CN105906250B - A kind of preparation method of physical simulation experiment analog material - Google Patents

A kind of preparation method of physical simulation experiment analog material Download PDF

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Publication number
CN105906250B
CN105906250B CN201610217671.2A CN201610217671A CN105906250B CN 105906250 B CN105906250 B CN 105906250B CN 201610217671 A CN201610217671 A CN 201610217671A CN 105906250 B CN105906250 B CN 105906250B
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China
Prior art keywords
parts
simulation experiment
preparation
mixed material
physical simulation
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CN201610217671.2A
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Chinese (zh)
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CN105906250A (en
Inventor
肖鹏
李树刚
林海飞
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Xian University of Science and Technology
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Xian University of Science and Technology
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

Abstract

The invention discloses a kind of preparation method of physical simulation experiment analog material, comprise the following steps:Following number is parts by weight, A, mixed material is added into mixer, heating stirring is carried out, mixed material includes, 100~120 parts of quartz sand, 35~50 parts of flyash, 15~30 parts of activated carbon, 20~50 parts of land plaster, 15~40 parts of cement and 200~300 parts of water;B, the mixed material after heating stirring is put into bobbing machine, and adds the additive for accounting for mixed material 1wt%~3wt%, consolidated;C, the raw material after tamping is subjected to heating crushing, obtains similarity simulation experiment material.The present invention can solve the problem that the deficiencies in the prior art, improve the reduction degree that similarity simulation experiment material is simulated for underground rock-soil layer.

Description

A kind of preparation method of physical simulation experiment analog material
Technical field
The present invention relates to geomechanics modeling technical field, especially a kind of system of physical simulation experiment analog material Preparation Method.
Background technology
Due to the mechanics study of the difficulty that the complexity and in-situ measurement of subterranean strata are tested, at the scene progress subterranean strata It is unpractiaca.So all it is come Study of The Underground engineering design and construction method by substantial amounts of geomechanical model test now Optimization, carry out construction process mechanics rule exploration.During geomechanics model is built, similarity simulation experiment material Whether can truly reflect the structure and property of underground rock-soil layer, turn into geomechanics model simulation effect height it is crucial because Element.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of preparation method of physical simulation experiment analog material, energy Enough solve the deficiencies in the prior art, improve the reduction degree that similarity simulation experiment material is simulated for underground rock-soil layer.
In order to solve the above technical problems, the technical solution used in the present invention is as follows.
A kind of preparation method of physical simulation experiment analog material, comprises the following steps:
Following number is parts by weight,
A, mixed material being added into mixer, carries out heating stirring, mixed material includes,
100~120 parts of quartz sand, 35~50 parts of flyash, 15~30 parts of activated carbon, 20~50 parts of gypsum Powder, 15~40 parts of cement and 200~300 parts of water;
B, the mixed material after heating stirring is put into bobbing machine, and adds the addition for accounting for mixed material 1wt%~3wt% Agent, consolidated;
C, the raw material after tamping is subjected to heating crushing, obtains similarity simulation experiment material.
Preferably, in step A, 5~15 parts of 4- amino -3- methyl-bromobenzoates are also included in mixed material.
Preferably, in step B, additive includes,
10~15 parts of 1,2- decanediols, 35~45 parts of ferrous sulfate, 3~5 parts of phenoxyacetyl chloride, 5~10 parts 2- nitrobenzamides, 5~8 parts of dibasic lead phosphite, 2~3 parts of diethylene-triamine pentaacetic acid sodium.
Preferably, in step B, before mixed material and additive is put into, it is painted with the surface of internal cavity of bobbing machine Interleaving agent.
Preferably, the interleaving agent includes,
30~35 parts of silicone oil, 3~5 parts of dipotassium hydrogen phosphate, 10~15 parts of acetone, 3~9 parts of 3- fluorine pyridines -4- Boric acid frequency is which ester.
Preferably, in the step A, heating and temperature control is at 75~85 DEG C;Mixing speed control 120~ 150rad/min。
Preferably, in the step C, heating and temperature control is at 135~160 DEG C.
It is using beneficial effect caused by above-mentioned technical proposal:The present invention is by improving similarity simulation experiment material Formula, the degree of adhesion of similarity simulation experiment material is improved, thus can effectively simulate along ground and be in long-term high in underground Time of day under pressure condition.In addition, the similarity simulation experiment material prepared by the present invention passes through when building test model Different ambient conditions can simulate a variety of ground Status Types, while only need to carry out when switching between different conditions It is corresponding to rinse and dry, it is convenient and swift.
Embodiment
In order that objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair It is bright.
The embodiments of the invention provide a kind of preparation method of physical simulation experiment analog material, including following step Suddenly:
Following number is parts by weight,
A, mixed material is added into mixer, carries out heating stirring, heating and temperature control is at 80 DEG C;Mixing speed control exists 130rad/min, mixed material include,
110 parts of quartz sand, 45 parts of flyash, 17 parts of activated carbon, 25 parts of land plaster, 20 parts of cement and 260 The water of part;And 5 parts of 4- amino -3- methyl-bromobenzoates.
B, the mixed material after heating stirring is put into bobbing machine, and adds the additive for accounting for mixed material 1.7wt%, entered Row tamping;Before mixed material and additive is put into, interleaving agent is painted with the surface of internal cavity of bobbing machine;Additive includes,
12 parts of 1,2- decanediols, 40 parts of ferrous sulfate, 4 parts of phenoxyacetyl chloride, 9 parts of 2- nitrobenzamides, 8 The dibasic lead phosphite, 3 parts of diethylene-triamine pentaacetic acid sodium of part;
Interleaving agent includes,
31 parts of silicone oil, 3 parts of dipotassium hydrogen phosphate, 11 parts of acetone, 8 parts of 3- fluorine pyridine -4- boric acid frequency any ester.
C, the raw material after tamping is subjected to heating crushing, obtains similarity simulation experiment material, heating and temperature control is 155 ℃。
Retrieved by inventor, the B of Chinese invention patent CN 103183495 be one with the present invention be closer to it is existing Technology.Inventor is contrasted using this prior art and preparation method provided by the invention, and material property is as follows:
As seen from the above table, there is wider performance interval using the similarity simulation experiment material prepared by the present invention, can Effectively to simulate various types of Lithology type.Because this similarity simulation experiment material has bigger tension and resistance to compression Strength Changes scope, so the geologic modelling for the frozen soil layer that is particularly suitable for use in.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (5)

1. a kind of preparation method of physical simulation experiment analog material, it is characterised in that comprise the following steps:
Following number is parts by weight,
A, mixed material being added into mixer, carries out heating stirring, mixed material includes,
5~15 parts of 4- amino -3- methyl-bromobenzoates, 100~120 parts of quartz sand, 35~50 parts of flyash, 15~30 The activated carbon, 20~50 parts of land plaster, 15~40 parts of cement and 200~300 parts of water of part;
B, the mixed material after heating stirring is put into bobbing machine, and adds the additive for accounting for mixed material 1wt%~3wt%, Consolidated;The additive includes 10~15 parts of 1,2- decanediols, 35~45 parts of ferrous sulfate, 3~5 parts of benzene oxygen acetyl Chlorine, 5~10 parts of 2- nitrobenzamides, 5~8 parts of dibasic lead phosphite, 2~3 parts of diethylene-triamine pentaacetic acid Sodium;
C, the raw material after tamping is subjected to heating crushing, obtains similarity simulation experiment material.
2. the preparation method of physical simulation experiment analog material according to claim 1, it is characterised in that:Step B In, before mixed material and additive is put into, interleaving agent is painted with the surface of internal cavity of bobbing machine.
3. the preparation method of physical simulation experiment analog material according to claim 2, it is characterised in that:It is described every Include from agent,
30~35 parts of silicone oil, 3~5 parts of dipotassium hydrogen phosphate, 10~15 parts of acetone, 3~9 parts of 3- fluorine pyridine -4- boric acid Frequency any ester.
4. the preparation method of physical simulation experiment analog material according to claim 1, it is characterised in that:Step A In, heating and temperature control is at 75~85 DEG C;Mixing speed is controlled in 120~150rad/min.
5. the preparation method of physical simulation experiment analog material according to claim 1, it is characterised in that:Step C In, heating and temperature control is at 135~160 DEG C.
CN201610217671.2A 2016-04-03 2016-04-03 A kind of preparation method of physical simulation experiment analog material Expired - Fee Related CN105906250B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5527387A (en) * 1992-08-11 1996-06-18 E. Khashoggi Industries Computer implemented processes for microstructurally engineering cementious mixtures
CN103183495A (en) * 2013-03-28 2013-07-03 山东大学 Fault analog simulation material used for fluid-solid coupling model test and preparation method thereof
CN103771781A (en) * 2014-01-02 2014-05-07 中煤科工集团重庆研究院有限公司 Similar material for coal and gas outburst simulation experiments and preparation method thereof
CN103964773A (en) * 2014-05-09 2014-08-06 中国矿业大学 Similar material for physical simulation of high-geo-temperature roadway
CN105092325A (en) * 2014-05-23 2015-11-25 中国石油化工股份有限公司 Natural sandstone simulation material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5527387A (en) * 1992-08-11 1996-06-18 E. Khashoggi Industries Computer implemented processes for microstructurally engineering cementious mixtures
CN103183495A (en) * 2013-03-28 2013-07-03 山东大学 Fault analog simulation material used for fluid-solid coupling model test and preparation method thereof
CN103771781A (en) * 2014-01-02 2014-05-07 中煤科工集团重庆研究院有限公司 Similar material for coal and gas outburst simulation experiments and preparation method thereof
CN103964773A (en) * 2014-05-09 2014-08-06 中国矿业大学 Similar material for physical simulation of high-geo-temperature roadway
CN105092325A (en) * 2014-05-23 2015-11-25 中国石油化工股份有限公司 Natural sandstone simulation material

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