CN105803680B - The method for preparing asphalt water-proof coiled material needle-punched geotextiles as raw material using polyester bottle slice - Google Patents

The method for preparing asphalt water-proof coiled material needle-punched geotextiles as raw material using polyester bottle slice Download PDF

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Publication number
CN105803680B
CN105803680B CN201410855455.1A CN201410855455A CN105803680B CN 105803680 B CN105803680 B CN 105803680B CN 201410855455 A CN201410855455 A CN 201410855455A CN 105803680 B CN105803680 B CN 105803680B
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needle
polyester
proof coiled
raw material
asphalt water
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CN105803680A (en
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智来宽
史敬月
吴昊
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Dalian Huayang New Materials Technology Co Ltd
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Dalian Huayang New Materials Technology Co Ltd
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Abstract

A method of asphalt water-proof coiled material needle-punched geotextiles are prepared by raw material of polyester bottle slice, it is mainly: polyester bottle slice enters extruder after pre-crystallized and is dry and squeezes out, the reworked material melt after being filtered mix in the duct after together into reactor.Melt passes through the processes such as hydrolysis, alcoholysis, homogenizing, decontamination reaggregation, final viscosity is homogenized and stable polyester fondant, then it filters through booster pump pressurization, filter again and is sprayed into filament through measuring from spinneret into spinning machine, by side-blown air cooling, through sub-wire, pendulum wire after tubular type air drawing, uniform web is formed on lapper, and fibre web output is sent to needing machine carries out needle thorn consolidation, cutting is wound, asphalt water-proof coiled material needle-punched geotextiles are made.The present invention, as raw material, can not only be recycled waste polyester bottle chip using waste polyester bottle chip, but also be conducive to energy saving, the production cost of reduction asphalt water-proof coiled material needle-punched geotextiles.

Description

The method for preparing asphalt water-proof coiled material needle-punched geotextiles as raw material using polyester bottle slice
Technical field
The present invention relates to a kind of preparation method of chemical fibre nonwoven products, especially production asphalt water-proof coiled materials to pierce soil with needle The preparation method of work cloth.
Background technique
For China's asphalt water-proof coiled material tire base fabric used at present mainly based on short polyester tire, short polyester tire is with poly- Non-woven cloth is made by shredding mixing, combing (or gas comb) networking, cross lapping, drawing-off and needle thorn consolidation in ester staple fiber, then Through sizing, impregnation, drying and be made.But since it haves the defects that in many performances, developed countries do not use substantially Or it is few using as modified asphalt waterproof coiled material tire base.With advances in technology, use has also been developed in recent years, China Polyester filament tire base fabric is the asphalt water-proof coiled material of base tire, and raw material is polyester slice.But it is not only wasted to be disposable Resource pollutes environment, and cost is also higher.
Using polyester bottle slice as raw material, produce long filament POY, the technique of FDY is mature, the country also use polyester bottle slice for Raw material produces the introduction of polyester geotex-tile or spun-bonded hot rolling non-woven fabric, but since waterproof coiled material tyre base is non-with terylene spun-bonded needle thorn Some particular/special requirements of woven cloths use current production method and technique that can't produce pitch using polyester bottle slice as raw material anti- Water coiled material needle-punched geotextiles.
Summary of the invention
The purpose of the present invention is to provide one kind to prepare asphalt water-proof coiled material needle-punched geotextiles by raw material of polyester bottle slice Method.
The present invention is mainly that raw material prepares asphalt water-proof coiled material needle as raw material substitution with polyester (PET) using polyester bottle slice The method for piercing geotextiles, therefore concrete operations of the invention are substantially same as the prior art, only because raw material changes some operations It is also changed correspondingly with parameter.
Method main contents of the invention are as follows:
1, the present invention is, first by its pre-crystallized and drying, to make dry bottle piece moisture content control using the polyester bottle slice of recycling as raw material System is in≤50PPM.
2, polyester bottles bottle piece is put into after extruder melting extrusion and enters filter, filtering accuracy is 50 μ.
3, the reworked material melt after being filtered enters reactor after mixing in the duct together.Melt passes through water The processes such as solution, alcoholysis, homogenizing, decontamination reaggregation, final viscosity obtain viscosity-adjusting agent to 0.70~0.80 ± 0.01dl/g it Between be homogenized and stable polyester fondant, then again through booster pump pressurization and filter filter into spinning machine, filtering accuracy 25 μ。
4, pump-metered is measured, is sprayed into filament from spinneret, the revolving speed by controlling metering pump controls the list of polyester filament Silk size is 2~4dpf.
5, polyester filament is by side-blown air cooling, through sub-wire, pendulum wire after tubular type air drawing, is formed on lapper uniform Fibre web output is sent to needing machine carries out needle thorn consolidation, cutting is wound, asphalt water-proof coiled material needle thorn geotechnique is made by web Cloth.
The invention has the following advantages over the prior art:
1, using waste polyester bottle chip as raw material, waste polyester bottle chip can not only be recycled, but also be conducive to It is energy saving, reduce the production cost of asphalt water-proof coiled material needle-punched geotextiles.
2, using asphalt water-proof coiled material needle-punched geotextiles produced by the invention, product performance index with use polyester for In the identical situation of geotextiles performance indicator of raw material, production cost can reduce by 500~600 yuan/ton or so.
Detailed description of the invention
Fig. 1 is process flow chart of the invention.
Specific embodiment
Embodiment 1:
It is pre-crystallized and in 160 DEG C in 170 DEG C that the polyester bottle slice of recycling is placed in the pre-crystallizer that drying capacity is 600Kg/h It is dry, make dry bottle piece moisture control in 48PPM.Polyester bottle slice after pre-crystallized and is dry enters screw extruder melting It squeezes out, each area's temperature of screw extruder: 276 DEG C, 281 DEG C, 284 DEG C, 285 DEG C, 285 DEG C, 285 DEG C, entering filter later, Filtering accuracy is 50 μ.Reworked material melt after being filtered enters reactor after mixing in the duct together.Melt passes through The processes such as hydrolysis, alcoholysis, homogenizing, decontamination reaggregation, final viscosity obtain the polyester of viscosity-adjusting agent to 0.72 ± 0.01dl/g Then melt is filtered through booster pump pressurization and filter into spinning machine again, filtering accuracy is 25 μ.Through measuring pump-metered, from spray Filament plate is sprayed into filament, spinning temperature: 285 DEG C, component pressure: 15Mpa, the revolving speed by controlling metering pump control polyester filament Filament number is 3dpf.Polyester filament is by side-blown air temperature: 22 DEG C, quenching air humidity: and 70%, cooling and drawing-off pressure: 0.55Mpa, through sub-wire, pendulum wire after tubular type air drawing, pendulum wire frequency: 750, the amplitude of oscillation: 45mm, with pendulum wire frequency on lapper Rate: 750, the amplitude of oscillation: 45mm, lapping speed: 8m/min, precompressed roll temperature: 125 DEG C, pre-needling bestock: 4000 needles/m, needle Thorn frequency: 940, needle pierces traverse: 40mm, and pre-needling needle is deep: 8.121mm, main needle pierce bestock: 4000 needles/m, punch frequency: 900, needle pierces traverse: 30mm, and main acupuncture needle is deep: 5.002mm, winding speed: 10m/min forms uniform web, by fibre web Output is sent to needing machine and carries out needle thorn consolidation, cutting winding, that is, asphalt water-proof coiled material needle-punched geotextiles is made, the polyester bottle slice Filament spunbond needle fabric product specification: 7.0 meters of breadth, grammes per square metre 135g/m2, filament number 3dpf, the longitudinal strength of product: 574.3N, the lateral strength of product: 568.3N, product longitudinal elongation: 58.9%, product transverse extension: 65.1%, grammes per square metre CV%: 4.8, it is heat-shrinked %:1.5%.
Embodiment 2:
Using polyester bottle slice as raw material, technical process is same as Example 1, and design parameter is as follows: drying capacity: 600Kg/h, in advance Crystallization temperature: 171 DEG C, drying temperature: 164 DEG C, bottle piece moisture content after doing: 45ppm, each area's temperature of screw extruder: 276 DEG C, 281 DEG C, 284 DEG C, 286 DEG C, 286 DEG C, 286 DEG C, enter filter later, filtering accuracy is 50 μ.After being filtered Reworked material melt enters reactor after mixing in the duct together.Melt passes through hydrolysis, alcoholysis, homogenizing, decontamination reaggregation etc. Process, final viscosity obtain the polyester fondant of viscosity-adjusting agent to 0.75 ± 0.01dl/g, are then pressurized and filter through booster pump again Device is filtered into spinning machine, and filtering accuracy is 25 μ.Pump-metered is measured, is sprayed into filament from spinneret, spinning temperature: 287 DEG C, Component pressure: 14Mpa, side-blown air temperature: 22 DEG C, quenching air humidity: 70%, drawing-off pressure: 0.57Mpa, pendulum wire frequency: 900, the amplitude of oscillation: 52mm, lapping speed: 7m/min, precompressed roll temperature: 130 DEG C, pre-needling bestock: 4000 needles/m, needle thorn frequency Rate: 1040, needle pierces traverse: 40mm, and pre-needling needle is deep: 8.3421mm, main needle pierce bestock: 4000 needles/m, punch frequency: 1000, needle pierces traverse: 30mm, and main acupuncture needle is deep: 5.014mm, winding speed: 8m/min forms uniform web, by fibre web Output is sent to needing machine and carries out needle thorn consolidation, cutting winding, that is, asphalt water-proof coiled material needle-punched geotextiles is made, the polyester bottle slice Filament spunbond needle fabric product specification: 7.0 meters of breadth, grammes per square metre 200g/m2, asphalt-felt tyre base grammes per square metre 280g/m2, monofilament fibre 3.5dpf is spent, the longitudinal strength of product: 985.4N, the lateral strength of product: 5915.3N, product longitudinal elongation: 54.4%, product is horizontal To elongation: 58.3%, grammes per square metre CV%:5.3 are heat-shrinked %:1.5%.

Claims (1)

1. a kind of method for preparing asphalt water-proof coiled material needle-punched geotextiles as raw material using polyester bottle slice, it is characterised in that:
1) first that its is pre-crystallized and dry using the polyester bottle slice of recycling as raw material, make dry bottle piece moisture control in≤50PPM;
2) polyester bottles bottle piece is put into after extruder melting extrusion and enters filter, filtering accuracy is 50 μ;
3) the reworked material melt after being filtered enters reactor together after mixing in the duct, melt is by hydrolysis, alcohol Solution, homogenizing, decontamination and reaggregation finally obtain viscosity-adjusting agent to homogenizing between 0.70~0.80 ± 0.01dl/g and stable Then polyester fondant is filtered through booster pump pressurization and filter into spinning machine again, filtering accuracy is 25 μ;
4) pump-metered is measured, is sprayed into filament from spinneret, the monofilament that the revolving speed by controlling metering pump controls polyester filament is fine Degree is 2~4dpf;
5) polyester filament through sub-wire, pendulum wire after tubular type air drawing, forms uniform fiber by side-blown air cooling on lapper Web output is sent to needing machine carries out needle thorn consolidation, cutting is wound, asphalt water-proof coiled material needle-punched geotextiles is made by net.
CN201410855455.1A 2014-12-31 2014-12-31 The method for preparing asphalt water-proof coiled material needle-punched geotextiles as raw material using polyester bottle slice Active CN105803680B (en)

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Publication number Priority date Publication date Assignee Title
CN106349929A (en) * 2016-08-23 2017-01-25 秦皇岛市地维建材有限公司 Environmental-friendly high-polymer modified asphalt waterproof coiled material and method for preparing same
CN107938177A (en) * 2017-12-27 2018-04-20 大连华阳新材料科技股份有限公司 With position iso-fineness polyester filament geotextiles preparation method
CN115418798A (en) * 2022-10-09 2022-12-02 江阴市华思诚无纺布有限公司 Polyester tire base fabric based on multilayer laying net and preparation method thereof

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Publication number Priority date Publication date Assignee Title
US6855650B1 (en) * 2000-08-25 2005-02-15 American Excelsior Company Synthetic fiber filled erosion control blanket
CN101724980A (en) * 2009-12-03 2010-06-09 梁本树 Process for producing polyester geotextile with raw material of PET bottle flakes
CN103215676A (en) * 2013-04-17 2013-07-24 龙福环能科技股份有限公司 Method for producing flat and long polyester POY (pre-oriented yarn) by recovering PET (polyethylene terephthalate) bottle sheets
CN103882534A (en) * 2012-12-20 2014-06-25 江苏蓝品纤维科技发展有限公司 Production process for utilizing waste bottle chips to produce high-grade core materials for textile use

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6855650B1 (en) * 2000-08-25 2005-02-15 American Excelsior Company Synthetic fiber filled erosion control blanket
CN101724980A (en) * 2009-12-03 2010-06-09 梁本树 Process for producing polyester geotextile with raw material of PET bottle flakes
CN103882534A (en) * 2012-12-20 2014-06-25 江苏蓝品纤维科技发展有限公司 Production process for utilizing waste bottle chips to produce high-grade core materials for textile use
CN103215676A (en) * 2013-04-17 2013-07-24 龙福环能科技股份有限公司 Method for producing flat and long polyester POY (pre-oriented yarn) by recovering PET (polyethylene terephthalate) bottle sheets

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