CN105902424A - Native ice-flower soothing restoring gel and preparation method thereof - Google Patents

Native ice-flower soothing restoring gel and preparation method thereof Download PDF

Info

Publication number
CN105902424A
CN105902424A CN201610238046.6A CN201610238046A CN105902424A CN 105902424 A CN105902424 A CN 105902424A CN 201610238046 A CN201610238046 A CN 201610238046A CN 105902424 A CN105902424 A CN 105902424A
Authority
CN
China
Prior art keywords
preparation
releived
flower
gel
skin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610238046.6A
Other languages
Chinese (zh)
Inventor
梁春梅
郑生华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610238046.6A priority Critical patent/CN105902424A/en
Publication of CN105902424A publication Critical patent/CN105902424A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/042Gels
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/30Characterized by the absence of a particular group of ingredients
    • A61K2800/33Free of surfactant

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to a preparation method of native ice-flower soothing restoring gel. The native ice-flower soothing restoring gel comprises the following ingredients (by weight): A, 7-70 parts of an aqueous phase composition; B, 30-90 parts of a functional phase composition; C, 1-3 parts of an anti-corrosion composition; and D, 0.01-0.1 part of an aroma-increasing composition. The aqueous phase composition comprises water, dipropylene glycol, glycerin and an ammonium acryloyldimethyltaurate/VP copolymer. The functional phase composition comprises an ice-flower extracting solution, an aloe extracting solution, beta(1,3)- glucan or beta(1,6)- glucan, sodium hyaluronate and glycerophosphoinositol choline. The invention has the following advantages: compounding of the functional phase composition has synergetic effects; with cooperation of sodium hyaluronate, the product has good effects of protecting damage of ultraviolet light to skin and repairing damaged keratoderma; and as the ingredients are all natural plant ingredients and only ingredients with a bacteriostasis function is used except conventional preservative ingredients, the product is very safe to skin and will not produce any irritating reaction.

Description

A kind of primary frost flower is releived maintenance gel and preparation method thereof
Technical field
The present invention relates to skin care item production technical field, a kind of primary frost flower is releived maintenance gel and preparation side thereof Method.
Background technology
Ice plant, is commonly called as ice leaf grass.Belong to Aizoaceae (Aizoaseae), cat-chop class plant, annual or 2 years Raw herbaceous plant, is a kind of plant grown in the nano-cloth Namib desert in South Africa, and it is the most ancient that nano-cloth desert is referred to as the whole world Always, one of the most arid desert.Nano-cloth Namib desert daylight is strong, and ice plant is through the strong photograph of ultraviolet After penetrating, the ice crystal of its rhizome Surface Creation saloid grain of a kind of class, the fresh and tender succulence of its leaf, can eat raw, often make in France arranges With, there is salt capsule on blade face, and entrance has saline taste, is then mostly used for ornamental plantation in China.Rich in various right in ice leaf grass extracting solution The element that skin is excellent: flesh alcohols material belongs to the one of glucose, is to promote indispensable vitamin B system in cells grown Row.Suppression activity in vivo acid element, plays scavenging activity, also has defying age, alleviate the effect that skin is nervous.Proline can carry The moistening effect of high keratodermatitis, adjusts skin condition, promotes skin metabolism.More can generate the glue constituting corium element Former protein ingredient, keeps skin elasticity, has the effect of beauty treatment.Rich in minerals nutrients such as sodium (Na) and potassium (K).Except this Outside, also rich in elements such as calcium, zinc, manganese.There is regulation oils and fats balance, effect of pore refining.
Existing skin care item have side effect mostly, and skin care item are irreversible to the damage of skin, after using Skin is severely damaged.
At present, market does not utilize ice leaf grass extracting solution to prepare skin-protection product.
Summary of the invention
It is an object of the invention to provide a kind of primary frost flower to releive maintenance gel and preparation method thereof, to solve the above-mentioned back of the body The problem proposed in scape technology.
For achieving the above object, the present invention provides following technical scheme: a kind of primary frost flower is releived the preparation of maintenance gel Method, includes following components by weight:
Described water phase components carries out proportioning by following weight portion:
Described function phase component carries out proportioning by following weight portion:
Described anticorrosion component carries out proportioning by following weight portion:
Decoyl hydroximic acid 0.5~1.0,
1,3-PD 0.1~0.2,
1,6-hexanediol 1.0~2.0.
Described perfume component of composing is quintessence oil.
A kind of primary frost flower described in preparation is releived the method for maintenance gel, comprises the following steps:
S1, each material of water phase components is added in system material pot, be heated to 80~85 DEG C, stirring mixing, dissolve all Even;
S2, by system material pot in water phase components be cooled to 40~45 DEG C, add function phase component each material, stirring mixing Uniformly;
S3, again antiseptic ingredient and each material composed in fragrant component are added in system material pot, be uniformly mixed;
S4, it is evacuated to-0.05MPa, deaeration;
S5, detect qualified, with 100~150 mesh filter screens filter dischargings, obtain finished product.
Compared with prior art, the invention has the beneficial effects as follows:
1, frost flower extracting solution, Aloe extraction solution, β (1,3)-glucosan, β (1,6)-glucosan, glycerol squama acid inositol choline The compound synergistic function of salt, coordinates the synergism of hyaluronate sodium etc., to protectiving ultraviolet to the damage of skin and skin Maintenance effect after skin horny layer is impaired is fine, and the agent of this group all uses the plant component of natural origin, and only use has antibacterial The composition of function does not use conventional preservatives component, and skin will not produce the most safely irritant reaction.It is a the safest Maintenance product is damaged after protection before efficient solarization, solarization.
2, instant invention overcomes sun-proof series products on existing market the most substantially use chemical sun or chemistry add physics prevent Shine agent, be easily caused the security disadvantages stimulating skin.
3, the present invention have the protective action to ultraviolet, the calm maintenance of releiving of sensitivity skin, shine after skin impaired The multiple efficacies such as maintenance, efficient replenishing water and preserving moisture.
What 4, effect thing of the present invention used is all that natural plants extracts, and utilizes plant sun mechanism, plays protection purple The outside line protective action to skin injury.
5, the present invention is in addition to the effect of protectiving ultraviolet, also has maintenance effect to having damaged skin, to sensitive skin The effect of releiving, also has stronger replenishing water and preserving moisture effect.
6, the present invention easily causes the preservative of skin irritation safety problem, essence, table without interpolation normal in cosmetics The materials such as face activating agent, and use instead without adding preservative, composing the methods such as fragrant with quintessence oil, further ensureing outside product function, Make Product Safety as mild as a dove.
Detailed description of the invention
Below in conjunction with specific embodiments, technical scheme is clearly and completely described, it is clear that institute The embodiment described is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, The every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, broadly falls into this The scope of bright protection.
[embodiment 1]:
A kind of primary frost flower is releived the preparation method of maintenance gel, includes following components by weight:
Described water phase components carries out proportioning by following weight portion:
Described function phase component carries out proportioning by following weight portion:
Described anticorrosion component carries out proportioning by following weight portion:
Decoyl hydroximic acid 0.5,
1,3-PD 0.2,
1,6-hexanediol 2.0.
Described perfume component of composing is quintessence oil.
A kind of primary frost flower described in preparation is releived the method for maintenance gel, comprises the following steps:
S1, each material of water phase components is added in system material pot, be heated to 85 DEG C, stirring mixing, it is uniformly dissolved;
S2, the water phase components in system material pot being cooled to 40 DEG C, add each material of function phase component, stirring mixing is all Even;
S3, again antiseptic ingredient and each material composed in fragrant component are added in system material pot, be uniformly mixed;
S4, it is evacuated to-0.05MPa, deaeration;
S5, detect qualified, with 150 mesh filter screens filter dischargings, obtain finished product.
[embodiment 2]:
A kind of primary frost flower is releived the preparation method of maintenance gel, includes following components by weight:
Described water phase components carries out proportioning by following weight portion:
Described function phase component carries out proportioning by following weight portion:
Described anticorrosion component carries out proportioning by following weight portion:
Decoyl hydroximic acid 0.8,
1,3-PD 0.15,
1,6-hexanediol 1.5.
Described perfume component of composing is quintessence oil.
A kind of primary frost flower described in preparation is releived the method for maintenance gel, comprises the following steps:
S1, each material of water phase components is added in system material pot, be heated to 82 DEG C, stirring mixing, it is uniformly dissolved;
S2, the water phase components in system material pot being cooled to 42 DEG C, add each material of function phase component, stirring mixing is all Even;
S3, again antiseptic ingredient and each material composed in fragrant component are added in system material pot, be uniformly mixed;
S4, it is evacuated to-0.05MPa, deaeration;
S5, detect qualified, with 100 mesh filter screens filter dischargings, obtain finished product.
The present embodiment is most preferred embodiment.
[embodiment 3]:
A kind of primary frost flower is releived the preparation method of maintenance gel, includes following components by weight:
Described water phase components carries out proportioning by following weight portion:
Described function phase component carries out proportioning by following weight portion:
Described anticorrosion component carries out proportioning by following weight portion:
Decoyl hydroximic acid 1.0,
1,3-PD 0.1,
1,6-hexanediol 1.0.
Described perfume component of composing is quintessence oil.
A kind of primary frost flower described in preparation is releived the method for maintenance gel, comprises the following steps:
S1, each material of water phase components is added in system material pot, be heated to 80 DEG C, stirring mixing, it is uniformly dissolved;
S2, the water phase components in system material pot being cooled to 45 DEG C, add each material of function phase component, stirring mixing is all Even;
S3, again antiseptic ingredient and each material composed in fragrant component are added in system material pot, be uniformly mixed;
S4, it is evacuated to-0.05MPa, deaeration;
S5, detect qualified, with 120 mesh filter screens filter dischargings, obtain finished product.
The primary frost flower obtained through technical scheme is releived maintenance gel, and this gel carries out measure of merit:
Skin ultraviolet protection, after-sun restorative measure of merit:
Clinical trial subjects measures of effectiveness
Select double blinding, random, comparative study test;Object (n=20) uses gel and the same matrix of Application Example 2 Formula does not add the Blank gel of effect thing and does placebo, one day twice, continuous surrounding.Volunteer is healthy women, year Age 20--45 year, use Application Example 2 gel in left face region, use same matrix Placebo gel in You Lian district Territory.
Skin area after using fixed dosage ultra violet lamp to smear 10 minutes, observed skin area after four hours Whether there is erythema situation because ultraviolet irradiates in skin.
Wherein: test result is marked with 5 points of full marks processed, preferably 5 points, worst is 0 point, its assessment result such as table Shown in 1.
Table 1:
Group 1 2 3 4 5 6 7 8 9 10 Meansigma methods
Left face 5 4 4 5 4 4 3 5 3 5
Right face 1 0 1 0 1 1 1 1 1 1
Group 11 12 13 14 15 16 17 18 19 20
Left face 4 5 4 5 3 5 4 5 2 5 4.2
Right face 1 0 0 0 1 0 0 0 0 2 0.6
Skin is releived effect, moisturizing measure of merit:
Clinical trial subjects measures of effectiveness
Select double blinding, random, comparative study test;Object (n=20) uses gel and the same matrix of Application Example 2 Formula does not add the blank of effect thing line glue of being crazy about and does placebo, one day twice, continuous surrounding.Volunteer is healthy women, Age 20--45 year, use Application Example 2 gel in left face region, use same matrix formula do not add effect thing Placebo Blank gel in right face region.
Test application area is used to smear with product after stimulating skin with 0.1% fruit acid, tester's readme scoring and employing Skin moisture analyzer test zones of different water content method is evaluated.
Wherein: test result is marked with 5 points of full marks processed, preferably 5 points, worst is 0 point, its assessment result such as table Shown in 2.
Table 2:
To sum up can show that this product is obvious in terms of releive skin irritant reaction and moistening effect after using, make skin exist Use rear skin moisture sufficient.
Although the present invention being described in detail with reference to previous embodiment, for a person skilled in the art, Technical scheme described in foregoing embodiments still can be modified by it, or carries out wherein portion of techniques feature With replacing, all within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in this Within the protection domain of invention.

Claims (6)

1. a primary frost flower is releived the preparation method of maintenance gel, it is characterised in that: include following components by weight:
The primary frost flower of one the most according to claim 1 is releived maintenance gel, it is characterised in that: described water phase components is by such as Lower weight portion carries out proportioning:
A kind of primary frost flower the most according to claim 1 is releived the preparation method of maintenance gel, it is characterised in that: described merit Proportioning can be carried out by phase component by following weight portion:
A kind of primary frost flower the most according to claim 1 is releived the preparation method of maintenance gel, it is characterised in that: described anti- Rotten component carries out proportioning by following weight portion:
Decoyl hydroximic acid 0.5~1.0,
1,3-PD 0.1~0.2,
1,6-hexanediol 1.0~2.0.
A kind of primary frost flower the most according to claim 1 is releived the preparation method of maintenance gel, it is characterised in that: described tax Fragrant component is quintessence oil.
6. the preparation a kind of primary frost flower as described in Claims 1 to 5 is releived the method for maintenance gel, it is characterised in that: include Following steps:
S1, each material of water phase components is added in system material pot, be heated to 80~85 DEG C, stirring mixing, it is uniformly dissolved;
S2, the water phase components in system material pot being cooled to 40~45 DEG C, add each material of function phase component, stirring mixing is all Even;
S3, again antiseptic ingredient and each material composed in fragrant component are added in system material pot, be uniformly mixed;
S4, it is evacuated to-0.05MPa, deaeration;
S5, detect qualified, with 100~150 mesh filter screens filter dischargings, obtain finished product.
CN201610238046.6A 2016-04-14 2016-04-14 Native ice-flower soothing restoring gel and preparation method thereof Pending CN105902424A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610238046.6A CN105902424A (en) 2016-04-14 2016-04-14 Native ice-flower soothing restoring gel and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610238046.6A CN105902424A (en) 2016-04-14 2016-04-14 Native ice-flower soothing restoring gel and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105902424A true CN105902424A (en) 2016-08-31

Family

ID=56747035

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610238046.6A Pending CN105902424A (en) 2016-04-14 2016-04-14 Native ice-flower soothing restoring gel and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105902424A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108938498A (en) * 2018-09-25 2018-12-07 广州好润生物科技有限公司 A kind of antiallergic remediation composition and its preparation method and application with inhibition histamine release

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2949682A1 (en) * 2009-09-07 2011-03-11 Rocher Yves Biolog Vegetale Use of ice plant (Mesembryanthemum crystallinum) extract for the preparation of a cosmetic or dermatological composition for protecting and/or regenerating skin and hair
CN103607882A (en) * 2012-02-06 2014-02-26 十兴株式会社 Technique and method for producing functional material originated from ice plant, and functional component
CN105147535A (en) * 2015-09-29 2015-12-16 丘桂荣 Essence capable of reducing wrinkles, compacting, repairing, whitening and removing freckles and preparing method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2949682A1 (en) * 2009-09-07 2011-03-11 Rocher Yves Biolog Vegetale Use of ice plant (Mesembryanthemum crystallinum) extract for the preparation of a cosmetic or dermatological composition for protecting and/or regenerating skin and hair
CN103607882A (en) * 2012-02-06 2014-02-26 十兴株式会社 Technique and method for producing functional material originated from ice plant, and functional component
CN105147535A (en) * 2015-09-29 2015-12-16 丘桂荣 Essence capable of reducing wrinkles, compacting, repairing, whitening and removing freckles and preparing method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
刘德军: "《现代中药化妆品制作工艺及配方》", 28 February 2009 *
吉林万通集团通化清水丽人化妆品有限公司: "《http://125.35.6.80:8080/ftba/itownet/hzp_ba/fw/pz.jsp?processid=20141124135311kzu9f&nid=20141124135311kzu9f》", 5 January 2015 *
杨彤: "《美容药物学(第2版)》", 30 April 2007 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108938498A (en) * 2018-09-25 2018-12-07 广州好润生物科技有限公司 A kind of antiallergic remediation composition and its preparation method and application with inhibition histamine release
CN108938498B (en) * 2018-09-25 2021-11-12 广州天然国度生物科技有限公司 Anti-allergy repair composition capable of inhibiting histamine release and preparation method and application thereof

Similar Documents

Publication Publication Date Title
CN103263372B (en) Natural flower petal and cosmetic adopting same
KR101374093B1 (en) The functional beauti-pacl and its manufacturing method
CN105168054A (en) Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask
CN105476950B (en) Moisturizing foam mildy wash and preparation method thereof
CN107811938A (en) A kind of natural tea pasta film and preparation method thereof
KR20160001112A (en) Composition for the treatment and improvement of atopic dermatitis
CN106309340A (en) Grapefruit juice anti-wrinkle skin care formula
KR102255283B1 (en) Mask pack composition containing complex mixtures comprising the extraction mixture from marine plants and mask pack using the same
CN108078854A (en) Hand frost and preparation method thereof is repaired in a kind of moisturizing
KR101822092B1 (en) Cosmetic composition for preventing thermal skin aging containing aloe vera leaves complex extract
CN108078864B (en) Tea bran-containing composition and preparation method and application thereof
KR101553873B1 (en) A textile products with excellent antimicrobial and blood circulating characteristics
CN109528526A (en) Plant essence skin conditioning agent and preparation method thereof and oil control and acne removal application
CN104188859B (en) A kind of crease-resistant skin care emulsion containing natural component extract and preparation method thereof
CN109568159A (en) Cosmetic composition and its preparation method and application is repaired in a kind of whitening
KR20200029289A (en) Cosmetic composition with skin soothing effect comprising mushroom complex extract, and manufacturing method thereof
CN113398043A (en) Composite hermetia illucens oil composition and application thereof
CN104814916A (en) Moisturizing essence and preparing method thereof
KR102047949B1 (en) Soap composition comprising mixture of Chojeong mineral water and extract of fruit from Hippophae Rhamnoides
CN104224676A (en) Spirulina anti-wrinkle anti-aging facial mask
CN105796436A (en) Skin whitening and bromhidrosis eliminating liquid
CN111450005A (en) Beautifying and skin-brightening composition, beautifying and skin-brightening skin care product and preparation method thereof
KR100955085B1 (en) The preparation method of composition for moisturizing skin comprising extracts of pine needle
CN105902424A (en) Native ice-flower soothing restoring gel and preparation method thereof
CN105640836B (en) A kind of surfactant and preparation method thereof containing lotus active constituent

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20160831