CN209034344U - A kind of acidification reaction device of rice husk silica - Google Patents

A kind of acidification reaction device of rice husk silica Download PDF

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Publication number
CN209034344U
CN209034344U CN201821658970.0U CN201821658970U CN209034344U CN 209034344 U CN209034344 U CN 209034344U CN 201821658970 U CN201821658970 U CN 201821658970U CN 209034344 U CN209034344 U CN 209034344U
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CN
China
Prior art keywords
cover board
rice husk
tank body
agitating paddle
blade
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201821658970.0U
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Chinese (zh)
Inventor
林然
梁伟柱
郑雪辉
曾翠银
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Guangzhou Tianhe Foreign Language School
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Guangzhou Tianhe Foreign Language School
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Priority to CN201821658970.0U priority Critical patent/CN209034344U/en
Application granted granted Critical
Publication of CN209034344U publication Critical patent/CN209034344U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of acidification reaction devices of rice husk silica, for rice husk acidification reaction, it discloses the top that the feeding port, acid inlet tube, stirring motor, reflux cooling tube are provided with reacting tank body, stirring motor is located at the middle at the top of reacting tank body, and shaft extends into reacting tank body;It is disposed with cover board, blade, blade, steam heating pipe from top to bottom in reacting tank body;It is covered with hole on cover board, reacting tank body inner wall is close at the edge of cover board, the centre of cover board is provided with the hole that agitating paddle passes perpendicularly through;The agitating paddle is connected with the shaft of stirring motor, and the other end passes through cover board, steam heating pipe extends to reacting tank body bottom, and blade is mounted on the two sides of agitating paddle, is covered with hole on blade.The utility model has the advantages that rice husk can be made to be fully immersed in acid solution during the reaction, it is ensured that rice husk and acid solution come into full contact with, do not need to increase additional stirring power, can greatly improve the efficiency of acidification reaction.

Description

A kind of acidification reaction device of rice husk silica
Technical field
The utility model relates to a kind of acidification reaction devices more particularly to a kind of use rice husk to prepare used in silica Acidification reaction device.
Background technique
Rice husk is a kind of renewable resource, silica containing about 20%, with the presence of hydrated amorphous state;China is water Seed rice plants big country, annual output occupies first place in the world, and paddy annual output accounts for about the 1/3 of global rice yield at 200,000,000 tons or more, produces per year 40,000,000 tons of rice husk or more.These rice husks have largely been burned off or have lost as waste for a long time, not only waste money Source also polluted environment.Silica is a kind of important inorganic powder material, coating, rubber, plastics, food, drug, It is all widely used in the products such as toothpaste.Silica is prepared from rice husk, not only increases the added value of rice husk, same to time-varying Waste be changed into values, has saved resource, also protects environment, meets Development of Green Industrialization direction.
Rice husk, which prepares silica, can be used the technique for first carrying out acidification reaction, carrying out high-temperature calcination again;Wherein acidification is anti- Answer the qualitative effects such as whiteness very crucial, to silica very big, can be removed by acidification reaction iron in rice husk, Calcium, sodium, potassium, manganese and other impurities, to improve silica product whiteness.Acidification reaction process due to rice husk is relatively light, It is readily suspended in above acid solution, leads to that substantial portion of rice husk contact acid solution is insufficient, reaction is not thorough, to influence titanium dioxide The quality of silicon product.In order to enable rice husk sufficiently to react with acid solution, generallys use and increase the methods such as mixing speed, but this side Method will often consume a large amount of power and energy, and cannot ensure that whole rice husks and acid solution come into full contact with simultaneously effecting reaction.
Utility model content
The utility model provides the acidification reaction device that a kind of rice husk prepares silica, can make rice husk during the reaction It is fully immersed in acid solution, it is ensured that rice husk and acid solution come into full contact with, do not need to increase additional stirring power, can greatly improve acid Change the efficiency of reaction.
The technical solution of the utility model is in reacting tank body 1, and feeding port 12, outlet valve 13, acid inlet tube 14 stir On the basis of mixing motor 10, feature is that have reflux cooling tube 11, cover board 21, agitating paddle 31, steam heating pipe 41, and described feeds intake Mouth 12, acid inlet tube 14, stirring motor 10, reflux cooling tube 11 are provided with the top of reacting tank body, and stirring motor 10 is located at reaction The middle at the top of tank body, shaft extend into reacting tank body 1;It is disposed with cover board from top to bottom in reacting tank body 1 21, blade 310, blade 310, steam heating pipe 41;Equispaced it is covered with hole on cover board 21, reaction is close at the edge of cover board 21 1 inner wall of tank body, cover board 21 centre be provided with the hole that agitating paddle 31 passes perpendicularly through;One end of the agitating paddle 31 and stirring electricity The shaft of machine 10 is connected, and the other end passes through cover board 21, steam heating pipe 41 extends to 1 bottom of reacting tank body, agitating paddle 31 It is covered with hole on tube body, blade 310 is mounted on the two sides of agitating paddle 31, and can rotate with agitating paddle 31, average on blade 310 Compartment of terrain is covered with hole.
Cover board 21 described above is the cover board 21 that a complete disc is merged by the plate of two panels semi circular surface shape, is covered with and is covering Hole on plate 21 is less than rice husk particle, and the hole among the cover board is connected by bearing with agitating paddle 31, two panels cover board 21 Medial surface respectively with bearing hinge connection, the cover board of semi circular surface can downward swing open, facilitate to tank body and launch rice husk, two panels cover board 21 Side be both provided with hook 210, launch rice husk after, can pull-up hook 210 be buckled in inner tank wall.
The blade 310 that each layer of agitating paddle 31 described in the utility model is transversely mounted is no less than two panels, longitudinal blade 310 The number of plies is no less than two layers, is covered with hole on blade 310 and is greater than rice husk particle, and when stirring allows rice husk particle to pass through.
The working principle of the utility model is due to being equipped with cover board inside reacting tank body, which only allows acid solution logical It crosses, rice husk particle is not allowed to pass through, cause rice husk particle that cannot be suspended on acid solution face, it is ensured that rice husk is complete in reaction process It is immersed in inside acid solution;Furthermore by installing blade on agitating paddle, rice husk particle can be made to pass through, reduce whipping process Resistance improves the uniformity of stirring;In short, improving acidification efficiency on the whole by installation cover board and the agitating paddle of blade And effect.
Operating procedure is as follows: first closing valve, opens feeding port, removes cover board hook, through feeding port in reacting tank body Rice husk is launched, is fed intake and is finished pull-up and hang up properly cover board hook;Then by acid inlet tube be added needed for acid, institute into acid measure to soak No cover board, charging finishes closing feeding port;Then starting stirring motor drives agitating paddle to be stirred, then opens steam heating Pipe, steam enter reactor tank and heat to system;The vapor and acid evaporated in reaction process can pass through the cooling tube that flows back Reactor tank is flow back into after condensing;End of reaction opens outlet valve discharging.
The utility model has the advantages that rice husk can be made to be fully immersed in acid solution during the reaction, it is ensured that rice husk and acid solution It comes into full contact with, need to increase additional stirring power, the efficiency of acidification reaction can be greatly improved.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the schematic perspective view of the utility model.
Specific embodiment
Specific embodiment of the present utility model is described in detail below in conjunction with attached drawing.It should be understood that herein Described specific embodiment is only used for describing and explaining the present invention, and is not intended to limit the utility model.
According to 1, Fig. 2, the utility model is in reacting tank body 1, feeding port 12, outlet valve 13, acid inlet tube 14, stirring electricity On the basis of machine 10, feature is that have reflux cooling tube 11, cover board 21, agitating paddle 31, steam heating pipe 41, the feeding port 12, acid inlet tube 14, stirring motor 10, reflux cooling tube 11 are provided with the top of reacting tank body, and stirring motor 10 is located at reactor tank The middle at the top of body, shaft extend into reacting tank body 1;Be disposed with from top to bottom in reacting tank body 1 cover board 21, Blade 310, blade 310, steam heating pipe 41;Equispaced it is covered with hole on cover board 21, reactor tank is close at the edge of cover board 21 1 inner wall of body, cover board 21 centre be provided with the hole that agitating paddle 31 passes perpendicularly through;One end of the agitating paddle 31 and stirring motor 10 shaft is connected, and the other end passes through cover board 21, steam heating pipe 41 extends to 1 bottom of reacting tank body, the pipe of agitating paddle 31 It is covered with hole on body, blade 310 is mounted on the two sides of agitating paddle 31, and can rotate with agitating paddle 31, between average on blade 310 It is covered with hole every ground.The cover board 21 is the cover board 21 that a complete disc is merged by the plate of two panels semi circular surface shape, is covered with and is covering Hole on plate 21 is less than rice husk particle, its aperture ratio rice husk particle of cover board 21 is small, only allow acid solution by, rice husk particle not It can pass through.Hole among the cover board is connected by bearing with agitating paddle 31, the medial surface of two panels cover board 21 respectively with bearing Hingedly, the downward swing open of cover board energy of semi circular surface, facilitates to tank body and launches rice husk, the side of two panels cover board 21 is both provided with extension After hook 210, dispensing rice husk, energy pull-up hook 210 is buckled in inner tank wall.
The blade 310 that each layer of agitating paddle 31 described in the utility model is transversely mounted is two panels, longitudinal 310 number of plies of blade It is two layers, is covered with hole on blade 310 and is greater than rice husk particle, when stirring allows rice husk particle to pass through.
In the present embodiment, the blade 310 of agitating paddle 31 is distributed in the two sides of mixing paddle axle, and about 31 agitating paddle is respectively equipped with two To blade 310;Its aperture ratio rice husk particle of blade 310 is big, allows rice husk particle to pass through when stirring, reduces whipping process Resistance, the uniformity for improving stirring.
Without departing from the thought that the utility model is created, any group is carried out to the various different embodiments of the utility model It closes, content disclosed by the utility model should all be considered as;In the range of the technology design of the utility model, technical solution is carried out Any combination for the thought created without prejudice to the utility model that a variety of simple modifications and different embodiments carry out, should all be at this Within the protection scope of utility model.

Claims (3)

1. a kind of acidification reaction device of rice husk silica, it includes reacting tank body, and feeding port, outlet valve, acid inlet tube stir Motor is mixed, it is characterized in that have reflux cooling tube, cover board, agitating paddle, steam heating pipe, the feeding port, acid inlet tube, stirring electricity Machine, reflux cooling tube are provided with the top of reacting tank body, and stirring motor is located at the middle at the top of reacting tank body, and shaft is to anti- It answers in tank body and extends;It is disposed with cover board, blade, steam heating pipe from top to bottom in reacting tank body;Between being averaged on cover board Every ground is covered with hole, reacting tank body inner wall is close at the edge of cover board, the centre of cover board is provided with the hole that agitating paddle passes perpendicularly through;It is described One end of agitating paddle is connected with the shaft of stirring motor, and the other end passes through cover board, steam heating pipe prolongs to reacting tank body bottom It stretches, hole is covered on the tube body of agitating paddle, blade is mounted on the two sides of agitating paddle, and can rotate with agitating paddle, average on blade Compartment of terrain is covered with hole.
2. the acidification reaction device of a kind of rice husk silica according to claim 1, it is characterized in that the cover board is The cover board of a complete disc is merged by the plate of two panels semi circular surface shape, the hole being covered on the cover board is less than rice husk particle, described Hole among cover board is connected by bearing with agitating paddle, the medial surface of two panels cover board respectively with bearing hinge connection, the lid of semi circular surface The downward swing open of plate energy facilitates to tank body and launches rice husk, and the side of two panels cover board is both provided with hook, dispensing rice husk finishes Afterwards, energy pull-up hook is buckled in inner tank wall.
3. the acidification reaction device of a kind of rice husk silica according to claim 1, it is characterized in that every in agitating paddle One layer of blade being transversely mounted is no less than two panels, and longitudinal blade number of plies is no less than two layers, and the hole being covered on blade is greater than rice husk Particle allows rice husk particle to pass through when stirring.
CN201821658970.0U 2018-10-12 2018-10-12 A kind of acidification reaction device of rice husk silica Expired - Fee Related CN209034344U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201821658970.0U CN209034344U (en) 2018-10-12 2018-10-12 A kind of acidification reaction device of rice husk silica

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201821658970.0U CN209034344U (en) 2018-10-12 2018-10-12 A kind of acidification reaction device of rice husk silica

Publications (1)

Publication Number Publication Date
CN209034344U true CN209034344U (en) 2019-06-28

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CN201821658970.0U Expired - Fee Related CN209034344U (en) 2018-10-12 2018-10-12 A kind of acidification reaction device of rice husk silica

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109200980A (en) * 2018-10-12 2019-01-15 广州市天河外国语学校 A kind of acidification reaction device of rice husk silica

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109200980A (en) * 2018-10-12 2019-01-15 广州市天河外国语学校 A kind of acidification reaction device of rice husk silica

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GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20190628

Termination date: 20201012