CN105859265A - Tabular corundum-based refractory brick for gas producer - Google Patents
Tabular corundum-based refractory brick for gas producer Download PDFInfo
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- CN105859265A CN105859265A CN201610307376.6A CN201610307376A CN105859265A CN 105859265 A CN105859265 A CN 105859265A CN 201610307376 A CN201610307376 A CN 201610307376A CN 105859265 A CN105859265 A CN 105859265A
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- andalusite
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- diamond spar
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/101—Refractories from grain sized mixtures
- C04B35/105—Refractories from grain sized mixtures containing chromium oxide or chrome ore
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
- C04B2235/3222—Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
Abstract
The invention relates to the field of gas producers, in particular to a muscovite-based refractory brick for a gas producer, made with: 35-45% of tabular corundum, 15-25% of bauxite, 15-25% of clay, 10-20% of saw dust, 1-6% of silica powder, 1-6% of oxidized alumina powder, 1-5% of kyanite, 1-4% of andalusite, 0.5-2% of calcium aluminate, 1-5% of an additive, and 0.5-2% of a coagulant; a production method of the brick includes the following steps: (1), crushing; (2), mixing; (3), ageing; (4), sintering; (5), holding temperature; (6), forming; (7), curing. The refractory brick of the invention is simple to manufacture, controllable in cost and good in high temperature resistance; since a large quantity of tabular corundum is used herein and tabular corundum has inherent characteristics, the refractory brick of the invention is better in thermal shock stability and bending strength than traditional refractory bricks.
Description
Technical field
The present invention relates to gas generator field, a kind of gas generator refractory brick based on plate diamond spar.
Background technology
Gas generator is the production that coal is converted into imflammable gas coal gas (being mainly composed of CO, H2, CH4 etc.)
Equipment, part gas generator uses refractory brick to pile up and forms.Its operation principle is: sieved by the coal meeting gasifying process index
After choosing, firing machine join in gas stove, blast self-produced steam with air gas mixture as gasifying agent from furnace bottom.Coal exists
Through physics, chemical reaction in stove, generating imflammable gas, gas in upper segment is through cyclone oil remover, electric trapper filtered tar. hypomere
Coal gas, through cyclone dust extractor dust out, is transported to user after mixing and uses.
Refractory brick is called for short firebrick.The refractory material being fired into refractory clay or other refractory raw materials.Faint yellow or band brown.Energy
The high temperature of resistance to 1580 DEG C 1770 DEG C.Also firebrick it is.There is the refractory material of definite shape and size.By process of preparing
Division can be divided into burnt brick, unburned brick, fused cast refractories (molten-cast brick), refratory insulating brick；Standard type can be divided into by shape and size
Brick, common brick, special shaped brick etc..Can be used as building kiln and the high temperature construction material of various Thermal Equipment and structural material, and
At high temperature it is amenable to various physicochemical change and mechanism.Such as chamotte brick, high-alumina brick, silica brick, magnesia brick etc..
Plate diamond spar be a kind of pure, burn till shrink alundum thoroughly without additive as any in MgO, B2O3 etc.,
Having crystallization α-al2o3crystal structure thick, well-developed, the content of Al2O3 is more than 99%.En plaque crystal structure,
Pore is little and holds one's breath that hole is more and the porosity is about the same with electro-corundum, and purity is high, and volume stability is good, and minimum reheating is received
Contracting, in order to have good thermal shock resistance and bending strength after the resistance to material produced or castable high-temperature process.
Summary of the invention
For the problems of the prior art, present invention is primarily targeted at, promote the fire resistant quality of existing refractory brick, improve resistance to
Firebrick service life, so that refractory brick has more the value in industry.
The object of the invention to solve the technical problems realizes by the following technical solutions.The one proposed according to the present invention
Gas generator refractory brick based on plate diamond spar, its formula consists of: plate diamond spar 35%-45%, bauxite 15%-25%,
Clay 15%-25%, wood flour 10%-20%, silicon powder 1%-6%, alumina powder 1%-6%, kyanite 1%-5%, andalusite 1%-4%,
Calcium aluminate 0.5%-2%, additive 1%-5%, coagulant 0.5%-2%.
Preferably, its formula consists of: plate diamond spar 40%, bauxite 20%, clay 15%, wood flour 15%, silicon powder 2%,
Alumina powder 2%, kyanite 1%, andalusite 1%, calcium aluminate 0.5%, additive 2%, coagulant 1.5%.
Preferably, described additive is Cr2O3, and described coagulant is sodium aluminate.
A kind of gas generator refractory brick based on plate diamond spar of the present invention, its preparation process comprises the following steps:
(1) pulverize: the components in certain proportion in above-mentioned formula is configured, use double-roll crusher above-mentioned formula will to remove andalusite and wood
Material outside bits mixes and pulverizes, and then wears into mixed-powder with ball mill and sieves, and mixed-powder fineness is 205 mesh,
Wood flour Raymond machine is levigate and sieves, and wood flour fineness is less than 1mm, and andalusite double-roll crusher is individually pulverized and enters ball mill
Pulverizing powder also sieves, and andalusite fineness of powder is 86 mesh；
(2) batch mixing: use Secondary mixing, above-mentioned mixed-powder, wood flour and andalusite powder are together placed in blender,
Mixing time is 2-3min for the first time, and rotating speed is 80-120r/min, is subsequently adding the water of 10%-12% and is allowed to be mixed into plastic
Shape, mixing time is 4-5min for the second time, and rotating speed is 150-210r/min；
(3) ageing mixture: ageing mixture is carried out in ageing mixture storehouse, the ageing mixture time is 10h, and ageing mixture equipment uses reversible moving formula distributing device；
(4) sintering: firing temperature uses 1400-1600 DEG C；
(5) insulation: temperature retention time is 4-6h；
(6) molding: molding uses semi-hard plastic double-stage vacuum extruding machine, and briquetting pressure is 10MPa, a size of 240mm × 115mm
× 90mm or 390mm × 190mm × 190mm；
(7) maintenance: at room temperature maintenance 48h.
Preferably, firing temperature uses 1450-1500 DEG C, and optimum temperature is 1500 DEG C.
By technique scheme, the refractory brick of the present invention at least has the advantage that
The refractory brick of the present invention is simple to manufacture, and cost is controlled, and resistance to elevated temperatures is excellent, and a large amount of due to plate diamond spar of the present invention
Use, and the inherent character of plate diamond spar itself so that the thermal shock resistance of refractory brick of the present invention and bending strength are more traditional resistance to
Firebrick is higher.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below in conjunction with tool
Body embodiment, is expanded on further the present invention.
Embodiment 1
A kind of gas generator refractory brick based on plate diamond spar of the present invention, its formula consists of: plate diamond spar 40%,
Bauxite 20%, clay 15%, wood flour 15%, silicon powder 2%, alumina powder 2%, kyanite 1%, andalusite 1%, aluminic acid
Calcium 0.5%, additive 2%, coagulant 1.5%.
Preferably, described additive is Cr2O3, and described coagulant is sodium aluminate.
A kind of gas generator refractory brick based on plate diamond spar of the present invention, its preparation process comprises the following steps:
(1) pulverize: the components in certain proportion in above-mentioned formula is configured, use double-roll crusher above-mentioned formula will to remove andalusite and wood
Material outside bits mixes and pulverizes, and then wears into mixed-powder with ball mill and sieves, and mixed-powder fineness is 205 mesh,
Wood flour Raymond machine is levigate and sieves, and wood flour fineness is less than 1mm, and andalusite double-roll crusher is individually pulverized and enters ball mill
Pulverizing powder also sieves, and andalusite fineness of powder is 86 mesh；
(2) batch mixing: use Secondary mixing, above-mentioned mixed-powder, wood flour and andalusite powder are together placed in blender,
Mixing time is 2-3min for the first time, and rotating speed is 80-120r/min, is subsequently adding the water of 10%-12% and is allowed to be mixed into plastic
Shape, mixing time is 4-5min for the second time, and rotating speed is 150-210r/min；
(3) ageing mixture: ageing mixture is carried out in ageing mixture storehouse, the ageing mixture time is 10h, and ageing mixture equipment uses reversible moving formula distributing device；
(4) sintering: firing temperature uses 1400-1600 DEG C；
(5) insulation: temperature retention time is 4-6h；
(6) molding: molding uses semi-hard plastic double-stage vacuum extruding machine, and briquetting pressure is 10MPa, a size of 240mm × 115mm
× 90mm or 390mm × 190mm × 190mm；
(7) maintenance: at room temperature maintenance 48h.
Preferably, firing temperature uses 1450-1500 DEG C, and optimum temperature is 1500 DEG C.
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.Skilled person will appreciate that of the industry,
The present invention is not restricted to the described embodiments, the principle that the present invention is simply described of the description in above-mentioned embodiment and description,
Without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these changes and improvements all fall
Enter in the scope of protection of present invention.Claimed scope is defined by appending claims and equivalent thereof.
Claims (5)
1. a gas generator refractory brick based on plate diamond spar, it is characterised in that: its formula consists of: plate diamond spar
35%-45%, bauxite 15%-25%, clay 15%-25%, wood flour 10%-20%, silicon powder 1%-6%, alumina powder 1%-6%,
Kyanite 1%-5%, andalusite 1%-4%, calcium aluminate 0.5%-2%, additive 1%-5%, coagulant 0.5%-2%.
A kind of gas generator refractory brick based on plate diamond spar the most according to claim 1, it is characterised in that: it is joined
Side consists of: plate diamond spar 40%, bauxite 20%, clay 15%, wood flour 15%, silicon powder 2%, alumina powder 2%, indigo plant
Spar 1%, andalusite 1%, calcium aluminate 0.5%, additive 2%, coagulant 1.5%.
A kind of gas generator refractory brick based on plate diamond spar the most according to claim 1, it is characterised in that: described
Additive be Cr2O3, described coagulant is sodium aluminate.
A kind of gas generator refractory brick based on plate diamond spar the most according to claim 1 and 2, it is characterised in that:
Preparation process comprises the following steps:
(1) pulverize: the components in certain proportion in above-mentioned formula is configured, use double-roll crusher above-mentioned formula will to remove andalusite and wood
Material outside bits mixes and pulverizes, and then wears into mixed-powder with ball mill and sieves, and mixed-powder fineness is 205 mesh,
Wood flour Raymond machine is levigate and sieves, and wood flour fineness is less than 1mm, and andalusite double-roll crusher is individually pulverized and enters ball mill
Pulverizing powder also sieves, and andalusite fineness of powder is 86 mesh；
(2) batch mixing: use Secondary mixing, above-mentioned mixed-powder, wood flour and andalusite powder are together placed in blender,
Mixing time is 2-3min for the first time, and rotating speed is 80-120r/min, is subsequently adding the water of 10%-12% and is allowed to be mixed into plastic
Shape, mixing time is 4-5min for the second time, and rotating speed is 150-210r/min；
(3) ageing mixture: ageing mixture is carried out in ageing mixture storehouse, the ageing mixture time is 10h, and ageing mixture equipment uses reversible moving formula distributing device；
(4) sintering: firing temperature uses 1400-1600 DEG C；
(5) insulation: temperature retention time is 4-6h；
(6) molding: molding uses semi-hard plastic double-stage vacuum extruding machine, and briquetting pressure is 10MPa, a size of 240mm × 115mm
× 90mm or 390mm × 190mm × 190mm；
(7) maintenance: at room temperature maintenance 48h.
A kind of gas generator refractory brick based on plate diamond spar the most according to claim 4, it is characterised in that: burn till
Temperature uses 1450-1500 DEG C, and optimum temperature is 1500 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610307376.6A CN105859265A (en) | 2016-05-11 | 2016-05-11 | Tabular corundum-based refractory brick for gas producer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610307376.6A CN105859265A (en) | 2016-05-11 | 2016-05-11 | Tabular corundum-based refractory brick for gas producer |
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| Publication Number | Publication Date |
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| CN105859265A true CN105859265A (en) | 2016-08-17 |
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| CN201610307376.6A Pending CN105859265A (en) | 2016-05-11 | 2016-05-11 | Tabular corundum-based refractory brick for gas producer |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110698172A (en) * | 2019-11-22 | 2020-01-17 | 常江 | Preparation method of flame-retardant refractory brick |
| CN113354400A (en) * | 2021-06-30 | 2021-09-07 | 湖南湘钢瑞泰科技有限公司 | Refractory plastic material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102992783A (en) * | 2011-09-14 | 2013-03-27 | 中钢集团耐火材料有限公司 | Corundum brick used for gas channel parts of bottle, can, glass kiln and combustion chamber of rangette |
| CN104446568A (en) * | 2014-12-15 | 2015-03-25 | 山东鲁阳股份有限公司 | Fireproof insulating brick and preparation method thereof |
| CN105367096A (en) * | 2015-11-25 | 2016-03-02 | 南京联合荣大工程材料有限责任公司 | Refractory raw material and blast furnace press-in material containing same |
-
2016
- 2016-05-11 CN CN201610307376.6A patent/CN105859265A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102992783A (en) * | 2011-09-14 | 2013-03-27 | 中钢集团耐火材料有限公司 | Corundum brick used for gas channel parts of bottle, can, glass kiln and combustion chamber of rangette |
| CN104446568A (en) * | 2014-12-15 | 2015-03-25 | 山东鲁阳股份有限公司 | Fireproof insulating brick and preparation method thereof |
| CN105367096A (en) * | 2015-11-25 | 2016-03-02 | 南京联合荣大工程材料有限责任公司 | Refractory raw material and blast furnace press-in material containing same |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110698172A (en) * | 2019-11-22 | 2020-01-17 | 常江 | Preparation method of flame-retardant refractory brick |
| CN113354400A (en) * | 2021-06-30 | 2021-09-07 | 湖南湘钢瑞泰科技有限公司 | Refractory plastic material and preparation method thereof |
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