CN105886388A - Biological fermentation tank - Google Patents
Biological fermentation tank Download PDFInfo
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- CN105886388A CN105886388A CN201610377034.1A CN201610377034A CN105886388A CN 105886388 A CN105886388 A CN 105886388A CN 201610377034 A CN201610377034 A CN 201610377034A CN 105886388 A CN105886388 A CN 105886388A
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/20—Material Coatings
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/38—Caps; Covers; Plugs; Pouring means
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M23/00—Constructional details, e.g. recesses, hinges
- C12M23/48—Holding appliances; Racks; Supports
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M27/00—Means for mixing, agitating or circulating fluids in the vessel
- C12M27/02—Stirrer or mobile mixing elements
- C12M27/08—Stirrer or mobile mixing elements with different stirrer shapes in one shaft or axis
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/12—Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/12—Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
- C12M41/18—Heat exchange systems, e.g. heat jackets or outer envelopes
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12M—APPARATUS FOR ENZYMOLOGY OR MICROBIOLOGY; APPARATUS FOR CULTURING MICROORGANISMS FOR PRODUCING BIOMASS, FOR GROWING CELLS OR FOR OBTAINING FERMENTATION OR METABOLIC PRODUCTS, i.e. BIOREACTORS OR FERMENTERS
- C12M41/00—Means for regulation, monitoring, measurement or control, e.g. flow regulation
- C12M41/12—Means for regulation, monitoring, measurement or control, e.g. flow regulation of temperature
- C12M41/18—Heat exchange systems, e.g. heat jackets or outer envelopes
- C12M41/24—Heat exchange systems, e.g. heat jackets or outer envelopes inside the vessel
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Abstract
The invention relates to a biological fermentation tank which comprises a motor, a speed reducer, a stirring device, an upper cover, a fermentation bucket and a support. The upper cover is arranged at the upper end of the fermentation bucket and provided with a stirring opening, and the stirring device is arranged in the stirring opening and comprises a stirring shaft and stirring blades arranged on the stirring shaft. The stirring blades comprise the first stirring blade and the second stirring blade, the second stirring blade is arranged at the lower end of the stirring shaft, the first stirring blade is a flood dragon rotary blade, and the second stirring blade is a frame type stirring blade. Coatings are arranged on the outer sides of the stirring blades, the fermentation bucket is provided with an inner barrel body, an outer jacket and a shell in sequence from inside to outside, a heat preservation device is arranged between the outer jacket and the shell, a heating device is arranged between the inner barrel body and the outer jacket, and a sensor is arranged in the heat preservation device. The stirring blades are formed by combining the flood dragon rotary blade and the frame type stirring blade, therefore, reactants can be comprehensively stirred and can be effectively prevented from being pasted to the inner wall of the fermentation bucket, and the reaction rate is increased.
Description
Technical field
The present invention relates to reaction vessel field, particularly to a kind of biological fermentation tank.
Background technology
Biological fermentation tank is the external environment condition device that microorganism produced, and bred and formed product during the fermentation, with passing
System container compare, it can to the production process of fermentation tank carries out strict sterilizing, and fermented product is fed in time,
Stirring, needs temperature, pressure, air mass flow are carried out the yeasting automatically controlling and providing good during producing.
Fermentation tank is widely used in the fermentation of microorganism fungus kind, has ferment fast, sanitation and hygiene and the advantage of large-scale production, fermentation tank
Need to ensure certain cleanliness factor during production and processing, it is to avoid the inoculation mouth of fermentation tank and sample tap are exposed to air
In, expose aerial fermented product by the dirts being unfavorable for antibacterial that growth breeds, virus, fungus etc. various in air
Dye, affects the ferment effect of fermentation tank, can cause certain waste, even sample analysis can be produced certain impact, make former
Material lost efficacy, and therefore, the sealing of fermentation tank is key issue to be solved in fermentation tank production process.
In fermentation tank, the mixing effect tool of fermentation tank is had a certain impact by the quality of paddle and the shape of paddle,
Existing paddle is easily subject to the impact of fermented product, can have certain corrosion, wear effect to paddle, in the process of stirring
The stirring thing of middle generation can be bonded on paddle, paddle can be produced certain impact, decrease the service life of fermentation tank.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, it is provided that a kind of biological fermentation tank, to solve in prior art
The problem existed.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of biological fermentation tank, it is characterised in that: include motor, reductor, agitating device, upper cover, fermenter and support, institute
Stating fermenter lower end and be provided with support, described fermenter upper end is provided with upper cover, described on cover and be provided with stirring port, described agitating device
Being arranged in stirring port, described motor via reducer is connected with agitating device, and described agitating device includes shaft and sets
Putting the paddle on shaft, described paddle includes that the first paddle and the second paddle, described second paddle set
Putting the lower end at shaft, described first paddle is flood dragon rotating vane, and described second paddle is frame type stirring leaf, described
Being provided with coating outside paddle, described fermenter is from inside to outside sequentially provided with inner barrel, external jacket and shell, described external jacket
And it is provided with attemperator between shell, is provided with heater between described inner barrel and external jacket, is provided with in described attemperator
Sensor；Covering on described and be provided with charging aperture, described fermenter lower end is provided with drain hole.
As a modification of the present invention, one end of described flood dragon rotating vane contacts with fermenter inwall, described frame
The shape of formula paddle is identical with the shape bottom fermenter.
As a modification of the present invention, described fermenter upper end is provided with condensing unit, and described condensing unit includes condensation
Pipeline, water inlet and outlet, described water inlet is connected with outlet by condensation pipe, and described condensation pipe is U-shaped cold
Solidifying pipeline.
As a modification of the present invention, described attemperator includes the warming plate being arranged on two ends and is arranged on insulation
Heat-preservation cotton between plate.
As a modification of the present invention, described heater includes that conduction oil charging aperture, heat conducting oil pipe, conduction oil are arranged
Material mouth and heating rod, described conduction oil charging aperture is arranged on the upper end of heat conducting oil pipe, and described conduction oil discharge gate is arranged on
Heat conducting oil pipe lower end, described heating rod is arranged on heat conducting oil pipe lower end.
As a modification of the present invention, the thickness of described coating is 0.9-1.5mm.
As a modification of the present invention, the processing technique of described coating is as follows: 1) first used the metal surface of paddle
Acetone enters
After row cleans 5-6 minute, paddle is put into the mixture of clear water, acetone and dehydrated alcohol, and to paddle
Carry out supersound process 14-18 minute, then paddle is put into distilled water solution, paddle is carried out 6-8 minute；Institute
The weight ratio stating clear water, acetone and dehydrated alcohol is 3:5:3；
2) polyethylene 38-46 part will add 40-50 part deionized water and be constantly stirred, and add during stirring
Stir 20-30 minute after cross-linking agent 5-9 part；
3) conch meal 5-7 part, bone powder 6-8 part are put into and carried out after being stirred 10-13 minute under the ethanol solution of 42%
Filter, the mixture after filtering puts in the high-pressure separator of 0.5-0.8MPa and is centrifuged machine separating and dehydrating, mixed after dehydration
Compound puts into the drying unit of 45-52 DEG C dries, and the mixture after drying is put in grinder and is ground, and
Mixture after grinding adds dehydrated alcohol 6-8 part, distilled water 5-9 part, hydroxy silicon oil 5-8 part and through step 2) anti-
Mixture after should is stirred；
4) copper powder 42-50 part, nikel powder 18-20 part, zinc powder 30-40 part are ground by grinder, the mixing after grinding
Thing adds through the reacted product of step 3), and addition dispersant 9-14 part, oleic acid 6-9 part are gone forward side by side at 20-35 DEG C
Row stirring reaction 20-28 minute, then in mixture, add dehydrated alcohol 3-5 part, distilled water 10-15 part, and make mixture exist
After being stirred reaction at 45-52 DEG C 12-15 minute, in mixed solution, add polyester resin 10-14 part and be stirred 5-8
After minute, mixed liquor is heated, and make mixed liquor carry out reaction 5-6 minute at 70-75 DEG C；
5), after the mixture paint brush processed through step 4) being carried out primary coating, carry out being heated to 95-by mixture
100 DEG C, the mixture after heating is placed in high-pressure injection device and sprays paddle, is then cooled to by mixture
70-75 DEG C, and after paddle being carried out secondary coating by paint brush, paddle good for coating is stood at 20-25 DEG C 5-7
After minute, then the paddle that coating is good is put into carry out to the drying unit of 120 DEG C dry 40-45 minute；
6) silver peroxide 1.5-2 part, zinc peroxide 3-4 part are put into after lapping device is ground, and by ground
Mixture is put in agitating device, and adds polyester resin 11-14 part, deionized water 3-5 part in agitating device, and makes mixing
Thing is stirred 15-20 minute at 51-54 DEG C；
7) Chlorizate chromium 1-3 part, silver peroxide 0.9-1.2 part, zinc peroxide 0.2-0.8 part are put in grinder and is ground
After, mixture is heated to 90-100 DEG C, and the mixture after heating is put into and is stirred mixing to the oleum lini of 15-20 DEG C
Close；
8), after carrying out the paddle after step 5) coating at 15-18 DEG C standing 20-25 minute, paddle is put into rotation
Rotary device rotates, will be after the reacted mixture of step 6) be heated to 105-110 DEG C, the mixed liquor after heating falls
Enter in high-pressure injection device, and the paddle in rotating is sprayed, the paddle after injection is put into the drying dress of 120 DEG C
Dry in putting, after paddle after drying takes out, will at after step 7) is reacted, mixture is heated to 84-86 DEG C, and
Mixed liquor after heating is poured in high-pressure injection device, and the paddle in rotating is sprayed, paddle after spraying
It is arranged in program control stove, and in device, is filled with noble gas, after making paddle stand 5-8 minute at 1025-1100 DEG C, and
Heating up device, make paddle stand 30-36 minute at 1300-1500 DEG C, the paddle after standing is put after taking out
Dry in entering the drying unit of 120 DEG C, can be prepared by.
As a modification of the present invention, the conch meal described in step 3) and bone powder in the processing technique of described coating
A diameter of 32-44 μm.
As a modification of the present invention, the spray of high-pressure injection device described in step 5) in the processing technique of described coating
Injection pressure is 0.4-0.45MPa.
As a modification of the present invention, in the processing technique of described coating, the noble gas described in step 8) is argon.
Owing to have employed above technology, the present invention compared with the prior art, has the advantage that as follows:
The invention discloses a kind of simple in construction, a kind of biological fermentation tank safe and reliable, easy to use, with low cost, this
Bright middle stirring vane is flood dragon rotating vane and frame type stirring leaf combines, and can carry out the reactant in biological fermentation tank entirely
The stirring in face, one end of flood dragon rotating vane contacts with fermenter inwall, can effectively prevent the reactant in fermenter from gluing
On the inwall of fermenter, can strike off fermenter in time, the reactant can being prevented effectively from fermenter is piled up, and frame stirs
Mix leaf can the reactant bottom agitator tank be stirred, effectively accelerate the speed of stirring, improve reaction rate；This
It is provided with heater in bright, by heating rod directly to heat-conducting oil heating, is effectively increased the speed of heating；The present invention is provided with
Attemperator, can be incubated biological fermentation tank, can effectively prevent heat to run off, it is ensured that fermentation tank reacts
Temperature, be effectively increased the speed of reaction；The present invention is provided with in upper cover chiller, can in time fermentation tank be carried out cold
But, can effectively prevent fermentation tank from because temperature is too high, fermentation tank is produced certain impact, effectively extend fermentation tank
Service life；
In the present invention, paddle surface is provided with coating, through paddle carries out three sprayings, can be effectively increased paddle
Wearability, rust-preventing characteristic and corrosion resistance, be provided with preventing viscosity substance in coating in the present invention, can effectively prevent reactant from boning
On paddle top layer, it is effectively increased the speed of paddle；Paddle is being carried out between coating by the present invention, paddle warp successively
Cross acetone clean after, and the mixture putting into clear water, acetone and dehydrated alcohol carry out supersound process after enter through distilled water again
Row cleans, and can effectively remove the impurity of metal surface residual, and form layer protective layer in metal surface, and the surface of formation is protected
Sheath can react with copper powder, nikel powder, the polyethylene of zinc powder, it is possible to forms a stratification compound in metal surface, it is possible to make
The significantly more efficient metal surface being bonded at paddle of coating；Polyethylene is reacted by the present invention with deionized water, cross-linking agent
After, after reacting with the conch meal after high-pressure filteration, bone powder, the mixture of formation and dehydrated alcohol, distilled water, hydroxyl
After base silicone oil reacts, mixture reaction generated and copper powder, nikel powder, zinc powder add the mixing that will be formed again after reacting
Thing and dispersant, oleic acid carry out reaction and answer, and the mixture of formation reacts with polyester resin, can be formed and have high-wearing feature
Material, the mixture of generation can react with through the paddle anticipated, can be effectively by coating and stirring
The metal surface of leaf bonds, and prevents metal surface from coming off, and adds the wearability of paddle, the mixture of generation
There is certain antibiotic property, can effectively reduce the formation of antibacterial in fermentation tank, effectively increase the antibiotic property of paddle；This
After silver oxide, zinc peroxide are reacted by invention, the mixture of formation is reacted with polyester resin, deionized water,
The mixture formed heats, and is reacted by the paddle of the mixture after heating with low temperature, it is possible to make the mixed of formation
Compound is higher to be pasted onto on paddle, and has antirust mixture the surface of paddle formation one layer, makes mixture more
Add and there is rustless property, it is possible to effectively extend the service life of paddle；By Chlorizate chromium, silver peroxide, peroxidating in the present invention
Zinc is mixed and heated, and is put into by the mixture after heating and mixes to the oleum lini of 15-20 DEG C, and adds after mixing
Put into high-pressure injection device after heat to spray, and the mixture of the mixture of high temperature with paddle surface reacted,
The mixture formed has corrosion resistance and antistick characteristic, can be effectively improved the whipping performance of paddle, effectively extend paddle
Service life.
Accompanying drawing explanation
Fig. 1 is a kind of biological fermentation tank structural representation；
In figure: 1, motor, 2, reductor, 3, agitating device, 4, upper cover, 5, fermenter, 6, support, 7, stirring port, 8, shaft,
9, paddle, the 10, first paddle, the 11, second paddle, 12, inner barrel, 13, external jacket, 14, shell, 15, attemperator,
16, heater, 17, sensor, 18, charging aperture, 19, drain hole, 20, condensing unit, 21, condensation pipe, 22, conduction oil enters
Material mouth, 23, heat conducting oil pipe, 24, conduction oil discharge gate, 25, heating rod.
Detailed description of the invention
Below in conjunction with the accompanying drawings and detailed description of the invention, it is further elucidated with the present invention.
Embodiment 1:
Visible in conjunction with accompanying drawing, a kind of biological fermentation tank, including motor 1, reductor 2, agitating device 3, upper cover 4, fermenter 5 and
Support 6, described fermenter 5 lower end is provided with support 6, and described fermenter 5 upper end is provided with upper cover 4, and described upper cover 4 is provided with stirring port
7, described agitating device 3 is arranged in stirring port 7, and described motor 1 is connected with agitating device 3 by reductor 2, described stirring dress
Putting 3 and include shaft 8 and the paddle 9 being arranged on shaft 8, described paddle 9 includes the first paddle 10 and
Two paddles 11, described second paddle 11 is arranged on the lower end of shaft 8, and described first paddle 10 is flood dragon pivoting leaf
Sheet, described second paddle 11 is frame type stirring leaf, is provided with coating outside described paddle 9, and described fermenter 5 from inside to outside depends on
Secondary inner barrel 12, external jacket 13 and the shell 14 of being provided with, is provided with attemperator 15 between described external jacket 13 and shell 14, described
It is provided with heater 16 between inner barrel 12 and external jacket 13, in described attemperator 15, is provided with sensor 17；On described upper cover 4
Being provided with charging aperture 18, described fermenter 5 lower end is provided with drain hole 19.
It is provided with sensor 17 in described attemperator 15；Temperature in attemperator 15 can be detected, and pass through
Controller is adjusted, and effectively prevents fermenter 5 from because reaction temperature is too high, reactant is produced certain impact.
One end of described flood dragon rotating vane contacts with fermenter 5 inwall, fermentation tank inwall can be scraped wall and stir
Mix, can effectively prevent reactant to be bonded on the inwall of fermenter 5, be effectively increased response speed, prevent from being bonded in fermentation tank
The carbonization because temperature is too high of the reactant of wall, the shape of described frame type stirring leaf is identical with the shape bottom fermenter 5, permissible
The reactant of the bottom of fermentation tank is stirred, is effectively increased the speed of stirring.
Described fermenter 5 upper end is provided with condensing unit 20, described condensing unit 20 include condensation pipe 21, water inlet and
Outlet, described water inlet is connected with outlet by condensation pipe 21, and described condensation pipe 21 is U-shaped condensation pipe, permissible
Fermenter 5 upper end is cooled down, prevents fermentation tank because temperature is too high, and fermenter 5 is produced certain impact, decrease
The use time of fermenter 5.
Described attemperator 15 includes the warming plate being arranged on two ends and the heat-preservation cotton being arranged between warming plate, permissible
Fermenter 5 is incubated, effectively prevents the reactant temperature when reaction, effectively prevent scattering and disappearing of heat.
Described heater 16 includes conduction oil charging aperture 22, heat conducting oil pipe 23, conduction oil discharge gate 24 and heating
Rod 25, described conduction oil charging aperture 22 is arranged on the upper end of heat conducting oil pipe 23, and described conduction oil discharge gate 24 is arranged on heat conduction
Oil-piping 23 lower end, described heating rod 25 is arranged on heat conducting oil pipe 23 lower end, by being passed through heat conduction in heat conducting oil pipe 23
Oil, can be by heating the heating rod 25 being arranged in heat conducting oil pipe 23, and heat conductive rod sends temperature to conduction oil,
And fermenter 5 is heated, it is effectively increased reaction efficiency.
The present invention, specifically used process is as follows: start fermentation tank, after reactant is entered fermentation tank by charging aperture 18,
Closing charging aperture 18, motor 1 drives agitating device 3 to be stirred fermented product, the first paddle 10 and the second paddle 11
Fermented product is carried out mix and blend, and reacted mixture is discharged by drain hole 19.
Being provided with coating outside described paddle 9, the thickness of described coating is 0.9mm.
The processing technique of described coating is as follows: after 1) first the metal surface of paddle 9 being carried out 5 minutes with acetone,
Paddle 9 is put into the mixture of clear water, acetone and dehydrated alcohol, and paddle 9 is carried out supersound process 18 minutes,
Again paddle 9 is put into distilled water solution and paddle 9 is carried out 6 minutes；Described clear water, acetone and dehydrated alcohol
Weight ratio be 3:5:3；
2) polyethylene 46 parts will add 40 parts of deionized waters and be constantly stirred, and during stirring, add cross-linking agent
Stir 20 minutes after 9 parts；
3) conch meal 7 parts, 6 parts of bone powder are put into and filter after being stirred 13 minutes under the ethanol solution of 42%, incited somebody to action
Mixture after filter is put in the high-pressure separator of 0.5MPa and is centrifuged machine separating and dehydrating, and the mixture after dehydration puts into 52 DEG C
Drying unit in dry, and the mixture after drying is put in grinder and is ground, and the mixing after grinding
Thing adds dehydrated alcohol 6 parts, distilled water 9 parts, hydroxy silicon oil 5 parts and through step 2) reacted mixture stirs
Mix；
4) copper powder 50 parts, nikel powder 18 parts, zinc powder 40 parts are ground by grinder, the mixture after grinding adds warp
Cross the reacted product of step 3), and at 20 DEG C, add dispersant 14 parts, oleic acid 6 parts and be stirred reacting 28 minutes,
In mixture, add dehydrated alcohol 3 parts, distilled water 15 parts again, and make mixture be stirred reacting 15 minutes at 45 DEG C
After, after adding 10 parts of polyester resin in mixed solution and being stirred 8 minutes, mixed liquor is heated, and make mixed liquor exist
Carry out at 70 DEG C reacting 6 minutes；
5), after the mixture paint brush processed through step 4) being carried out primary coating, carry out being heated to 95 by mixture
DEG C, the mixture after heating is placed in high-pressure injection device and sprays paddle 9, then mixture is cooled to 75
DEG C, and after paddle 9 being carried out secondary coating by paint brush, after paddle 9 good for coating is stood 7 minutes at 20 DEG C,
Again paddle 9 good for coating is put into and carry out drying 40 minutes to the drying unit of 120 DEG C；
6) silver peroxide 2 parts, zinc peroxide 3 parts are put into after lapping device is ground, and by ground mixture
Put in agitating device 3, and in agitating device 3, add 14 parts of polyester resin, deionized water 3 parts, and make mixture at 54 DEG C
Under be stirred 15 minutes；
7) Chlorizate chromium 3 parts, silver peroxide 0.9 part, zinc peroxide 0.8 part are put into after being ground in grinder, to mixture
Be heated to 90 DEG C, and will heating after mixture put into be stirred to the oleum lini of 20 DEG C mixing；
8), after carrying out standing 25 minutes at 15 DEG C by the paddle 9 after step 5) coating, paddle 9 is put into rotation dress
Rotate in putting, will be after the reacted mixture of step 6) be heated to 105 DEG C, high pressure spray poured into by the mixed liquor after heating
In injection device, and the paddle 9 in rotating is sprayed, the drying unit that the paddle 9 after injection puts into 120 DEG C is entered
Row is dried, and after the paddle 9 after drying takes out, will be heated at 86 DEG C by mixture after step 7) is reacted, and by after heating
Mixed liquor pour in high-pressure injection device, and to rotate in paddle 9 spray, paddle after injection 9 is arranged at
In program control stove, and in device, it is filled with noble gas, after making paddle 9 stand 8 minutes at 1025 DEG C, and device is risen
Temperature, makes paddle 9 stand 36 minutes at 1300 DEG C, and the paddle 9 after standing puts into the drying unit of 120 DEG C after taking out
Dry, can be prepared by.
Conch meal described in step 3) and a diameter of 44 μm of bone powder in the processing technique of described coating.
In the processing technique of described coating, the expulsion pressure of high-pressure injection device described in step 5) is 0.4MPa.
In the processing technique of described coating, the noble gas described in step 8) is argon.
Embodiment 2:
Being provided with coating outside described paddle 9, the thickness of described coating is 1mm.
The processing technique of described coating is as follows: after 1) first the metal surface of paddle 9 being carried out 6 minutes with acetone,
Paddle 9 is put into the mixture of clear water, acetone and dehydrated alcohol, and paddle 9 is carried out supersound process 14 minutes,
Again paddle 9 is put into distilled water solution and paddle 9 is carried out 8 minutes；Described clear water, acetone and dehydrated alcohol
Weight ratio be 3:5:3；
2) polyethylene 38 parts will add 50 parts of deionized waters and be constantly stirred, and during stirring, add cross-linking agent
Stir 30 minutes after 5 parts；
3) conch meal 5 parts, 8 parts of bone powder are put into and filter after being stirred 10 minutes under the ethanol solution of 42%, incited somebody to action
Mixture after filter is put in the high-pressure separator of 0.8MPa and is centrifuged machine separating and dehydrating, and the mixture after dehydration puts into 45 DEG C
Drying unit in dry, and the mixture after drying is put in grinder and is ground, and the mixing after grinding
Thing adds dehydrated alcohol 8 parts, distilled water 5 parts, hydroxy silicon oil 8 parts and through step 2) reacted mixture stirs
Mix；
4) copper powder 42 parts, nikel powder 20 parts, zinc powder 30 parts are ground by grinder, the mixture after grinding adds warp
Cross the reacted product of step 3), and at 35 DEG C, add dispersant 9 parts, oleic acid 9 parts and be stirred reacting 20 minutes, then
Dehydrated alcohol 5 parts, distilled water 10 parts is added in mixture, and after making mixture be stirred reacting 12 minutes at 52 DEG C,
After adding 14 parts of polyester resin in mixed solution and being stirred 5 minutes, mixed liquor is heated, and make mixed liquor 75
Carry out at DEG C reacting 5 minutes；
5), after the mixture paint brush processed through step 4) being carried out primary coating, carry out being heated to 100 by mixture
DEG C, the mixture after heating is placed in high-pressure injection device and sprays paddle 9, then mixture is cooled to 70
DEG C, and after paddle 9 being carried out secondary coating by paint brush, after paddle 9 good for coating is stood 5 minutes at 25 DEG C,
Again paddle 9 good for coating is put into and carry out drying 45 minutes to the drying unit of 120 DEG C；
6) silver peroxide 1.5 parts, zinc peroxide 4 parts are put into after lapping device is ground, and by ground mixing
Thing is put in agitating device 3, and adds 11 parts of polyester resin, deionized water 5 parts in agitating device 3, and makes mixture 51
20 minutes it are stirred at DEG C；
7) Chlorizate chromium 1 part, silver peroxide 1.2 parts, zinc peroxide 0.2 part are put into after being ground in grinder, to mixture
Be heated to 100 DEG C, and will heating after mixture put into be stirred to the oleum lini of 15 DEG C mixing；
8), after carrying out standing 20 minutes at 18 DEG C by the paddle 9 after step 5) coating, paddle 9 is put into rotation dress
Rotate in putting, will be after the reacted mixture of step 6) be heated to 110 DEG C, high pressure spray poured into by the mixed liquor after heating
In injection device, and the paddle 9 in rotating is sprayed, the drying unit that the paddle 9 after injection puts into 120 DEG C is entered
Row is dried, and after the paddle 9 after drying takes out, will be heated at 84 DEG C by mixture after step 7) is reacted, and by after heating
Mixed liquor pour in high-pressure injection device, and to rotate in paddle 9 spray, paddle after injection 9 is arranged at
In program control stove, and in device, it is filled with noble gas, after making paddle 9 stand 5 minutes at 1100 DEG C, and device is risen
Temperature, makes paddle 9 stand 30 minutes at 1500 DEG C, and the paddle 9 after standing puts into the drying unit of 120 DEG C after taking out
Dry, can be prepared by.
Conch meal described in step 3) and a diameter of 44 μm of bone powder in the processing technique of described coating.
In the processing technique of described coating, the expulsion pressure of high-pressure injection device described in step 5) is 0.4MPa.
In the processing technique of described coating, the noble gas described in step 8) is argon.
Embodiment 3:
Being provided with coating outside described paddle 9, the thickness of described coating is 1.2mm.
The processing technique of described coating is as follows: after 1) first the metal surface of paddle 9 being carried out 6 minutes with acetone,
Paddle 9 is put into the mixture of clear water, acetone and dehydrated alcohol, and paddle 9 is carried out supersound process 16 minutes,
Again paddle 9 is put into distilled water solution and paddle 9 is carried out 7 minutes；Described clear water, acetone and dehydrated alcohol
Weight ratio be 3:5:3；
2) polyethylene 41 parts will add 48 parts of deionized waters and be constantly stirred, and during stirring, add cross-linking agent
Stir 29 minutes after 8 parts；
3) conch meal 6 parts, 7 parts of bone powder are put into and filter after being stirred 12 minutes under the ethanol solution of 42%, incited somebody to action
Mixture after filter is put in the high-pressure separator of 0.8MPa and is centrifuged machine separating and dehydrating, and the mixture after dehydration puts into 50 DEG C
Drying unit in dry, and the mixture after drying is put in grinder and is ground, and the mixing after grinding
Thing adds dehydrated alcohol 6 parts, distilled water 9 parts, hydroxy silicon oil 5 parts and through step 2) reacted mixture stirs
Mix；
4) copper powder 48 parts, nikel powder 18 parts, zinc powder 35 parts are ground by grinder, the mixture after grinding adds warp
Cross the reacted product of step 3), and at 35 DEG C, add dispersant 10 parts, oleic acid 9 parts and be stirred reacting 28 minutes,
In mixture, add dehydrated alcohol 4 parts, distilled water 10 parts again, and make mixture be stirred reacting 15 minutes at 45 DEG C
After, after adding 13 parts of polyester resin in mixed solution and being stirred 8 minutes, mixed liquor is heated, and make mixed liquor exist
Carry out at 72 DEG C reacting 5 minutes；
5), after the mixture paint brush processed through step 4) being carried out primary coating, carry out being heated to 100 by mixture
DEG C, the mixture after heating is placed in high-pressure injection device and sprays paddle 9, then mixture is cooled to 73
DEG C, and after paddle 9 being carried out secondary coating by paint brush, after paddle 9 good for coating is stood 6 minutes at 24 DEG C,
Again paddle 9 good for coating is put into and carry out drying 43 minutes to the drying unit of 120 DEG C；
6) silver peroxide 2 parts, zinc peroxide 3 parts are put into after lapping device is ground, and by ground mixture
Put in agitating device 3, and in agitating device 3, add 14 parts of polyester resin, deionized water 3 parts, and make mixture at 51 DEG C
Under be stirred 20 minutes；
7) Chlorizate chromium 1 part, silver peroxide 1.2 parts, zinc peroxide 0.2 part are put into after being ground in grinder, to mixture
Be heated to 100 DEG C, and will heating after mixture put into be stirred to the oleum lini of 18 DEG C mixing；
8), after carrying out standing 23 minutes at 18 DEG C by the paddle 9 after step 5) coating, paddle 9 is put into rotation dress
Rotate in putting, will be after the reacted mixture of step 6) be heated to 109 DEG C, high pressure spray poured into by the mixed liquor after heating
In injection device, and the paddle 9 in rotating is sprayed, the drying unit that the paddle 9 after injection puts into 120 DEG C is entered
Row is dried, and after the paddle 9 after drying takes out, will be heated at 84 DEG C by mixture after step 7) is reacted, and by after heating
Mixed liquor pour in high-pressure injection device, and to rotate in paddle 9 spray, paddle after injection 9 is arranged at
In program control stove, and in device, it is filled with noble gas, after making paddle 9 stand 8 minutes at 1049 DEG C, and device is risen
Temperature, makes paddle 9 stand 34 minutes at 1400 DEG C, and the paddle 9 after standing puts into the drying unit of 120 DEG C after taking out
Dry, can be prepared by.
Conch meal described in step 3) and a diameter of 32 μm of bone powder in the processing technique of described coating.
In the processing technique of described coating, the expulsion pressure of high-pressure injection device described in step 5) is 0.45MPa.
In the processing technique of described coating, the noble gas described in step 8) is argon.
The performance test results of table 1 paddle
Above-described embodiment is only the preferred technical solution of the present invention, and is not construed as the restriction for the present invention, the guarantor of the present invention
The technical scheme that the scope of protecting should be recorded with claim, replaces including the equivalent of technical characteristic in the technical scheme that claim is recorded
The scheme of changing is protection domain, and equivalent the most in this range is improved, also within protection scope of the present invention.
Claims (10)
1. a biological fermentation tank, it is characterised in that: include motor, reductor, agitating device, upper cover, fermenter and support,
Described fermenter lower end is provided with support, and described fermenter upper end is provided with upper cover, described on cover and be provided with stirring port, described stirring fills
Putting and be arranged in stirring port, described motor via reducer is connected with agitating device, described agitating device include shaft and
The paddle being arranged on shaft, described paddle includes the first paddle and the second paddle, described second paddle
Being arranged on the lower end of shaft, described first paddle is flood dragon rotating vane, and described second paddle is frame type stirring leaf, institute
Stating and be provided with coating outside paddle, described fermenter is from inside to outside sequentially provided with inner barrel, external jacket and shell, described outer clip
It is provided with attemperator between set and shell, is provided with heater between described inner barrel and external jacket, sets in described attemperator
There is sensor；Covering on described and be provided with charging aperture, described fermenter lower end is provided with drain hole.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that: one end of described flood dragon rotating vane with send out
Ferment bucket inwall contacts, and the shape of described frame type stirring leaf is identical with the shape bottom fermenter.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that: described fermenter upper end is provided with condensation dress
Putting, described condensing unit includes condensation pipe, water inlet and outlet, and described water inlet passes through condensation pipe and outlet phase
Even, described condensation pipe is U-shaped condensation pipe.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that: described attemperator includes being arranged on two ends
Warming plate and the heat-preservation cotton that is arranged between warming plate.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that: described heater includes that conduction oil feeds
Mouth, heat conducting oil pipe, conduction oil discharge gate and heating rod, described conduction oil charging aperture is arranged on the upper end of heat conducting oil pipe,
Described conduction oil discharge gate is arranged on heat conducting oil pipe lower end, and described heating rod is arranged on heat conducting oil pipe lower end.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that: the thickness of described coating is 0.9-1.5mm.
A kind of biological fermentation tank the most according to claim 1, it is characterised in that the processing technique of described coating is as follows: 1)
After the metal surface of paddle is first carried out 5-6 minute with acetone, paddle is put into clear water, acetone and anhydrous second
In the mixture of alcohol, and paddle is carried out supersound process 14-18 minute, then paddle is put into distilled water solution stirring
Mix leaf and be carried out 6-8 minute；The weight ratio of described clear water, acetone and dehydrated alcohol is 3:5:3；
2) polyethylene 38-46 part will add 40-50 part deionized water and be constantly stirred, and add during stirring
Stir 20-30 minute after cross-linking agent 5-9 part；
3) conch meal 5-7 part, bone powder 6-8 part are put into and carried out after being stirred 10-13 minute under the ethanol solution of 42%
Filter, the mixture after filtering puts in the high-pressure separator of 0.5-0.8MPa and is centrifuged machine separating and dehydrating, mixed after dehydration
Compound puts into the drying unit of 45-52 DEG C dries, and the mixture after drying is put in grinder and is ground, and
Mixture after grinding adds dehydrated alcohol 6-8 part, distilled water 5-9 part, hydroxy silicon oil 5-8 part and through step 2) anti-
Mixture after should is stirred；
4) copper powder 42-50 part, nikel powder 18-20 part, zinc powder 30-40 part are ground by grinder, the mixing after grinding
Thing adds through the reacted product of step 3), and addition dispersant 9-14 part, oleic acid 6-9 part are gone forward side by side at 20-35 DEG C
Row stirring reaction 20-28 minute, then in mixture, add dehydrated alcohol 3-5 part, distilled water 10-15 part, and make mixture exist
After being stirred reaction at 45-52 DEG C 12-15 minute, in mixed solution, add polyester resin 10-14 part and be stirred 5-8
After minute, mixed liquor is heated, and make mixed liquor carry out reaction 5-6 minute at 70-75 DEG C；
5), after the mixture paint brush processed through step 4) being carried out primary coating, carry out being heated to 95-by mixture
100 DEG C, the mixture after heating is placed in high-pressure injection device and sprays paddle, is then cooled to by mixture
70-75 DEG C, and after paddle being carried out secondary coating by paint brush, paddle good for coating is stood at 20-25 DEG C 5-7
After minute, then the paddle that coating is good is put into carry out to the drying unit of 120 DEG C dry 40-45 minute；
6) silver peroxide 1.5-2 part, zinc peroxide 3-4 part are put into after lapping device is ground, and by ground
Mixture is put in agitating device, and adds polyester resin 11-14 part, deionized water 3-5 part in agitating device, and makes mixing
Thing is stirred 15-20 minute at 51-54 DEG C；
7) Chlorizate chromium 1-3 part, silver peroxide 0.9-1.2 part, zinc peroxide 0.2-0.8 part are put in grinder and is ground
After, mixture is heated to 90-100 DEG C, and the mixture after heating is put into and is stirred mixing to the oleum lini of 15-20 DEG C
Close；
8), after carrying out the paddle after step 5) coating at 15-18 DEG C standing 20-25 minute, paddle is put into rotation
Rotary device rotates, will be after the reacted mixture of step 6) be heated to 105-110 DEG C, the mixed liquor after heating falls
Enter in high-pressure injection device, and the paddle in rotating is sprayed, the paddle after injection is put into the drying dress of 120 DEG C
Dry in putting, after paddle after drying takes out, will at after step 7) is reacted, mixture is heated to 84-86 DEG C, and
Mixed liquor after heating is poured in high-pressure injection device, and the paddle in rotating is sprayed, paddle after spraying
It is arranged in program control stove, and in device, is filled with noble gas, after making paddle stand 5-8 minute at 1025-1100 DEG C, and
Heating up device, make paddle stand 30-36 minute at 1300-1500 DEG C, the paddle after standing is put after taking out
Dry in entering the drying unit of 120 DEG C, can be prepared by.
A kind of biological fermentation tank the most according to claim 7, it is characterised in that: step 3) in the processing technique of described coating
Described conch meal and bone powder a diameter of 32-44 μm.
A kind of biological fermentation tank the most according to claim 7, it is characterised in that: step 5) in the processing technique of described coating
The expulsion pressure of described high-pressure injection device is 0.4-0.45MPa.
A kind of biological fermentation tank the most according to claim 7, it is characterised in that: step in the processing technique of described coating
8) noble gas described in is argon.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281979A (en) * | 2016-08-31 | 2017-01-04 | 江苏绿扬生物电子工程有限公司 | High-efficiency vertical fermentation tank |
| CN106282005A (en) * | 2016-08-31 | 2017-01-04 | 江苏绿扬生物电子工程有限公司 | Vertical digester |
| CN106367339A (en) * | 2016-08-31 | 2017-02-01 | 江苏绿扬生物电子工程有限公司 | Fermentation tank |
| CN106635788A (en) * | 2017-01-04 | 2017-05-10 | 上海应用技术大学 | Coaxial different-speed combined paddle reactor |
| CN108559695A (en) * | 2018-04-10 | 2018-09-21 | 江西东旺动物微生物有限公司 | A kind of fermentation system convenient for feeding |
| CN109181934A (en) * | 2018-09-30 | 2019-01-11 | 广西秀美壮乡能源环保有限公司 | A kind of Brewing equipment of fen-flavor type white spirit |
| CN109568612A (en) * | 2018-12-06 | 2019-04-05 | 肇庆市天臻生物化工技术有限公司 | Amyloid fermentation medium continuous sterilization system and method |
| CN115305192A (en) * | 2022-10-12 | 2022-11-08 | 江苏岭南重工股份有限公司 | Multifunctional fermentation tank and processing technology thereof |
| CN118086036A (en) * | 2024-04-19 | 2024-05-28 | 江苏弗洛瑞生物工程设备有限公司 | Stable defoaming's multicavity room microorganism fermentation cylinder |
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| CN203569077U (en) * | 2013-09-29 | 2014-04-30 | 哈尔滨学院 | Fermentation tank |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106281979A (en) * | 2016-08-31 | 2017-01-04 | 江苏绿扬生物电子工程有限公司 | High-efficiency vertical fermentation tank |
| CN106282005A (en) * | 2016-08-31 | 2017-01-04 | 江苏绿扬生物电子工程有限公司 | Vertical digester |
| CN106367339A (en) * | 2016-08-31 | 2017-02-01 | 江苏绿扬生物电子工程有限公司 | Fermentation tank |
| CN106367339B (en) * | 2016-08-31 | 2019-08-16 | 江苏绿扬生物电子工程有限公司 | Fermentor |
| CN106635788A (en) * | 2017-01-04 | 2017-05-10 | 上海应用技术大学 | Coaxial different-speed combined paddle reactor |
| CN108559695A (en) * | 2018-04-10 | 2018-09-21 | 江西东旺动物微生物有限公司 | A kind of fermentation system convenient for feeding |
| CN109181934A (en) * | 2018-09-30 | 2019-01-11 | 广西秀美壮乡能源环保有限公司 | A kind of Brewing equipment of fen-flavor type white spirit |
| CN109568612A (en) * | 2018-12-06 | 2019-04-05 | 肇庆市天臻生物化工技术有限公司 | Amyloid fermentation medium continuous sterilization system and method |
| CN115305192A (en) * | 2022-10-12 | 2022-11-08 | 江苏岭南重工股份有限公司 | Multifunctional fermentation tank and processing technology thereof |
| CN118086036A (en) * | 2024-04-19 | 2024-05-28 | 江苏弗洛瑞生物工程设备有限公司 | Stable defoaming's multicavity room microorganism fermentation cylinder |
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| CN105886388B (en) | 2018-06-05 |
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