CN105778636A - Environment-friendly exterior wall elastic styling paint and preparation method thereof - Google Patents

Environment-friendly exterior wall elastic styling paint and preparation method thereof Download PDF

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Publication number
CN105778636A
CN105778636A CN201410842953.2A CN201410842953A CN105778636A CN 105778636 A CN105778636 A CN 105778636A CN 201410842953 A CN201410842953 A CN 201410842953A CN 105778636 A CN105778636 A CN 105778636A
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China
Prior art keywords
stirring
exterior wall
environment
emulsion
mould wash
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CN201410842953.2A
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Chinese (zh)
Inventor
侯进全
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SHANGHAI BOHENG BUILDING MATERIALS TECHNOLOGY DEVELOPMENT CO LTD
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SHANGHAI BOHENG BUILDING MATERIALS TECHNOLOGY DEVELOPMENT CO LTD
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Priority to CN201410842953.2A priority Critical patent/CN105778636A/en
Publication of CN105778636A publication Critical patent/CN105778636A/en
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  • Compositions Of Macromolecular Compounds (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention relates to an environment-friendly exterior wall elastic styling paint and a preparation method thereof. The paint comprises the following components, by weight: 25-40 parts of resin synthetic emulsion, 40-55 parts of powders, 2-5 parts of auxiliary agents, and 10-20 parts of water. According to the formula, all water is first added into a stirring kettle, and stirring is carried out with a speed of 300-600r/m; under continuous stirring, the first three among the auxiliary agents are sequentially added into the stirring kettle, and the mixture is well mixed by stirring; the powders are sequentially added into the stirring kettle according to the order in the formula; the stirring speed is adjusted to 1200-1600r/m, and stirring is carried out for 45-60min; after high-speed dispersion, the stirring speed is reduced to a low speed of 500-600r/m; all the resin synthetic emulsion is added into the stirring kettle; when the resin synthetic emulsion is well mixed, the rest part of the auxiliary agents are added; and a thickening agent is added under slow stirring, until a needed viscosity is reached. Compared with prior arts, the method provided by the invention has the advantages of low cost and simple process, and the product has the advantages of good elasticity, good weatherability and the like.

Description

A kind of environment-friendly exterior wall elasticity mould wash and preparation method thereof
Technical field
The present invention relates to elastic coating, be specifically related to environment-friendly exterior wall elasticity mould wash and preparation method thereof.
Background technology
Development along with coating industry, the various performances of coating and the demand of moulding are also got more and more, in the middle of the process of this development, external wall elastic building coating can be widely popularized, while being satisfied with the elongation percentage of elastomeric material and covering fine cracks, some effects such as various plucking and plucking Pericarpium Citri tangerinae stricture of vagina are done for coating, is promoted widely and approve.From before single flat be coated onto the flexible exterior coating having an elongation percentage to the complex layer coating having moulding.But in the process of construction, he is the coating of a cladding, to carry out priming paint construction, middle painting plucking moulding layer, upper 2 times finish paints during construction.So during construction, operation is too many, and cost of labor cost is higher.On secondary basis, our meeting the market requirement does one-time formed galling paint, handle modeling and weather-proof combine, so both convenient construction paint film also full perfections.
Patent application 200410058168.4 discloses a kind of decoration of exterior wall elastic coating and manufacture method,, polycarboxylic acids ammonium, alkylphenol polyoxyethylene, hydroxyethyl cellulose intoxicated by acrylic acid self-crosslinking copolymer emulsion, different crying of a child the beautiful jade-3-ketone of 5-chloro-2-methyl-4-, n-octyl group-different crying of a child beautiful jade, three normal-butyl phosphate esters, propylene glycol, 2,2,4-trimethyl-1,3-pentanediol mono isobutyrate, titanium dioxide, triple superphosphate, Pulvis Talci, Gao Lingshi, 2-amino-2-methyl-1-propanol, polyurethane-modified polyethers are agitated, grinding is made.Although this coating is elastic better has certain weatherability, but relatively costly, preparation complexity.
Summary of the invention
Defect that the purpose of the present invention is contemplated to overcome above-mentioned prior art to exist and a kind of cost is low, operation simple, good springiness, weatherability are strong environment-friendly exterior wall elasticity mould wash and preparation method thereof is provided.
The purpose of the present invention can be achieved through the following technical solutions: a kind of environment-friendly exterior wall elasticity mould wash, it is characterised in that this coating includes the component of following weight portion: resins synthesis emulsion 25~40, powder body 40-55, auxiliary agent 2-5, water 10-20.
Described resins synthesis emulsion particle diameter is at 0.01-0.02 micron, and viscosity is at 300~1500Pa s, and testing conditions is: 2#.60rpm, 25 DEG C.His its existing good elongation percentage of this emulsion, and stain resistance has again good weatherability.
Described resins synthesis emulsion is made by the following method: by weight percentage, commercially available emulsion is added 80%, water 14%, cellulose 0.1%, coalescents 3.2%, propylene glycol 2.0%, adhesion promoter 0.2%, defoamer 0.1%, thickening agent 0.3% and progressive dose 0.1% stir at normal temperatures a kind of is with granular cream liquid to be resins synthesis emulsion.
Described commercially available emulsion includes styrene-acrylic emulsion, pure-acrylic emulsion or silicone acrylic emulsion.
Described powder body includes the component of following weight portion: rutile-type exterior wall titanium dioxide (1250 order) 10~30, Kaolin (1250 order) 1~10, barium sulfate (1250 order) 5~15, triple superphosphate (1250 order) 10~30;
Described powder body includes the component of following weight portion: rutile-type exterior wall titanium dioxide 20, Kaolin 5, barium sulfate 10, triple superphosphate 20.
Described auxiliary agent includes the component of following weight portion: antibacterial is with 0.2, and propylene glycol is with 1.0, and defoamer is with 0.3, and dispersant is with 0.6, and cellulose 0.3, thickening agent is with 1.
The preparation method of a kind of environment-friendly exterior wall elasticity mould wash, it is characterised in that the method comprises the following steps:
(1) first all being put in stirred tank by water by recipe requirements, 300-600 rev/min is stirred;
(2) it is kept stirring for and by the stirred tank of input successively of first three in auxiliary agent, stirs;
(3) to be mixed uniformly after powder body is sequentially added in stirred tank according to formula order, speed is transferred to 1200-1600 and turns, carry out the stirring of 45-60 minute;
(4) when, after high speed dispersion, being down to low speed 500-600 and turn, resins synthesis emulsion is all added in stirred tank;
(5) resins synthesis emulsion is stirring evenly and then adding into remainder auxiliary agent;
(6) slowly stirring addition thickening agent is transferred to required viscosity again.
Adding auxiliary agent according to formula can make auxiliary agent be fully utilized, and will not be neutralized each other.Need to carry out high speed dispersion after powder body adds, can disperse when speed is inadequate to be fully that product produces precipitation.
Compared with prior art, the invention have the advantages that
(1) this elasticity mould wash becomes complex layer coating into monolayer mould wash;
(2) construction aspect operation tails off simply;
(3) construction cost, reduction of erection time can be reduced;
(4) reduce aberration and construction connects a batch problem.
Detailed description of the invention
Below embodiments of the invention being elaborated, the present embodiment is carried out under premised on technical solution of the present invention, gives detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following embodiment.
The auxiliary agent adopted in example below is: antibacterial SA-16, propylene glycol BS-12, defoamer XA-26, dispersant FA-34, cellulose B-30K, thickening agent ZA-48.
Embodiment 1
A kind of preparation method of environment-friendly exterior wall elasticity mould wash, the method comprises the following steps:
(1) first all being put in stirred tank by water 15kg by recipe requirements, 300 revs/min are stirred;
(2) it is kept stirring for and SA-160.2kg, BS-121.0kg, XA-260.3kg are put in stirred tank successively, stirring;
(3) to be mixed uniformly after by powder body: rutile-type exterior wall titanium dioxide 20kg, Kaolin 5kg, barium sulfate 10kg, triple superphosphate 20kg is sequentially added in stirred tank according to formula order, and speed is transferred to 1200 turns, carries out the stirring of 45 minutes;
(4) when, after high speed dispersion, being down to low speed 500 turns, resins synthesis emulsion 30kg is all added in stirred tank;Described resins synthesis emulsion particle diameter is at 0.01-0.02 micron, and viscosity is at 300~1500Pa s, and testing conditions is: 2#.60rpm, 25 DEG C.Described resins synthesis emulsion is made by the following method: by weight percentage, commercially available emulsion is added 80%, water 14%, cellulose 0.1%, coalescents 3.2%, propylene glycol 2.0%, adhesion promoter 0.2%, defoamer 0.1%, thickening agent 0.3% and progressive dose 0.1% stir at normal temperatures a kind of is with granular cream liquid to be resins synthesis emulsion.
(5) resins synthesis emulsion is stirring evenly and then adding into remainder auxiliary agent: FA-340.6kg, B-300.3kg, ZA-481kg;
(6) slowly stirring addition thickening agent is transferred to required viscosity again.
Embodiment 2
A kind of preparation method of environment-friendly exterior wall elasticity mould wash, the method comprises the following steps:
(1) first all being put in stirred tank by water 10kg by recipe requirements, 300 revs/min are stirred;
(2) it is kept stirring for and SA-160.2kg, BS-120.5kg, XA-260.3kg are put in stirred tank successively, stirring;
(3) to be mixed uniformly after by powder body: rutile-type exterior wall titanium dioxide 30kg, Kaolin 1kg, barium sulfate 5kg, triple superphosphate 10kg is sequentially added in stirred tank according to formula order, and speed is transferred to 1500 turns, carries out the stirring of 50 minutes;
(4) when, after high speed dispersion, being down to low speed 500-600 and turn, resins synthesis emulsion 25kg is all added in stirred tank;Described resins synthesis emulsion particle diameter is at 0.01-0.02 micron, and viscosity is at 300~1500Pa s, and testing conditions is: 2#.60rpm, 25 DEG C.Described resins synthesis emulsion is made by the following method: by weight percentage, commercially available emulsion is added 80%, water 14%, cellulose 0.1%, coalescents 3.2%, propylene glycol 2.0%, adhesion promoter 0.2%, defoamer 0.1%, thickening agent 0.3% and progressive dose 0.1% stir at normal temperatures a kind of is with granular cream liquid to be resins synthesis emulsion.
(5) resins synthesis emulsion is stirring evenly and then adding into remainder auxiliary agent: FA-340.2kg, B-300.3kg, ZA-480.5kg;
(6) slowly stirring addition thickening agent is transferred to required viscosity again.
Embodiment 3
A kind of preparation method of environment-friendly exterior wall elasticity mould wash, the method comprises the following steps:
(1) first all being put in stirred tank by water 20kg by recipe requirements, 600 revs/min are stirred;
(2) it is kept stirring for and SA-160.2kg, BS-121.6kg, XA-260.3kg are put in stirred tank successively, stirring;
(3) to be mixed uniformly after by powder body: rutile-type exterior wall titanium dioxide 15kg, Kaolin 5kg, barium sulfate 5kg, triple superphosphate 15kg is sequentially added in stirred tank according to formula order, and speed is transferred to 1600 turns, carries out the stirring of 60 minutes;
(4) when, after high speed dispersion, being down to low speed 500-600 and turn, resins synthesis emulsion 40kg is all added in stirred tank;Described resins synthesis emulsion particle diameter is at 0.01-0.02 micron, and viscosity is at 300~1500Pa s, and testing conditions is: 2#.60rpm, 25 DEG C.Described resins synthesis emulsion is made by the following method: by weight percentage, commercially available emulsion is added 80%, water 14%, cellulose 0.1%, coalescents 3.2%, propylene glycol 2.0%, adhesion promoter 0.2%, defoamer 0.1%, thickening agent 0.3% and progressive dose 0.1% stir at normal temperatures a kind of is with granular cream liquid to be resins synthesis emulsion.
(5) resins synthesis emulsion is stirring evenly and then adding into remainder auxiliary agent: FA-340.6kg, B-300.3kg, ZA-482kg;
(6) slowly stirring addition thickening agent is transferred to required viscosity again.
The performance of the coating obtained by above-described embodiment is as follows:
Embodiment 1 Embodiment 2 Embodiment 3
Hot strength 1.0 1.2 1.5
Elongation at break 200 180 250
Anti-aging test 510 420 600
Abrasion resistance 2000 2000 2000

Claims (8)

1. an environment-friendly exterior wall elasticity mould wash, it is characterised in that this coating includes the component of following weight portion: resins synthesis emulsion 25~40, powder body 40-55, auxiliary agent 2-5, water 10-20.
2. environment-friendly exterior wall elasticity mould wash according to claim 1, it is characterised in that described resins synthesis emulsion particle diameter is at 0.01-0.02 micron, and viscosity is at 300~1500Pa s, and testing conditions is: 2#.60rpm, 25 DEG C.
3. environment-friendly exterior wall elasticity mould wash according to claim 1 and 2, it is characterized in that, described resins synthesis emulsion is made by the following method: by weight percentage, adds 80% by commercially available emulsion, water 14%, cellulose 0.1%, coalescents 3.2%, propylene glycol 2.0%, adhesion promoter 0.2%, defoamer 0.1%, thickening agent 0.3% and progressive dose 0.1% stir at normal temperatures a kind of is with granular cream liquid to be resins synthesis emulsion.
4. environment-friendly exterior wall elasticity mould wash according to claim 3, it is characterised in that described commercially available emulsion includes styrene-acrylic emulsion, pure-acrylic emulsion or silicone acrylic emulsion.
5. environment-friendly exterior wall elasticity mould wash according to claim 1, it is characterized in that, described powder body includes the component of following weight portion: the Kaolin 1~10 of rutile-type exterior wall titanium dioxide 10~30,1250 order of 1250 orders, the triple superphosphate 10~30 of barium sulfate 5~15,1250 order of 1250 orders.
6. environment-friendly exterior wall elasticity mould wash according to claim 5, it is characterised in that described powder body includes the component of following weight portion: rutile-type exterior wall titanium dioxide 20, Kaolin 5, barium sulfate 10, triple superphosphate 20.
7. environment-friendly exterior wall elasticity mould wash according to claim 1, it is characterised in that described auxiliary agent includes the component of following weight portion: antibacterial is with 0.2, and propylene glycol is with 1.0, and defoamer is with 0.3, and dispersant is with 0.6, and cellulose 0.3, thickening agent is with 1.
8. the preparation method of an environment-friendly exterior wall elasticity mould wash as claimed in claim 1, it is characterised in that the method comprises the following steps:
(1) first all being put in stirred tank by water by recipe requirements, 300-600 rev/min is stirred;
(2) it is kept stirring for and by the stirred tank of input successively of first three in auxiliary agent, stirs;
(3) to be mixed uniformly after powder body is sequentially added in stirred tank according to formula order, speed is transferred to 1200-1600 and turns, carry out the stirring of 45-60 minute;
(4) when, after high speed dispersion, being down to low speed 500-600 and turn, resins synthesis emulsion is all added in stirred tank;
(5) resins synthesis emulsion is stirring evenly and then adding into remainder auxiliary agent;
(6) slowly stirring addition thickening agent is transferred to required viscosity again.
CN201410842953.2A 2014-12-25 2014-12-25 Environment-friendly exterior wall elastic styling paint and preparation method thereof Pending CN105778636A (en)

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Application Number Priority Date Filing Date Title
CN201410842953.2A CN105778636A (en) 2014-12-25 2014-12-25 Environment-friendly exterior wall elastic styling paint and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107118647A (en) * 2017-06-20 2017-09-01 东台市明山石涂料有限公司 A kind of elastic outer wall paint and preparation method thereof
CN115073987A (en) * 2022-07-27 2022-09-20 昆山爱克树脂有限公司 Novel single-layer elastic napping water-based paint

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101624487A (en) * 2009-08-06 2010-01-13 徐贵才 Elastic paint
CN101955700A (en) * 2009-09-08 2011-01-26 广东美涂士建材股份有限公司 Acid rain resistant flexible outer wall emulsion paint
CN103113796A (en) * 2011-11-16 2013-05-22 上海富臣化工有限公司 Elastic antifouling aqueous fluorocarbon exterior wall paint

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101624487A (en) * 2009-08-06 2010-01-13 徐贵才 Elastic paint
CN101955700A (en) * 2009-09-08 2011-01-26 广东美涂士建材股份有限公司 Acid rain resistant flexible outer wall emulsion paint
CN103113796A (en) * 2011-11-16 2013-05-22 上海富臣化工有限公司 Elastic antifouling aqueous fluorocarbon exterior wall paint

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107118647A (en) * 2017-06-20 2017-09-01 东台市明山石涂料有限公司 A kind of elastic outer wall paint and preparation method thereof
CN115073987A (en) * 2022-07-27 2022-09-20 昆山爱克树脂有限公司 Novel single-layer elastic napping water-based paint

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Application publication date: 20160720

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