CN105768113B - A kind of production method of sugar-free naked oats dietary fiber chewable tablets - Google Patents

A kind of production method of sugar-free naked oats dietary fiber chewable tablets Download PDF

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CN105768113B
CN105768113B CN201610141665.3A CN201610141665A CN105768113B CN 105768113 B CN105768113 B CN 105768113B CN 201610141665 A CN201610141665 A CN 201610141665A CN 105768113 B CN105768113 B CN 105768113B
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naked oats
sugar
added
dietary fiber
chewable tablets
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CN105768113A (en
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周新虎
陈翔
刘海波
张春林
孔小勇
戴源
朱超
段占峰
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Jiangsu Yanghe Brewery JSCL
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/14Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/04Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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Abstract

The invention discloses a kind of production methods of sugar-free naked oats dietary fiber chewable tablets, belong to wine brewing comprehensive utilization of resources field.The method of the present invention includes selection, gelatinization, liquefaction, saccharification, fermentation, alcohol precipitation, neutralization, centrifugation, addition the auxiliary material mixing, granulation, drying, tabletting, packed products step of raw material.It is different from the chewable tablets of starch-containing carbohydrate, has sugar-free, high microsteping, high nutrition, health care in one by the chewable tablets that above-mentioned technique is brewed out, there is typical naked oats faint scent, sweet and sour taste, good physics chewing mouthfeel.Simultaneously as the proper amount of edible chewable tablets has weight-reducing, reduces blood lipid, hypoglycemic, norcholesterol and prevents cardiovascular disease, raising immunocompetence has preferable health-care effect containing plurality kinds of health care beneficiating ingredient.

Description

A kind of production method of sugar-free naked oats dietary fiber chewable tablets
Technical field
The present invention relates to a kind of production methods of sugar-free naked oats dietary fiber chewable tablets, belong to wine brewing comprehensive utilization of resources neck Domain.
Background technique
Naked oats are also known as naked oats, a kind of low sugar, high nutrition, high energy food.Protein content average out to 15.6%, 8 kinds of ammonia Base acid composition relatively balances, and lysine content is higher than rice and wheat flour, beta glucan content 3.2%~6.8%, fat content It is higher, 5.5 times of rice, wherein 40% is unsaturated oleic acid.Beta glucan, have good effect of weight reducing, reduce blood lipid, Reduce blood glucose, reduce cholesterol and prevent cardiovascular disease, improve immunocompetence etc. suffers from outstanding performance.Utilize oats Wheat prepares sugar-free naked oats diet fiber product with certain market prospects.
China's sugarfree foods be often referred to without containing white sugar, glucose, maltose, fructose, fructose syrup food, do not limit The content of starch of glucose can be converted into human body, but then to define sugarfree foods not starch-containing in Europe.It has been reported and uses The mixed bacteria of bud short stalk enzyme and the new mushroom of tea directly utilizes starch and protein in wheat bran, is prepared for a kind of dietary fiber.However, Content of starch about 10% in wheat bran, content are difficult using the method for strain fermentation far below the starch 65%-70% in naked oats To realize that decomposition or the fermentation period of high content of starch greatly extend, make being difficult to control for quality.
Summary of the invention
In order to overcome the above problem, the present invention provides a kind of production method of sugar-free naked oats dietary fiber chewable tablets, systems Containing the nutriment in naked oats in standby obtained product, dietary fiber, protein, beta glucan retain the nutrition guarantor of naked oats Strong substance, and its unique composite flavor.
The method is using naked oats as primary raw material, and raw material is added yeast and carries out liquid hair after crushing, gelatinization, saccharification Ferment removes sugar with converted starch to decompose, and it is former then to obtain the sugar-free dietary fiber in naked oats through alcohol precipitation, neutralization, centrifugal method Material, then mixed with auxiliary material, through granulation, drying, tabletting, sterilizing is made sugar-free naked oats dietary fiber chewable tablets.
In one embodiment of the invention, which comprises
(1) it crushes: using naked oats as raw material, cleaned, immersion, using wet pulverizing slurrying, material-water ratio 1:4~1:6;
(2) be gelatinized: Thermostable α-Amylase, enzyme activity 30000U/g, usage amount 0.2g/kg- is added in the slurry crushed 0.33g/kg is gelatinized 90min in 95~105 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 U/g of enzyme activity is added, and usage amount is 0.67g/kg-2g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast, usage amount 2.5g/kg-5g/kg is added Fermentation to alcoholic strength is 5-7%vol;
(5) alcohol precipitation: fermentation liquid adds alcohol, makes alcoholic strength 20%vol or so, is uniformly mixed, and precipitates 12h or more, supernatant Liquid is collected as naked oats wine, and sedimentary is dietary fibre materials.
(6) neutralize: calcium carbonate is added in sedimentary, mixes, and neutralizes the organic acid that fermentation process generates;
(7) be centrifuged: centrifugation obtains naked oats dietary fibre materials;
(8) mixing of dietary fiber and auxiliary material: dehydration carrot meal, dehydration spinach powder and naked oats dietary fibre materials are mixed It closes, sweetener, adhesive is added;
(9) be granulated and dry: material mixing is finished and is granulated in waving in pelletizer, is sieved, dry;
(10) tabletting and sterilizing: particle tabletting in tablet press machine sterilizes, as finished product then at far-infrared baking oven.
In one embodiment of the invention, the immersion of the step (1) is to impregnate 2h.
In one embodiment of the invention, the yeast fermentation time of the step (4) is 96h.
In one embodiment of the invention, the yeast of the step (4) is Angel Yeast powder.
In one embodiment of the invention, the additive amount of the calcium carbonate of the step (6) is relative to sedimentary amount 0.05%.
In one embodiment of the invention, supplementary product kind and additive amount in the step (8) are as follows: with dietary fiber weight Amount is 100% meter, and xylitol 5%-8%, carboxymethyl cellulose 0.3%-0.5%, Arabic gum 0.4%-0.5%, dehydration are recklessly Carrot powder 4%-7%, dehydration spinach powder 3%-5%, citric acid 0.2%-0.3%.
In one embodiment of the invention, the step (9) was 5 meshes, in an oven 60 DEG C drying one hour.
In one embodiment of the invention, the step (10) is in 110 DEG C of sterilizing 10min of far-infrared baking oven.
The present invention also provides a kind of preparation method of sugar-free naked oats dietary fiber, this method is to utilize above-mentioned steps (1) extremely Step (7).
Sugar-free naked oats dietary fiber chewable tablets of the invention meet stringent sugarfree foods requirement, and have nutrition and health care function Can, have certain market prospects, while being related to the comprehensive utilization of naked oats wine brewing resource.The sugar-free technique of chewable tablets passes through naked oats liquid State biofermentation eliminates starch, the method for alcohol precipitation, which remains in naked oats, largely seeks while so that starch is switched to ethyl alcohol wine brewing Health care material is supported, such as cellulose, protein, beta glucan.The intake of dietary fiber, which facilitates human body, reduces cholesterol, the prevention heart Vascular diseases have effect well.Ferment the lactic acid of generation in chewable tablets, improves mouthfeel to neutralize acidity, contains one in chewable tablets Quantitative calcium lactate, also functions to calcium supplementing effect.It is added to dehydrated vegetables carrot, spinach simultaneously, makes the more battalion of chewable tablets addition It forms point and comfortable taste degree.
It has the advantage that
1, wine brewing comprehensive utilization of resources, for naked oats by liquid state fermentation, clear liquid is naked oats wine, insoluble alcohol precipitation nutrition and health care object Matter is dietary fibre materials.
2, by the specificity using alpha amylase, decomposing alpha starch makes cellulose in naked oats, hemicellulose, lignin, egg White matter, beta glucan several functions composition are able to retain and extract.
3, not content glucose, maltose, starchy carbohydrate ingredient in the chewing flake products, with practical significance without confectionery Product.
4, by addition calcium carbonate, so that lactic acid in fermentation is switched to calcium lactate, reduce the mouthfeel of lactic acid, while adding lemon Acid keeps tart flavour moderate, preferable compound mouthfeel.
5, by addition xylitol, Arabic gum, dehydration carrot meal, dehydration spinach powder, increase its nutritional ingredient, together Shi Tiandu is palatable, and physics chewing mouthfeel is good.
Specific embodiment
Technical solution of the invention is further illustrated combined with specific embodiments below, these embodiments should not be understood as It is the limitation to technical solution.
Embodiment 1: sugar-free naked oats dietary fiber chewable tablets are prepared as follows
(1) it crushes: using naked oats as raw material, cleaned, immersion 2h, using wet pulverizing slurrying, material-water ratio 1:4;
(2) it is gelatinized: the slurry crushed, addition Thermostable α-Amylase, enzyme activity 30000u/g, usage amount 0.2g/kg, 90min is gelatinized in 105 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 u/g of enzyme activity is added, and usage amount is 2g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast is added, and usage amount is 2.5g/kg fermentation 96h, fermentation finish, and alcoholic strength is about 7%vol;
(5) alcohol precipitation: fermentation liquid adds alcohol, makes alcoholic strength 20%vol, is uniformly mixed, and precipitates 12h or more, supernatant Siphon is collected as naked oats wine, and sedimentary is dietary fibre materials;
(6) neutralize: 0.05% calcium carbonate of sedimentary amount is added in sedimentary, mixes, and neutralizes the part that fermentation process generates Organic acid lactic acid;
(7) it is centrifuged: naked oats dietary fibre materials is obtained using centrifuge;
(8) mixing of dietary fiber and auxiliary material: xylitol 5%, Arabic gum 0.4%, takes off carboxymethyl cellulose 0.3% Water carrot meal 4%, dehydration spinach powder 3%, citric acid 0.2% mix in mixing machine with naked oats dietary fiber;
(9) be granulated and dry: material mixing is finished and is granulated in waving in pelletizer, crosses 5 meshes.60 DEG C of dryings in baking oven again One hour;
(10) tabletting and sterilizing: particle tabletting in tablet press machine, then at 110 DEG C of sterilizing 10min of far-infrared baking oven;As at Product.
Organoleptic detection: product is brown brown, and appearance rounding is smooth, and color is uniform, neat in edge;Mouthfeel is fine and glossy, and acidity can Mouthful, light sweet tea, entrance is smooth, free from extraneous odour.Physico-chemical tests: slice weight 0.6g ± 3%, moisture≤3%, friability≤1%, cellulose >= 450mg/ piece, protein >=20mg/ piece, beta glucan >=20mg/ piece, calcium >=60mg/ piece.Starch 0mg/ piece, reduced sugar 0mg/ Piece.
Embodiment 2: sugar-free naked oats dietary fiber chewable tablets are prepared as follows
(1) it crushes: using naked oats as raw material, cleaned, immersion 2h, using wet pulverizing slurrying, material-water ratio 1:5;
(2) be gelatinized: Thermostable α-Amylase, enzyme activity 30000u/g, usage amount 0.33g/kg is added in the slurry crushed 90min is gelatinized in 100 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 u/g of enzyme activity is added, and usage amount is 0.67g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast is added, and usage amount is 5g/kg fermentation 96h, Fermentation finishes, and alcoholic strength is about 6%vol;
(5) alcohol precipitation: fermentation liquid adds alcohol, makes alcoholic strength 30%vol, is uniformly mixed, and precipitates 12h or more, supernatant Siphon is collected as naked oats wine, and sedimentary is dietary fibre materials;
(6) neutralize: 0.05% calcium carbonate of sedimentary amount is added in sedimentary, mixes, and neutralizes the part that fermentation process generates Organic acid lactic acid;
(7) it is centrifuged: naked oats dietary fibre materials is obtained using centrifuge;
(8) mixing of dietary fiber and auxiliary material: xylitol 7%, Arabic gum 0.4%, takes off carboxymethyl cellulose 0.4% Water carrot meal 5%, dehydration spinach powder 4%, citric acid 0.2% mix in mixing machine with naked oats dietary fiber;
(9) be granulated and dry: material mixing is finished and is granulated in waving in pelletizer, crosses 5 meshes;60 DEG C of dryings in baking oven again One hour.
(10) tabletting and sterilizing: particle tabletting in tablet press machine, then at 110 DEG C of sterilizing 10min of far-infrared baking oven, packaging is For finished product.
Organoleptic detection: product is brown brown, and appearance rounding is smooth, and color is uniform, neat in edge;Mouthfeel is fine and glossy, and acidity can Mouthful, light sweet tea, entrance is smooth, free from extraneous odour.Physico-chemical tests: slice weight 0.6g ± 3%, moisture≤3%, friability≤1%, cellulose >= 480mg/ piece, protein >=20mg/ piece, beta glucan >=23mg/ piece, calcium >=60mg/ piece, starch 0mg/ piece, reduced sugar 0mg/ Piece.
Embodiment 3: sugar-free naked oats dietary fiber chewable tablets are prepared as follows
(1) it crushes: using naked oats as raw material, cleaned, immersion 2h, using wet pulverizing slurrying, material-water ratio 1:6;
(2) be gelatinized: alpha-amylase amylase, enzyme activity 30000u/g, usage amount 0.25g/ is added in the slurry crushed Kg is gelatinized 90min in 105 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 u/g of enzyme activity is added, and usage amount is 1.5g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast is added, and usage amount 3g/kg, ferment 96h, Fermentation finishes, and alcoholic strength is about 5%vol;
(5) alcohol precipitation: fermentation liquid adds alcohol, and alcoholic strength is made to be greater than 40%vol, is uniformly mixed, and precipitates 12h or more, supernatant Liquid siphon is collected as naked oats wine, and sedimentary is dietary fibre materials;
(6) neutralize: 0.05% calcium carbonate of sedimentary amount is added in sedimentary, mixes, and neutralizes the part that fermentation process generates Organic acid lactic acid;
(7) it is centrifuged: naked oats dietary fibre materials is obtained using centrifuge;
(8) mixing of dietary fiber and auxiliary material: xylitol 8%, Arabic gum 0.5%, takes off carboxymethyl cellulose 0.5% Water carrot meal 7%, dehydration spinach powder 5%, citric acid 0.3% mix in mixing machine with naked oats dietary fiber;
(9) be granulated and dry: material mixing is finished and is granulated in waving in pelletizer, crosses 5 meshes, then 60 DEG C of dryings in baking oven One hour;
(10) tabletting and sterilizing: particle tabletting in tablet press machine, then at 110 DEG C of sterilizing 10min of far-infrared baking oven, packaging is For finished product.
Organoleptic detection: product is brown brown, and appearance rounding is smooth, and color is uniform, neat in edge;Mouthfeel is fine and glossy, and acidity can Mouthful, light sweet tea, entrance is smooth, free from extraneous odour.Physico-chemical tests: slice weight 0.6g ± 3%, moisture≤3%, friability≤1%, cellulose >= 500mg/ piece, protein >=20mg/ piece, beta glucan >=25mg/ piece, calcium >=60mg/ piece, starch 0mg/ piece, reduced sugar 0mg/ Piece.
Although the present invention has been described by way of example and in terms of the preferred embodiments, it is not intended to limit the invention, any to be familiar with this skill The people of art can do various change and modification, therefore protection model of the invention without departing from the spirit and scope of the present invention Enclosing subject to the definition of the claims.

Claims (7)

1. a kind of preparation method of sugar-free naked oats dietary fiber chewable tablets, which is characterized in that it is main that the method, which is with naked oats, Raw material, raw material are added yeast progress liquid state fermentation to decompose and remove sugar with converted starch, then after crushing, gelatinization, saccharification The sugar-free dietary fiber raw material in naked oats is obtained through alcohol precipitation, neutralization, centrifugal method, then is mixed with auxiliary material, through granulation, drying, pressure Piece, sterilizing is made sugar-free naked oats dietary fiber chewable tablets;
The method is specifically:
(1) it crushes: using naked oats as raw material, cleaned, immersion, using wet pulverizing slurrying, material-water ratio 1:4~1:6;
(2) be gelatinized: Thermostable α-Amylase, enzyme activity 30000U/g, usage amount 0.2g/kg- is added in the slurry crushed 0.33g/kg is gelatinized 90min in 95~105 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 U/g of enzyme activity is added, and usage amount is 0.67g/kg-2g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast fermentation, usage amount 2.5g/kg-5g/kg is added It is 5-7%vol to alcoholic strength;
(5) alcohol precipitation: fermentation liquid adds alcohol, makes alcoholic strength 20%vol or so, is uniformly mixed, and precipitates 12h or more, and supernatant is received Integrate as naked oats wine, sedimentary is dietary fibre materials;
(6) neutralize: calcium carbonate is added in sedimentary, mixes, and neutralizes the organic acid that fermentation process generates;
(7) be centrifuged: centrifugation obtains naked oats dietary fibre materials;
(8) mixing of dietary fiber and auxiliary material: dehydration carrot meal, dehydration spinach powder are mixed with naked oats dietary fibre materials, added Enter sweetener, adhesive;
(9) be granulated and dry: material mixing is finished and is granulated in waving in pelletizer, is sieved, dry;
(10) tabletting and sterilizing: particle tabletting in tablet press machine sterilizes, as sugar-free naked oats dietary fiber then at far-infrared baking oven Chewable tablets.
2. the method according to claim 1, wherein the yeast fermentation time of the step (4) is 96h.
3. the method according to claim 1, wherein the additive amount of the calcium carbonate of the step (6) be relative to The 0.05% of sedimentary amount.
4. the method according to claim 1, wherein supplementary product kind and additive amount in the step (8) are as follows: with meals Eating fibre weight is 100% meter, xylitol 5%-8%, carboxymethyl cellulose 0.3%-0.5%, Arabic gum 0.4%- 0.5%, carrot meal 4%-7%, dehydration spinach powder 3%-5%, citric acid 0.2%-0.3% are dehydrated.
5. being done for 60 DEG C in an oven the method according to claim 1, wherein the step (9) was 5 meshes Dry one hour.
6. the method according to claim 1, wherein the step (10) is sterilized in 110 DEG C of far-infrared baking oven 10min。
7. a kind of method for preparing sugar-free naked oats dietary fiber, which is characterized in that the method is:
(1) it crushes: using naked oats as raw material, cleaned, immersion, using wet pulverizing slurrying, material-water ratio 1:4~1:6;
(2) be gelatinized: Thermostable α-Amylase, enzyme activity 30000U/g, usage amount 0.2g/kg- is added in the slurry crushed 0.33g/kg is gelatinized 90min in 95~105 DEG C of high temperature;
(3) be saccharified: the slurry that will be gelatinized is cooled to 60 DEG C of constant temperature, and carbohydrase, 150,000 U/g of enzyme activity is added, and usage amount is 0.67g/kg-2g/kg, be saccharified 30min;
(4) ferment: the slurry that will be saccharified is cooled to 30 DEG C of constant temperature, and yeast fermentation, usage amount 2.5g/kg-5g/kg is added It is 4-6%vol to alcoholic strength;
(5) alcohol precipitation: fermentation liquid adds alcohol, makes alcoholic strength 20%vol or so, is uniformly mixed, and precipitates 12h or more, and supernatant is received Integrate as naked oats wine, sedimentary is dietary fibre materials;
(6) neutralize: calcium carbonate is added in sedimentary, mixes, and neutralizes the organic acid that fermentation process generates;
(7) be centrifuged: centrifugation obtains sugar-free naked oats dietary fiber.
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CN111184212A (en) * 2020-01-13 2020-05-22 珲春华瑞参业生物工程股份有限公司 Preparation method of ginseng polysaccharide tablet
CN113973963A (en) * 2021-10-27 2022-01-28 上海圣岳生物科技有限公司 Tabletting candy for promoting synthesis of human collagen and preparation method thereof

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