture between different pot time to there is certain difference, thus unit batch is too small (as used Big volume always mixes device, and the most total mixed device volume is limited eventually, the most then strengthen and produce into Originally) quality forming product is not sufficiently stable.And microwave method produces low moisture starch due to microwave certainly Body can avoid the deficiency of above method to hot feature.
Summary of the invention
Purpose: in order to overcome the deficiencies in the prior art, the present invention provides a kind of microwave method Produce the manufacture method of low moisture starch.
Technical scheme: for solving above-mentioned technical problem, the technical solution used in the present invention is:
A kind of microwave method produces the manufacture method of low moisture starch, comprises the steps:
Step one: select and meet the corn starch of GB/T8885-2008 national standard as material;
Step 2: utilize gravity system to dig stone device equally the material in Raw material pail In, material is pressed certain thickness and is spread on a moving belt by stone device;
Step 3: conveyer belt arranges the speed of service by corresponding material thickness, and material is sent into multistage Microwave drying oven carries out heating, is dried, sterilizing;Every section of microwave drying in multistage microwave drying oven Heating-up temperature in case improves successively;
Step 4: material is sent into blender and carries out loose powder;
Step 5: use the vibrosieve of aperture 100 mesh that material is sieved, obtain particle diameter little Finished product low moisture starch in 100 mesh;
Step 6: low moisture starch is detected by following index:
Organoleptic indicator: white powder, there is gloss, free from extraneous odour;Physical and chemical index: acidity butt ° T≤1.80, moisture %≤3.0, ash %≤0.15, speckle/cm2≤ 0.7, dioxy Change sulfur mg/kg≤30.0, fineness 100 mesh % >=99.0;Microbiological indicator: aerobe is total Number≤500cfu/g, mycete, yeast sum≤30cfu/g, coliform≤30MPN/100g;
Step 7: carry out metering packing by standard regulation;
Wherein, step 2, three, four, five, use semiclosed processing;Surrounding air cleanliness factor Reach preparation and the region division of crude drug process environments etc. in " Good Manufacturing Practice and Quality Control of Drug " The grit maximum allowable number of 300,000 grades in Ji, i.e. particle diameter >=5um: 10,500,000/ Cubic meter;Microorganism maximum allowable number: flcating germ 60,000/cubic metre;Settling bacteria 1000 Individual/ware.
Preferably, described step 3 uses four sections of microwave drying ovens, four sections of microwave drying It is 80 DEG C, 95 DEG C, 110 DEG C, 125 DEG C that case heating-up temperature sets gradually.
Preferably, in described four sections of microwave drying ovens, it is provided with temperature sensor, uses Temperature in control microwave drying oven in real time.
Preferably, described material is spread on a moving belt by the thickness of 0.02 meter, transmits Tape speed is set to 1.2 ms/min.
Preferably, described material is spread on a moving belt by the thickness of 0.025 meter, transmits Tape speed is set to 0.9 m/min.
Beneficial effect: the microwave method that the present invention provides produces the manufacture method of low moisture starch, its Advantage is as follows:
One, product quality is more stable: owing to whole production line realizes line production, automatization Degree is higher, can monitor temperature of charge, moisture in real time simultaneously, and carries out omnidistance accurately control System.Ensure the stability of product quality.
Two, energy-saving and emission-reduction: microwave treatment case, through strict matched design, makes microwave energy obtain Coupling, energy is fully used, and can save energy for same production capacity compared with additive method Amount 30%.Simultaneously because it is at relative closure that microwave method produces the whole production procedure of low moisture starch In the environment of carry out, the most just can largely avoided the pollution of dust, reduce dust quick-fried Fried risk.Most importantly the heating means of microwave method production low moisture starch are more traditional Steam or oil heating, equipment itself do not produce any affect environment pollutant (include noise, Dust, harmful exhaust etc.), it is a kind of heating means of environmental protection.
Three, automaticity is high, it is easy to control: microwave method produces the main work of low moisture starch Process flow Dou Shi automatization: gravity system feed, the uniform stone of stone device, microwave are dry The PLC of dry case selects Delta PLC to control, equipment is single break down time, it is possible to individually locate Reason product, it is to avoid because the fault of equipment own causes product to be wasted.Microwave enclosure use external The advanced online infrared temperature of multiple spot, installs the contactless temperature measurement on-line of import producing line Instrument, grasps display temperature of charge in real time, thus realizes accurately controlling baking temperature, it is to avoid temperature Too high affect product quality, technique initialization and Automated condtrol more in conveniently producing, can be carried out.This Outer also employing PID regulates self energy control mode, reduces temperature fluctuation.Microwave power converts heat energy Having instantaneity, heat material without thermal inertia, material is heated at once, otherwise material is just Can not get microwave heat and stop heating.The most whole flow production line automaticity height is prone to Operation and control.
Four, save area, improve working conditions: setting of conventional dry method low moisture Starch Production Standby the hugest, need to take the biggest plant area.And microwave method produces low water Divide its compact equipment of starch, take plant area the least, save the biggest spatial area. Unpleasant noise, height will not be produced during microwave method produces low moisture starch simultaneously The environment of heat, contaminated gas etc., which significantly improves working environment and labor condition.
Accompanying drawing explanation
Fig. 1 is gravity system, the structural representation of stone device;
Fig. 2 is gravity system A-A profile;
Fig. 3 is the structural representation of microwave drying oven.
Detailed description of the invention
Below in conjunction with the accompanying drawings the present invention is further described.
A kind of microwave method produces the manufacture method of low moisture starch, comprises the steps:
Step one: select and meet the corn starch of GB/T8885-2008 national standard as material;
Step 2: as shown in Figure 1 and Figure 2, utilizes autofeed by the material in Raw material pail 1 In system 2, the Wa Liao mechanism of feed driven by motor digs in stone device 3 equally, stone device 3 Material is layered on conveyer belt by certain thickness by the mixer structure 32 that the stone motor 31 of bottom drives On 4;
Step 3: as it is shown on figure 3, conveyer belt 4 arranges the speed of service by corresponding material thickness, Material is sent into four sections of microwave drying ovens 5 carry out heating, be dried, sterilizing;Four sections of microwave drying In case 5, the heating-up temperature in every section of microwave drying oven 5 improves successively;Four sections of microwave drying ovens 5 It is 80 DEG C, 95 DEG C, 110 DEG C, 125 DEG C that heating-up temperature sets gradually;
Step 4: material is sent into blender and carries out loose powder;
Step 5: use the vibrosieve of aperture 100 mesh that material is sieved, obtain particle diameter little Finished product low moisture starch in 100 mesh;
Step 6: low moisture starch is detected by following index:
Organoleptic indicator: white powder, there is gloss, free from extraneous odour;Physical and chemical index: acidity butt ° T≤1.80, moisture %≤3.0, ash %≤0.15, speckle/cm2≤ 0.7, dioxy Change sulfur mg/kg≤30.0, fineness 100 mesh % >=99.0;Microbiological indicator: aerobe is total Number≤500cfu/g, mycete, yeast sum≤30cfu/g, coliform≤30MPN/100g;
Step 7: carry out metering packing by standard regulation;
Wherein, step 2, three, four, five, use semiclosed processing;Surrounding air cleanliness factor Reach preparation and the region division of crude drug process environments etc. in " Good Manufacturing Practice and Quality Control of Drug " The grit maximum allowable number of 300,000 grades in Ji, i.e. particle diameter >=5um: 10,500,000/ Cubic meter;Microorganism maximum allowable number: flcating germ 60,000/cubic metre;Settling bacteria 1000 Individual/ware.
Preferably, in described four sections of microwave drying ovens, it is provided with temperature sensor, uses The temperature in microwave drying oven and the temperature of observation material is controlled in real time.
Embodiment 1, described material is spread on a moving belt by the thickness of 0.02 meter, transmits belt speed Degree is set to 1.2 ms/min.
Embodiment 2, described material is spread on a moving belt by the thickness of 0.025 meter, transmits belt speed Degree is set to 0.9 m/min.
The above is only the preferred embodiment of the present invention, it should be pointed out that: for the art For those of ordinary skill, under the premise without departing from the principles of the invention, it is also possible to make some Improvements and modifications, these improvements and modifications also should be regarded as protection scope of the present invention.

Claims (5)

1. the manufacture method of a microwave method production low moisture starch, it is characterised in that: include as follows Step:
Step one: select and meet the corn starch of GB/T8885-2008 national standard as material;
Step 2: utilize gravity system to dig stone device equally the material in Raw material pail In, material is pressed certain thickness and is spread on a moving belt by stone device;
Step 3: conveyer belt arranges the speed of service by corresponding material thickness, and material is sent into multistage Microwave drying oven carries out heating, is dried, sterilizing;Every section of microwave drying in multistage microwave drying oven Heating-up temperature in case improves successively;
Step 4: material is sent into blender and carries out loose powder;
Step 5: use the vibrosieve of aperture 100 mesh that material is sieved, obtain particle diameter little Finished product low moisture starch in 100 mesh;
Step 6: low moisture starch is detected by following index:
Organoleptic indicator: white powder, there is gloss, free from extraneous odour;Physical and chemical index: acidity butt ° T≤1.80, moisture %≤3.0, ash %≤0.15, speckle/cm2≤ 0.7, dioxy Change sulfur mg/kg≤30.0, fineness 100 mesh % >=99.0;Microbiological indicator: aerobe is total Number≤500cfu/g, mycete, yeast sum≤30cfu/g, coliform≤30MPN/100g;
Step 7: carry out metering packing by standard regulation;
Wherein, step 2, three, four, five, use semiclosed processing;Surrounding air cleanliness factor Reach preparation and the region division of crude drug process environments etc. in " Good Manufacturing Practice and Quality Control of Drug " The grit maximum allowable number of 300,000 grades in Ji, i.e. particle diameter >=5um: 10,500,000/ Cubic meter;Microorganism maximum allowable number: flcating germ 60,000/cubic metre;Settling bacteria 1000 Individual/ware.
Microwave method the most according to claim 1 produces the manufacture method of low moisture starch, and it is special Levy and be: described step 3 uses four sections of microwave drying ovens, four sections of microwave drying oven heating-up temperatures Set gradually is 80 DEG C, 95 DEG C, 110 DEG C, 125 DEG C.
Microwave method the most according to claim 2 produces the manufacture method of low moisture starch, and it is special Levy and be: in described four sections of microwave drying ovens, be provided with temperature sensor, control in real time Temperature in microwave drying oven and the temperature of low moisture starch.
Microwave method the most according to claim 2 produces the manufacture method of low moisture starch, and it is special Levy and be: described material is spread on a moving belt by the thickness of 0.02 meter, and line speed is arranged It it is 1.2 ms/min.
Microwave method the most according to claim 2 produces the manufacture method of low moisture starch, and it is special Levy and be: described material is spread on a moving belt by the thickness of 0.025 meter, and line speed is arranged It it is 0.9 m/min.
CN201610393600.8A 2016-06-03 2016-06-03 Manufacturing method for producing low-moisture starch through microwave method Pending CN105906726A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470590A (en) * 2017-09-07 2019-03-15 中冶长天国际工程有限责任公司 A kind of online moisture content detection device of material and its detection method
CN110229240A (en) * 2019-06-01 2019-09-13 江苏昕宇药业有限公司 A kind of microwave manufacture craft of low moisture starch

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101050240A (en) * 2007-05-09 2007-10-10 重庆昊元生物产业(集团)有限公司 Process for preparing modified starch
CN102358756A (en) * 2011-08-11 2012-02-22 江苏昕宇药业有限公司 Manufacture method for medicinal starch
CN103712427A (en) * 2014-01-16 2014-04-09 长沙开元机电设备有限公司 Coal dust drying device
CN103743202A (en) * 2014-01-17 2014-04-23 河南勃达微波设备有限责任公司 Animal medicine nicarbazin drying process

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101050240A (en) * 2007-05-09 2007-10-10 重庆昊元生物产业(集团)有限公司 Process for preparing modified starch
CN102358756A (en) * 2011-08-11 2012-02-22 江苏昕宇药业有限公司 Manufacture method for medicinal starch
CN103712427A (en) * 2014-01-16 2014-04-09 长沙开元机电设备有限公司 Coal dust drying device
CN103743202A (en) * 2014-01-17 2014-04-23 河南勃达微波设备有限责任公司 Animal medicine nicarbazin drying process

Non-Patent Citations (1)

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Title
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109470590A (en) * 2017-09-07 2019-03-15 中冶长天国际工程有限责任公司 A kind of online moisture content detection device of material and its detection method
CN109470590B (en) * 2017-09-07 2024-03-12 中冶长天国际工程有限责任公司 Online moisture detection device and method for materials
CN110229240A (en) * 2019-06-01 2019-09-13 江苏昕宇药业有限公司 A kind of microwave manufacture craft of low moisture starch

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Application publication date: 20160831

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