CN105869711A - Insulating layer material of iron disk electric heating element and preparation method of insulating layer material - Google Patents
Insulating layer material of iron disk electric heating element and preparation method of insulating layer material Download PDFInfo
- Publication number
- CN105869711A CN105869711A CN201610438850.9A CN201610438850A CN105869711A CN 105869711 A CN105869711 A CN 105869711A CN 201610438850 A CN201610438850 A CN 201610438850A CN 105869711 A CN105869711 A CN 105869711A
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- China
- Prior art keywords
- insulating layer
- layer material
- iron pan
- class heating
- pan class
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/10—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances metallic oxides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/126—Preparation of silica of undetermined type
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/181—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
- C01B33/183—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N10/00—Thermoelectric devices comprising a junction of dissimilar materials, i.e. devices exhibiting Seebeck or Peltier effects
- H10N10/80—Constructional details
Abstract
The invention provides an insulating layer material of an iron disk electric heating element and a preparation method of the insulating layer material. The insulating layer material of the iron disk electric heating element is prepared from the following ingredients in parts by weight: 60-80 parts of highest crystallizing fused magnesia, 5 parts of calcined kaolin, 0.4-1 part of aluminium oxide fine power, 0.2-0.5 part of methyl silicone resin, and 5-10 parts of amorphous SiO2 fine power. The insulating layer material of the iron disk electric heating element is scientific and reasonable in formula, has favorable plasticity, dampproof insulativity and crack resistance, and can be widely applied to electric heating elements such as electric heating iron disks.
Description
Technical field
The present invention relates to material technology, particularly relate to insulating layer material and the system thereof of a kind of iron pan class heating
Preparation Method.
Background technology
Fused magnesium oxide is a kind of topmost insulation high-temperature-resistant packing material, and it has superior insulating properties
Can be widely used in various electrical heating elements with high-termal conductivity.But have a disadvantage in that electrician's level aoxidizes
The plasticity of magnesium own is poor, needs kalamein parts when generally using, after bigger undergauge, and just meeting
Possesses certain hardness.When being applied to iron pan class heating, after oil pressure molding, its hardness is undesirable,
Easily cracking, poor plasticity, constrain fused magnesium oxide application in this series products significantly.
Summary of the invention
It is an object of the invention to, apply at iron pan class heating for above-mentioned existing fused magnesium oxide
Time, after oil pressure molding, its hardness is undesirable, easy to crack, the problem of poor plasticity, proposes a kind of iron pan
The insulating layer material of class heating, this material prescription science, rationally, there is excellent physicochemical property,
Can be as the insulant needing oil pressure to shape, as wrapped up the insulant of heating wire in electric heating iron pan groove.
For achieving the above object, the technical solution used in the present invention is: a kind of iron pan class heating exhausted
Edge layer material (is called for short: iron pan powder), including each component that weight proportion is following:
Further, the insulating layer material of described iron pan class heating, including following each of weight proportion
Component:
Further, described calcined kaolin, is a kind of nonmetallic minerals, is a kind of viscous with kaolinite race
Soil mineral are main clay and clay rock.Because of white and fine and smooth, also known as white clouds soil.
Further, described aluminium oxide is micron order aluminium oxide, possesses excellent dispersibility, excellent suction
Attached property.
Further, described methyl silicon resin is a kind of methyl silicon resin being dissolved in toluene.Methyl silicon
SiO in resin2Content is the highest (about contains the SiO of 80%wt after complete oxidation2, contain according to hard resin
Amount calculates [DSC]) it is the perfect binding agent for 300 DEG C of environment above, and there is good electric draw last breath
Edge performance.
Further, described amorphous Si O2Powder particle size is less than 250-325 mesh, be a kind of high-performance,
Volume stable anti-cracking agent.Amorphous Si O of the present invention2After fine powder mixes according to proportioning, have the most micro-
Expand, high effect leakage proof, high-durability, high cracking resistance..
Another object of the present invention also discloses the preparation of the insulating layer material of a kind of iron pan class heating
Method, comprises the following steps: after weighing each component according to weight proportion, and blender mix homogeneously obtains ferrum
The insulating layer material of dish class heating.
Further, described amorphous Si O2The preparation of fine powder comprises the following steps: with Silicon chloride., hydrogen
Gas, air (with oxymeter) are as raw material, and wherein Silicon chloride., hydrogen, the amount ratio of air can use often
Rule ratio, by Silicon chloride., hydrogen, air mixing, and with 0.3-0.5m3The ratio of/Kg puts into water
Solving the reaction that is hydrolyzed in stove, reaction temperature is 900-1100 DEG C, and reaction generates silicon dioxide primary particle;
The aggregated device of this reactant is gathered into state of aggregation particle, through cyclonic separation, two-stage air injection deacidification, boiling
Rise bed screening and obtain amorphous Si O2Fine powder.
Another object of the present invention additionally provides a kind of iron pan class heating, by above-mentioned iron pan class electric heating
The insulating layer material of element is wrapped up in heating wire oil pressure and is shaped or by the insulating barrier material of above-mentioned iron pan class heating
Expect that direct oil pressure, in metallic channel, is dried at 200~400 DEG C after molding and obtains iron pan class in 2~4 hours
Heating.
Further, described oil pressure pressure is 300-600kg/cm2。
The insulating layer material scientific formulation of iron pan class heating of the present invention, rationally, its preparation method is simple,
Easy, have the advantage that compared with prior art
The present invention is with high activity amorphous Si O2Fine powder is raw material, improves fused magnesium oxide powder plasticity
Performance so that it is possess higher room temperature hardness, excellent line degeneration energy.Have more excellent after its molding
High-temperature insulation performance, excellent damp proof insulation performance, excellent anti-crack performance, can be widely used in
In the heating of electric heating iron pan class.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further described:
Embodiment 1
Present embodiment discloses the insulating layer material of a kind of iron pan class heating, as follows including weight proportion
Each component:
Described aluminium oxide is micron order aluminium oxide, possesses excellent dispersibility, excellent adsorptivity.Described
Methyl silicon resin is a kind of methyl silicon resin being dissolved in toluene.SiO in methyl silicon resin2Content is the highest
(after complete oxidation, about contain the SiO of 80%wt2, calculating [DSC] according to solid resin content) and it is to use
In the perfect binding agent of 300 DEG C of environment above, and there are superior electrical insulating properties.Described amorphous
SiO2Powder particle size is less than 250 mesh, is a kind of high-performance, volume stable anti-cracking agent.Nothing in the present embodiment
Setting SiO2After fine powder mixes according to proportioning, grinding forms, and is that one has efficient microdilatancy, Effective Anti
Ooze, high-durability, high cracking resistance
The preparation method of the insulating layer material of iron pan class heating, comprises the following steps: join according to weight
After weighing each component, mix homogeneously obtains the insulating layer material of iron pan class heating.The most amorphous
SiO2The preparation of fine powder comprises the following steps: with Silicon chloride., hydrogen, air (with oxymeter) as raw material,
By Silicon chloride., hydrogen, air mixing, and with 0.3-0.5m3The ratio of/Kg is put in hydrolysis stove
Row hydrolysis, this input process is uninterrupted continuously, and reaction temperature is 900-1100 DEG C, reacts generation two
Silicon oxide primary particle;The aggregated device of this reactant is gathered into state of aggregation particle, through cyclonic separation, twin-stage
Air injection deacidification, ebullated bed screening obtain amorphous Si O2Fine powder.
The performance parameter of the insulating layer material of the present embodiment iron pan class heating is as follows after testing:
Bulk density: 2.8-2.9g/cm3
Compressive resistance (800 DEG C of Χ 3h): >=60Mpa
Mar proof :≤6cc
Line change after burning: (800 DEG C of Χ 3h) :≤1%.
Electrical insulation properties :≤0.5mA
High-Voltage Insulation: 1500V/1mA.s
The insulating layer material using iron pan class heating of the present invention prepares iron pan class heating, by iron pan
The direct oil pressure of insulating layer material of class heating in metallic channel, oil pressure pressure: 300kg/cm2Heat treatment
Dry temperature: be dried at 450 DEG C and prepare iron pan powder in 3 hours.
Embodiment 2
Present embodiment discloses the insulating layer material of a kind of iron pan class heating, as follows including weight proportion
Each component:
Described aluminium oxide is micron order aluminium oxide, possesses excellent dispersibility, excellent adsorptivity.Described
Methyl silicon resin is a kind of methyl silicon resin being dissolved in toluene.SiO in methyl silicon resin2Content is the highest
(after complete oxidation, about contain the SiO of 80%wt2, calculating [DSC] according to solid resin content) and it is to use
In the perfect binding agent of 300 DEG C of environment above, and there are superior electrical insulating properties.Described amorphous
SiO2Powder particle size is less than 250 mesh, is a kind of high-performance, volume stable anti-cracking agent.Nothing in the present embodiment
Setting SiO2After fine powder mixes according to proportioning, grinding forms, and is that one has efficient microdilatancy, Effective Anti
Ooze, high-durability, high cracking resistance.
The preparation method of the insulating layer material of iron pan class heating, comprises the following steps: join according to weight
After weighing each component, mix homogeneously obtains the insulating layer material of iron pan class heating.The most amorphous
SiO2The preparation of fine powder comprises the following steps: with Silicon chloride., hydrogen, air (with oxymeter) as raw material,
By Silicon chloride., hydrogen, air mixing, and with 0.3-0.5m3The ratio of/Kg is put in hydrolysis stove
Row hydrolysis, reaction temperature is 900-1100 DEG C, and reaction generates silicon dioxide primary particle;This reaction
The aggregated device of thing is gathered into state of aggregation particle, through cyclonic separation, two-stage air injection deacidification, ebullated bed sieve
Choosing obtains amorphous Si O2Fine powder.
The performance parameter of the insulating layer material of the present embodiment iron pan class heating is as follows after testing:
Bulk density: 2.32-2.34g/cm3
Compressive resistance (800 DEG C of Χ 3h): >=40Mpa
Mar proof :≤5cc
Line change after burning: (800 DEG C of Χ 3h) :≤0.5%.
Electrical insulation properties :≤0.5mA
High-Voltage Insulation: 1500V/1mA.s
The insulating layer material using iron pan class heating of the present invention prepares iron pan class heating, by iron pan
The direct oil pressure of insulating layer material of class heating in metallic channel, oil pressure pressure: 600kg/cm2Heat treatment
Dry temperature: be dried at 270 DEG C and prepare iron pan powder in 15 hours.
Embodiment 3
Present embodiment discloses the insulating layer material of a kind of iron pan class heating, as follows including weight proportion
Each component:
Described aluminium oxide is micron order aluminium oxide, possesses excellent dispersibility, excellent adsorptivity.Described
Methyl silicon resin is a kind of methyl silicon resin being dissolved in toluene.SiO in methyl silicon resin2Content is the highest
(after complete oxidation, about contain the SiO of 80%wt2, calculating [DSC] according to solid resin content) and it is to use
In the perfect binding agent of 300 DEG C of environment above, and there are superior electrical insulating properties.Described amorphous
SiO2Powder particle size is less than 250 mesh, is a kind of high-performance, volume stable anti-cracking agent.Nothing in the present embodiment
Setting SiO2After fine powder mixes according to proportioning, grinding forms, and is that one has efficient microdilatancy, Effective Anti
Ooze, high-durability, high cracking resistance.
The preparation method of the insulating layer material of iron pan class heating, comprises the following steps: join according to weight
After weighing each component, mix homogeneously obtains the insulating layer material of iron pan class heating.The most amorphous
SiO2The preparation of fine powder comprises the following steps: with Silicon chloride., hydrogen, air (with oxymeter) as raw material,
By Silicon chloride., hydrogen, air mixing, and with 0.3-0.5m3The ratio of/Kg puts into hydrolysis continuously
Be hydrolyzed in stove reaction, and reaction temperature is 900-1100 DEG C, and reaction generates silicon dioxide primary particle;
The aggregated device of this reactant is gathered into state of aggregation particle, through cyclonic separation, two-stage air injection deacidification, boiling
Rise bed screening and obtain amorphous Si O2Fine powder.
The performance parameter of the insulating layer material of the present embodiment iron pan class heating is as follows after testing:
Bulk density: 2.30-2.32g/cm3
Compressive resistance (800 DEG C of Χ 3h): >=50Mpa
Mar proof :≤6cc
Line change after burning: (800 DEG C of Χ 3h) :≤0.8%.
Electrical insulation properties :≤0.5mA
High-Voltage Insulation: 1500V/1mA.s
The insulating layer material using iron pan class heating of the present invention prepares iron pan class heating, by iron pan
The direct oil pressure of insulating layer material of class heating in metallic channel, oil pressure pressure: 500kg/cm2Heat treatment
Dry temperature: be dried at 320 DEG C and prepare iron pan powder in 8 hours.
Last it is noted that various embodiments above is only in order to illustrate technical scheme, rather than to it
Limit;Although the present invention being described in detail with reference to foregoing embodiments, the ordinary skill of this area
Personnel it is understood that the technical scheme described in foregoing embodiments still can be modified by it, or
The most some or all of technical characteristic is carried out equivalent;And these amendments or replacement, do not make phase
The essence answering technical scheme departs from the scope of various embodiments of the present invention technical scheme.
Claims (9)
1. the insulating layer material of an iron pan class heating, it is characterised in that include that weight proportion is as follows
Each component:
The insulating layer material of iron pan class heating the most according to claim 1, it is characterised in that bag
Include each component that weight proportion is following:
The insulating layer material of iron pan class heating the most according to claim 1 or claim 2, it is characterised in that
Described aluminium oxide is micron order aluminium oxide.
The insulating layer material of iron pan class heating the most according to claim 1 or claim 2, it is characterised in that
Described methyl silicon resin is a kind of methyl silicon resin being dissolved in toluene.
The insulating layer material of iron pan class heating the most according to claim 1 or claim 2, it is characterised in that
Described amorphous Si O2Powder particle size is less than 250-325 mesh.
6. the preparation of the insulating layer material of iron pan class heating described in a claim 1-5 any one
Method, it is characterised in that comprise the following steps: after weighing each component according to weight proportion, blender mixes
Close the insulating layer material uniformly obtaining iron pan class heating.
The most according to claim 6, the preparation method of the insulating layer material of iron pan class heating, it is special
Levy and be, described amorphous Si O2The preparation of fine powder comprises the following steps: by Silicon chloride., hydrogen, sky
Gas mixes, and with 0.3-0.5m3The ratio of/Kg puts into the reaction that is hydrolyzed in hydrolysis stove, reaction temperature
For 900-1100 DEG C, reaction generates silicon dioxide primary particle;The aggregated device of this reactant is gathered into gathering
State particle, obtains amorphous Si O through cyclonic separation, two-stage air injection deacidification, ebullated bed screening2Fine powder.
8. an iron pan class heating, it is characterised in that by ferrum described in claim 1-5 any one
The insulating layer material of dish class heating is wrapped up in heating wire oil pressure and is shaped or by claim 1-6 any one
The direct oil pressure of insulating layer material of described iron pan class heating in metallic channel, after molding 200~
It is dried at 400 DEG C and within 2~4 hours, obtains iron pan class heating.
Iron pan class heating the most according to claim 8, it is characterised in that described oil pressure pressure is
300-600kg/cm2。
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110945965A (en) * | 2017-06-01 | 2020-03-31 | 金叡院 | Radiator with heating device |
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CN1208016A (en) * | 1998-08-27 | 1999-02-17 | 沈阳化工股份有限公司 | Gas phase process preparing white carbon |
CN1923750A (en) * | 2006-09-28 | 2007-03-07 | 庄伟� | Preparation method of high temperature resisting electrothermal insulating magnesia material |
US20080258270A1 (en) * | 2004-10-13 | 2008-10-23 | Commissariat A L'energie Atomique | Mgo-Based Coating for Electrically Insulating Semiconductive Substrates and Production Method Thereof |
CN102254652A (en) * | 2011-04-20 | 2011-11-23 | 荆巍 | Preparation method of magnesia heat-conducting insulating material for electric heating tube |
CN103971786A (en) * | 2013-12-27 | 2014-08-06 | 上海实业振泰化工有限公司 | Electric-grade organic coating high-temperature-resistant insulating magnesia powder for electric ovens and production method of electric-grade organic coating high-temperature-resistant insulating magnesia powder |
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2016
- 2016-06-17 CN CN201610438850.9A patent/CN105869711B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1208016A (en) * | 1998-08-27 | 1999-02-17 | 沈阳化工股份有限公司 | Gas phase process preparing white carbon |
US20080258270A1 (en) * | 2004-10-13 | 2008-10-23 | Commissariat A L'energie Atomique | Mgo-Based Coating for Electrically Insulating Semiconductive Substrates and Production Method Thereof |
CN1923750A (en) * | 2006-09-28 | 2007-03-07 | 庄伟� | Preparation method of high temperature resisting electrothermal insulating magnesia material |
CN102254652A (en) * | 2011-04-20 | 2011-11-23 | 荆巍 | Preparation method of magnesia heat-conducting insulating material for electric heating tube |
CN103971786A (en) * | 2013-12-27 | 2014-08-06 | 上海实业振泰化工有限公司 | Electric-grade organic coating high-temperature-resistant insulating magnesia powder for electric ovens and production method of electric-grade organic coating high-temperature-resistant insulating magnesia powder |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110945965A (en) * | 2017-06-01 | 2020-03-31 | 金叡院 | Radiator with heating device |
CN110945965B (en) * | 2017-06-01 | 2022-02-15 | 金叡院 | Radiator with heating device |
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Address after: 115000 huizhuang village, Yong'an Town, Dashiqiao City, Yingkou City, Liaoning Province Patentee after: Liaoning Jiashun Technology Co.,Ltd. Address before: 115109 huizhuang village, Yong'an Town, Dashiqiao City, Yingkou City, Liaoning Province Patentee before: LIAONING JIASHUN CHEMICAL SCIENCE AND TECHNOLOGY Co.,Ltd. |