CN105777405A - Pesticide and fertilizer mixture containing thiamethoxam and monosultap - Google Patents
Pesticide and fertilizer mixture containing thiamethoxam and monosultap Download PDFInfo
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- CN105777405A CN105777405A CN201610353272.9A CN201610353272A CN105777405A CN 105777405 A CN105777405 A CN 105777405A CN 201610353272 A CN201610353272 A CN 201610353272A CN 105777405 A CN105777405 A CN 105777405A
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- diacloden
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
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Abstract
The invention discloses a pesticide and fertilizer mixture containing thiamethoxam and monosultap. The mixture comprises thiamethoxam and fertilizer. Pesticide and fertilizer granules each comprise three effective component layers from inside to outside. Of the three effective component layers, at least one is wrapped by thiamethoxam, and at least one is wrapped by monosultap. Pesticide granules and fertilizer are mixed into the pesticide and fertilizer mixture, and after a farmer applies the mixture once, the aims of pest preventing, bacteria killing and weeding in advance can be achieved and comprehensive nutrients can be provided for crops.
Description
Technical field
The present invention relates to technical field of pesticide, particularly a kind of medicament-fertilizer mixture containing Diacloden and Cupric sulfate.
Background technology
Medicine fertilizer is to be mixed mutually with fertilizer formula according to a certain percentage by pesticide, and fertilizer and pesticide are stable in specific compound system the novel ecological compound fertilizer formed by certain Technology, generally with the carrier of fertilizer used as pesticides.Medicine fertilizer has the effective ingredient of pesticide and fertilizer concurrently, applied once, the crop needs to N,P,K fertilizers can be met, the insect of harm plant can be killed again simultaneously, thus, two operating procedures that can realize field unite two into one, and this not only saves labour force, and decreases the consumption of time and the energy.
Diacloden is a kind of insecticide in anabasine, the alternative insect CNS nicotinic acetylcholine esterase receptor that suppresses, and then blocks the normal conduction of insect CNS, causes insect to occur during paralysis machine dead.Diacloden not only have tag, stomach toxicity, systemic activity, and there is the features such as fast, the lasting period length of higher activity, better safety, wider array of insecticidal spectrum and speed of action, it is the better kind replacing that those are high to mammalian toxicity, having residual and the organophosphor of environmental problem, carbamate, organochlorine insecticides.
Cupric sulfate is the analog of the nereistoxin of synthetic, enters in insect bodies and is quickly converted to nereistoxin or Dihydronereistoxin element, have stronger tag, stomach toxicity and Uptake and translocation effect, the larva of lepidoptera pest is had good prevention effect.Belong to bionic-type pesticide, natural enemy impact is little, non-resistant, without residual hazard, free from environmental pollution, it is the current comparatively ideal medicament of comprehensive control insect pest.This medicament can prevent and treat the various pests on the crops such as Oryza sativa L., vegetable, wheat, barley and highland barley, Semen Maydis, Folium Camelliae sinensis, fruit tree effectively, particularly rice leaf roller, striped rice borer, yellow rice borer etc. is had specially good effect.
The application for a patent for invention that application publication number is CN105037024A discloses a kind of fertilizer granules containing Cupric sulfate and Diacloden, is made up of the component of following weight percents: Cupric sulfate 1.5%～40%；Diacloden 0.03%～10%；Synergist 0.2%～1%；Fertilizer 20%～35%；Binding agent 6%～10%；Dispersant 6%～10%；Carrier complements to 100%.Pesticide and fertilizer are mixed use by this fertilizer granules thing, make field parasite killing and two operating procedures of nutrient supply unite two into one, and this not only saves labour force, and decreases time and energy resource consumption ability；But pesticide active ingredient has only been carried out one layer of parcel by its preparation technology, and in soil, duration of efficacy is not long, it does not have slow release effect.
Summary of the invention
The invention provides a kind of medicament-fertilizer mixture containing Diacloden and Cupric sulfate, this method can reduce the consumption that makes of pesticide and fertilizer, reduces the pollution to environment, decreases peasant and discharge the number of times of pesticide and fertilizer.
For achieving the above object, the technical scheme is that
A kind of medicament-fertilizer mixture containing Diacloden and Cupric sulfate, including Diacloden and Cupric sulfate, fertilizer and auxiliary material A, described Diacloden and Cupric sulfate make the granular pesticide containing Diacloden and Cupric sulfate, granular pesticide containing Diacloden and Cupric sulfate includes ground floor effective ingredient layer from the inside to the outside, second layer effective ingredient layer and third layer effective ingredient layer, wherein:
In ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, crosslinking agent B 2 ~ 12%, surplus is adjuvant C；
In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, cross-linking agent D3 ~ 15%, surplus is adjuvant E；
In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, binding agent F5 ~ 30%, cross-linking agent G1 ~ 10%, surplus is adjuvant H；
Wherein, ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer have at least one layer to be enclosed with Diacloden, has at least one layer to be enclosed with Cupric sulfate；Auxiliary material A is identical or different with adjuvant C, and adjuvant C is identical from adjuvant E or different, and adjuvant E and adjuvant H is identical or different；Crosslinking agent B adopts high molecular weight water soluble polymer, and cross-linking agent D adopts cellulose or cellulosate, and cross-linking agent D and cross-linking agent G is identical or different.
Preferably, in ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, crosslinking agent B 3.5 ~ 10%, surplus is adjuvant C；
In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, cross-linking agent D5 ~ 11%, surplus is adjuvant E；
In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, binding agent F15 ~ 30%, cross-linking agent G1 ~ 5%, surplus is adjuvant H.
Further, by the gross weight gauge of medicament-fertilizer mixture, it is respectively as follows: the granular pesticide 0.5 ~ 50% containing Diacloden and Cupric sulfate, fertilizer 20 ~ 45% containing the granular pesticide of Diacloden and Cupric sulfate and the percentage by weight of fertilizer.
Further, described fertilizer can select powder or granule, including the one or two or more in nitrogenous fertilizer, phosphate fertilizer and potash fertilizer.Preferably, described fertilizer also includes one or more in micronutrient boron, molybdenum, zinc, copper, manganese, ferrum.Preferably, the part by weight of nitrogenous fertilizer, phosphate fertilizer and potash fertilizer is 10 ~ 40:3 ~ 20:8 ~ 25.
Preferably, described crosslinking agent B is with polyvinylpyrrolidone for the best.
Described cross-linking agent D be preferably in sodium carboxymethyl cellulose, hydroxyethyl cellulose and methylcellulose one or more.
Also being enclosed with protective layer outside described third layer effective ingredient layer, in protective layer, the percentage by weight of each component is: binding agent I3 ~ 4%, cross-linking agent J0.5 ~ 0.8%, pigment 0.01 ~ 0.03%, and surplus is adjuvant K；Wherein, described binding agent I and binding agent F is identical or different, and cross-linking agent J and cross-linking agent G is identical or different, and adjuvant K and adjuvant H is identical or different.
In third layer effective ingredient layer, described cross-linking agent G is Borax, and described binding agent F is the weight ratio of dextrin, dextrin and Borax is 1:0.15.
Above-described auxiliary material A, adjuvant C, adjuvant E, adjuvant H, the customary adjuvant of pesticide is prepared in employing, such as clay, white carbon, zeolite, Kaolin, calcium carbonate, montmorillonite, potter's clay etc..
Above-described binding agent I, it is possible to adopt the one in dextrin, polyamide；Cross-linking agent J, it is possible to adopt the one in Borax, acrylic resin, epoxy resin.
The invention have the benefit that (1) present invention is by adopting different cross-linking agent at different effective ingredient layers, to reach different consolidation effects, promote or regulate the release of Diacloden and Cupric sulfate, reach effect quick-acting, middle and the long-acting effect killing pest and disease damage having both；(2) present invention is aided with the Jacket thickness that different layers is different, regulates the rate of release of Diacloden and Cupric sulfate, helps to realize the sustained release performance of granular pesticide, it is ensured that pesticide activity component can realize release smoothly in the process of plant growth；(3) present invention for the feature of pest and disease damage, as needed in different layer parcel Diaclodens or Cupric sulfate, or can wrap up Diacloden and Cupric sulfate simultaneously, meet the insect protected needs of Different Crop.(4) present invention selects suitable water-soluble cross-linker, without additionally adding organic solvent, surfactant carry out molten in advance, only need to control suitable moisture and temperature can realize the solidification of cross-linking agent, pollute without to soil without organic solvent, surfactant, it is to avoid the phenomenon that soil produces to harden occurs；(4) present invention adopt can the granular pesticide of slow release and fertilizer be mixed and made into medicine fertilizer, peasant household only needs a dispenser, while reaching to shift to an earlier date insect protected, sterilizing, weeding purpose, the demand of comprehensive nutrition also can be provided for crops, thus, decrease medication, use fertile number of times, reduce labor cost；Reduce pesticide and Fertilizer application amount, decrease the pollution to environment.
Detailed description of the invention
The invention provides a kind of medicament-fertilizer mixture containing Diacloden and Cupric sulfate, including Diacloden and Cupric sulfate, fertilizer and auxiliary material A, Diacloden and Cupric sulfate make the granular pesticide containing Diacloden and Cupric sulfate, granular pesticide containing Diacloden and Cupric sulfate includes ground floor effective ingredient layer from the inside to the outside, second layer effective ingredient layer and third layer effective ingredient layer, wherein: in ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, crosslinking agent B 2 ~ 12%, surplus is adjuvant C；In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, cross-linking agent D3 ~ 15%, surplus is adjuvant E；In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, binding agent F5 ~ 30%, cross-linking agent G1 ~ 10%, surplus is adjuvant H；Wherein, ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer have at least one layer to be enclosed with Diacloden, has at least one layer to be enclosed with Cupric sulfate；Auxiliary material A is identical or different with adjuvant C, and adjuvant C is identical from adjuvant E or different, and adjuvant E and adjuvant H is identical or different；Crosslinking agent B adopts high molecular weight water soluble polymer, and cross-linking agent D adopts cellulose or cellulosate, and cross-linking agent D and cross-linking agent G is identical or different.Crosslinking agent B is with polyvinylpyrrolidone for the best.Cross-linking agent D be preferably in sodium carboxymethyl cellulose, hydroxyethyl cellulose and methylcellulose one or more.
The above-mentioned composition being more highly preferred to containing the granular pesticide of Diacloden and Cupric sulfate is that in ground floor effective ingredient layer, each component is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, crosslinking agent B 4 ~ 10%, surplus is adjuvant C at the percentage by weight of ground floor effective ingredient layer；In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, cross-linking agent D5 ~ 11%, surplus is adjuvant E；In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, binding agent F5 ~ 30%, cross-linking agent G1 ~ 5%, surplus is adjuvant H.
Needs according to crop insect protected, sterilizing and weeding and crop alimentary demand, granular pesticide and fertilizer containing Diacloden and Cupric sulfate can do suitable proportioning adjustment, by the gross weight gauge of medicament-fertilizer mixture, it is respectively as follows: the granular pesticide 0.5 ~ 50% containing Diacloden and/or Cupric sulfate, fertilizer 20 ~ 45% containing the granular pesticide of Diacloden and Cupric sulfate and the percentage by weight of fertilizer.
Further, fertilizer can select powder or granule, including the one or two or more in nitrogenous fertilizer, phosphate fertilizer and potash fertilizer.Preferably, described fertilizer also includes one or more in micronutrient boron, molybdenum, zinc, copper, manganese, ferrum.Preferably, the part by weight of nitrogenous fertilizer, phosphate fertilizer and potash fertilizer is 10 ~ 40:3 ~ 20:8 ~ 25.
For better protecting pesticide active ingredient not fall off in packaging and transportation; protective layer also can be enclosed with outside third layer effective ingredient layer; in protective layer, the percentage by weight of each component is: binding agent I3 ~ 4%, cross-linking agent J0.5 ~ 0.8%, pigment 0.01 ~ 0.03%, and surplus is adjuvant K；Wherein, described binding agent I and binding agent F is identical or different, and cross-linking agent J and cross-linking agent G is identical or different, and adjuvant K and adjuvant H is identical or different.
Needs according to cost control and slow release effect, in third layer effective ingredient layer, cross-linking agent G is preferably Borax, and it is 1:0.15 that binding agent F is preferably the weight ratio of dextrin, dextrin and Borax.
Above-described auxiliary material A, adjuvant C, adjuvant E, adjuvant H, the customary adjuvant of pesticide is prepared in employing, such as clay, white carbon, zeolite, Kaolin, calcium carbonate, montmorillonite, potter's clay etc..
Above-described binding agent I, it is possible to adopt the one in dextrin, polyamide；Cross-linking agent J, it is possible to adopt the one in Borax, acrylic resin, epoxy resin.
Presented below more specifically help to understand the present invention containing the specific embodiment of Diacloden and/or the fertilizer granules of Cupric sulfate, but protection scope of the present invention is not limited to following example.
Preparation embodiment 1
Granular pesticide containing Diacloden and Cupric sulfate:
Ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden 1%, polyvinylpyrrolidone 2%, Kaolin and clay surplus；
Second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Cupric sulfate 4%, sodium carboxymethyl cellulose 3.5%, Kaolin and clay surplus；
Third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Cupric sulfate 4%, dextrin 8%, Borax 1.2%, Kaolin, calcium carbonate and clay surplus.
Ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer carry out proportioning by the weight of 1:1:1.
In fertilizer, each component accounts for the percentage by weight of fertilizer and is: ammonium sulfate 20%, ammonium chloride 8%, ammonium dihydrogen phosphate 20%, potassium chloride 32%, ammonium molybdate 0.03%, zinc sulphate heptahydrate 0.09%, copper sulphate pentahydrate 0.03%, carbamide surplus.
Preparation method: (1) is containing the preparation of Diacloden and the fertilizer granules of Cupric sulfate: mixed by the raw material of every layer of effective ingredient layer respectively, then successively solidifies pelletize, it is thus achieved that containing the fertilizer granules of Diacloden and Cupric sulfate with granulating disc.
(2) percentage by weight containing component each in the medicament-fertilizer mixture of Diacloden and Cupric sulfate is: the fertilizer granules 10% containing Diacloden and Cupric sulfate, fertilizer 49%, surplus is Kaolin and clay, by above-mentioned each component mix homogeneously, prepare the medicament-fertilizer mixture containing Diacloden and Cupric sulfate.
Preparation embodiment 2
Granular pesticide containing Diacloden and Cupric sulfate:
Ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden 2%, polyvinylpyrrolidone 3.5%, Kaolin and clay surplus；
Second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden 2%, Cupric sulfate 8%, sodium carboxymethyl cellulose 5%, Kaolin and clay surplus；
Third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Cupric sulfate 8%, dextrin 15%, Borax 2.5%, Kaolin, calcium carbonate and clay surplus.
Ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer carry out proportioning by the weight of 1:2:1.
In fertilizer, each component accounts for the percentage by weight of fertilizer and is: ammonium sulfate 21%, ammonium chloride 7%, ammonium dihydrogen phosphate 20%, potassium chloride 40%, ammonium molybdate 0.03%, zinc sulphate heptahydrate 0.09%, copper sulphate pentahydrate 0.03%, fulvic acid diamidogen ferrum 0.02%, carbamide surplus.
Preparation method: (1) is containing the preparation of Diacloden and/or the fertilizer granules of Cupric sulfate: mixed by the raw material of every layer of effective ingredient layer respectively, then successively solidifies pelletize, it is thus achieved that containing the fertilizer granules of Diacloden and Cupric sulfate with granulating disc.
(2) percentage by weight containing component each in the medicament-fertilizer mixture of Diacloden and Cupric sulfate is: the fertilizer granules 4% containing Diacloden and Cupric sulfate, fertilizer 35%, surplus is Kaolin and clay, by above-mentioned each component mix homogeneously, prepare the medicament-fertilizer mixture containing Diacloden and Cupric sulfate.
Preparation embodiment 3
Granular pesticide containing Diacloden and Cupric sulfate:
Ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Cupric sulfate 20%, polyvinylpyrrolidone 12%, Kaolin and clay surplus；
Second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden 5%, Cupric sulfate 15%, sodium carboxymethyl cellulose 15%, Kaolin and clay surplus；
Third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden 15%, Cupric sulfate 5%, dextrin 30%, Borax 4.5%, Kaolin, calcium carbonate and clay surplus.
Protective layer, each component at the percentage by weight of protective layer is: dextrin 3.5%, Borax 0.55%, pigment 0.02%, Kaolin, clay and calcium carbonate surplus.
Ground floor effective ingredient layer, second layer effective ingredient layer, third layer effective ingredient layer and protective layer carry out proportioning by the weight of 1:2:1:0.02.
In fertilizer, each component accounts for the percentage by weight of fertilizer and is: ammonium sulfate 21%, ammonium chloride 7%, ammonium dihydrogen phosphate 20%, potassium chloride 40%, ammonium molybdate 0.03%, zinc sulphate heptahydrate 0.09%, copper sulphate pentahydrate 0.03%, fulvic acid diamidogen ferrum 0.02%, carbamide surplus.
Preparation method: (1) is containing the preparation of Diacloden and the fertilizer granules of Cupric sulfate: mixed by the raw material of every layer of effective ingredient layer respectively, then successively solidifies pelletize, it is thus achieved that containing the fertilizer granules of Diacloden and/or Cupric sulfate with granulating disc.
(2) percentage by weight containing component each in the medicament-fertilizer mixture of Diacloden and Cupric sulfate is: the fertilizer granules 5% containing Diacloden and Cupric sulfate, fertilizer 45%, surplus is Kaolin and clay, by above-mentioned each component mix homogeneously, prepare the medicament-fertilizer mixture containing Diacloden and/or Cupric sulfate.
Preparation embodiment 4
Granular pesticide containing Diacloden and Cupric sulfate:
Ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden 2%, Cupric sulfate 9%, polyvinylpyrrolidone 6%, Kaolin and clay surplus；
Second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden 3%, Cupric sulfate 9%, sodium carboxymethyl cellulose 8%, Kaolin and clay surplus；
Third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden 4%, Cupric sulfate 9%, dextrin 24%, Borax 3.6%, Kaolin, calcium carbonate and clay surplus.
Protective layer, each component at the percentage by weight of protective layer is: dextrin 4%, Borax 0.6%, pigment 0.01%, Kaolin, clay and calcium carbonate surplus.
Ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer carry out proportioning by the weight of 1:1:1:0.02.
In fertilizer, each component accounts for the percentage by weight of fertilizer and is: ammonium sulfate 20%, ammonium chloride 8%, ammonium dihydrogen phosphate 20%, potassium chloride 32%, ammonium molybdate 0.03%, zinc sulphate heptahydrate 0.09%, copper sulphate pentahydrate 0.03%, carbamide surplus.
Preparation method: (1) is containing the preparation of Diacloden and the fertilizer granules of Cupric sulfate: mixed by the raw material of every layer of effective ingredient layer respectively, then successively solidifies pelletize, it is thus achieved that containing the fertilizer granules of Diacloden and/or Cupric sulfate with granulating disc.
(2) percentage by weight containing component each in the medicament-fertilizer mixture of Diacloden and Cupric sulfate is: the fertilizer granules 5% containing Diacloden and/or Cupric sulfate, fertilizer 45%, surplus is Kaolin and clay, by above-mentioned each component mix homogeneously, prepare the medicament-fertilizer mixture containing Diacloden and/or Cupric sulfate.
Preparation embodiment 5
Granular pesticide containing Diacloden and Cupric sulfate:
Ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden 1.2%, Cupric sulfate 3.6%, polyvinylpyrrolidone 3%, Kaolin and clay surplus；
Second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden 1.2%, Cupric sulfate 3.6%, sodium carboxymethyl cellulose 3.5%, Kaolin and clay surplus；
Third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden 1.2%, Cupric sulfate 3.6%, dextrin 21%, Borax 3.15%, Kaolin, calcium carbonate and clay surplus.
Ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer carry out proportioning by the weight of 1:2:2.
In fertilizer, each component accounts for the percentage by weight of fertilizer and is: ammonium sulfate 18%, ammonium chloride 7%, ammonium dihydrogen phosphate 20%, potassium chloride 50%, ammonium molybdate 0.03%, zinc sulphate heptahydrate 0.09%, copper sulphate pentahydrate 0.03%, fulvic acid diamidogen ferrum 0.02%, carbamide surplus.
Preparation method: (1) is containing the preparation of Diacloden and the fertilizer granules of Cupric sulfate: mixed by the raw material of every layer of effective ingredient layer respectively, then successively solidifies pelletize, it is thus achieved that containing the fertilizer granules of Diacloden and Cupric sulfate with granulating disc.
(2) percentage by weight containing component each in the medicament-fertilizer mixture of Diacloden and Cupric sulfate is: the fertilizer granules 10% containing Diacloden and Cupric sulfate, fertilizer 45%, surplus is Kaolin and clay, by above-mentioned each component mix homogeneously, prepare the medicament-fertilizer mixture containing Diacloden and Cupric sulfate.
Drug effect checking embodiment
The fertilizer granules containing Diacloden and Cupric sulfate of the embodiment of the present invention 1,2,3,4,5 preparation is used by the method described below:
Select embodiment 1 ~ 5, according to unified cost budgeting consumption, sow in experimental plot, somewhere, Rongshui Guangxi county, fertilizer granules is spread fertilizer over the fields before rice growing, experimental plot randomly chooses, in 60 days, 90 days, within 120 days, investigate the prevention effect of aphid, snout moths larva respectively, and when results the growing state of checking Oryza sativa L..Test sets three repetitions (i.e. three pieces of experimental plots), and aphid, snout moths larva prevention effect are in Table 1, and Oryza sativa L. mature condition is in Table 2.
From the testing result of upper table, the fertilizer granules containing Diacloden and Cupric sulfate of the present invention has good aphid, a snout moths larva prevention effect, and can effectively facilitate increasing production of rice and increase income.
Claims (10)
1. containing a medicament-fertilizer mixture for Diacloden and Cupric sulfate, including Diacloden and Cupric sulfate, fertilizer and auxiliary material A, it is characterised in that:
Described Diacloden and Cupric sulfate make the granular pesticide containing Diacloden and Cupric sulfate, and the granular pesticide containing Diacloden and Cupric sulfate includes ground floor effective ingredient layer from the inside to the outside, second layer effective ingredient layer and third layer effective ingredient layer, wherein:
In ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, crosslinking agent B 2 ~ 12%, surplus is adjuvant C；
In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, cross-linking agent D3 ~ 15%, surplus is adjuvant E；
In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 0.15 ~ 20%, binding agent F5 ~ 30%, cross-linking agent G1 ~ 10%, surplus is adjuvant H；
Wherein, ground floor effective ingredient layer, second layer effective ingredient layer and third layer effective ingredient layer have at least one layer to be enclosed with Diacloden, has at least one layer to be enclosed with Cupric sulfate；Auxiliary material A is identical or different with adjuvant C, and adjuvant C is identical from adjuvant E or different, and adjuvant E and adjuvant H is identical or different；Crosslinking agent B adopts high molecular weight water soluble polymer, and cross-linking agent D adopts cellulose or cellulosate, and cross-linking agent D and cross-linking agent G is identical or different.
2. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1, it is characterised in that:
In ground floor effective ingredient layer, each component at the percentage by weight of ground floor effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, crosslinking agent B 3.5 ~ 10%, surplus is adjuvant C；
In second layer effective ingredient layer, each component at the percentage by weight of second layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, cross-linking agent D5 ~ 11%, surplus is adjuvant E；
In third layer effective ingredient layer, each component at the percentage by weight of third layer effective ingredient layer is: Diacloden and/or Cupric sulfate 4.8 ~ 10%, binding agent F15 ~ 30%, cross-linking agent G1 ~ 5%, surplus is adjuvant H.
3. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 and 2, it is characterised in that:
By the gross weight gauge of medicament-fertilizer mixture, it is respectively as follows: the granular pesticide 0.5 ~ 50% containing Diacloden and Cupric sulfate, fertilizer 20 ~ 45% containing the granular pesticide of Diacloden and Cupric sulfate and the percentage by weight of fertilizer.
4. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 and 2, it is characterised in that:
Described fertilizer is powder or granule, including the one or two or more in nitrogenous fertilizer, phosphate fertilizer and potash fertilizer.
5. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 or 4, it is characterised in that:
In described fertilizer, the part by weight of nitrogenous fertilizer, phosphate fertilizer and potash fertilizer is 10 ~ 40:3 ~ 20:8 ~ 25.
6. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 and 2, it is characterised in that:
Described crosslinking agent B is polyvinylpyrrolidone.
7. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 6, it is characterised in that:
Described cross-linking agent D is one or more in sodium carboxymethyl cellulose, hydroxyethyl cellulose and methylcellulose.
8. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 and 2, it is characterised in that:
Also being enclosed with protective layer outside described third layer effective ingredient layer, in protective layer, the percentage by weight of each component is: binding agent I3 ~ 4%, cross-linking agent J0.5 ~ 0.8%, pigment 0.01 ~ 0.03%, and surplus is adjuvant K；Wherein, described binding agent I and binding agent F is identical or different, and cross-linking agent J and cross-linking agent G is identical or different, and adjuvant K and adjuvant H is identical or different.
9. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 1 and 2, it is characterised in that:
In third layer effective ingredient layer, described cross-linking agent G is Borax, and described binding agent F is the weight ratio of dextrin, dextrin and Borax is 1:0.15.
10. the medicament-fertilizer mixture containing Diacloden and Cupric sulfate according to claim 4, it is characterised in that:
Described fertilizer also includes one or more in micronutrient boron, molybdenum, zinc, copper, manganese, ferrum.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610353272.9A CN105777405A (en) | 2016-05-25 | 2016-05-25 | Pesticide and fertilizer mixture containing thiamethoxam and monosultap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610353272.9A CN105777405A (en) | 2016-05-25 | 2016-05-25 | Pesticide and fertilizer mixture containing thiamethoxam and monosultap |
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| Publication Number | Publication Date |
|---|---|
| CN105777405A true CN105777405A (en) | 2016-07-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610353272.9A Pending CN105777405A (en) | 2016-05-25 | 2016-05-25 | Pesticide and fertilizer mixture containing thiamethoxam and monosultap |
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| Country | Link |
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| CN (1) | CN105777405A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107628898A (en) * | 2017-09-27 | 2018-01-26 | 广西南宁桂尔创环保科技有限公司 | One kind is containing Diacloden preventing and treating pest and disease damage new drug fertilizer and preparation method thereof |
| CN111454092A (en) * | 2020-05-13 | 2020-07-28 | 河南好年景生物发展有限公司 | Broad-spectrum intelligent controlled-release pesticide fertilizer granule and preparation method and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102696587A (en) * | 2012-06-15 | 2012-10-03 | 河南好年景生物发展有限公司 | Compound controlled-release granular pesticide preparation and preparation method thereof |
| CN102805097A (en) * | 2012-08-13 | 2012-12-05 | 广西汇丰生物科技有限公司 | Granules containing monosultap and thiamethoxam |
| CN105037024A (en) * | 2015-07-09 | 2015-11-11 | 广西兄弟农药厂(普通合伙) | Pesticide-fertilizer granules containing Monosultap and Thiamethoxam |
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2016
- 2016-05-25 CN CN201610353272.9A patent/CN105777405A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102696587A (en) * | 2012-06-15 | 2012-10-03 | 河南好年景生物发展有限公司 | Compound controlled-release granular pesticide preparation and preparation method thereof |
| CN102805097A (en) * | 2012-08-13 | 2012-12-05 | 广西汇丰生物科技有限公司 | Granules containing monosultap and thiamethoxam |
| CN105037024A (en) * | 2015-07-09 | 2015-11-11 | 广西兄弟农药厂(普通合伙) | Pesticide-fertilizer granules containing Monosultap and Thiamethoxam |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107628898A (en) * | 2017-09-27 | 2018-01-26 | 广西南宁桂尔创环保科技有限公司 | One kind is containing Diacloden preventing and treating pest and disease damage new drug fertilizer and preparation method thereof |
| CN111454092A (en) * | 2020-05-13 | 2020-07-28 | 河南好年景生物发展有限公司 | Broad-spectrum intelligent controlled-release pesticide fertilizer granule and preparation method and application thereof |
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Application publication date: 20160720 |