CN105753756A - Allicin-processing technology - Google Patents
Allicin-processing technology Download PDFInfo
- Publication number
- CN105753756A CN105753756A CN201410786333.1A CN201410786333A CN105753756A CN 105753756 A CN105753756 A CN 105753756A CN 201410786333 A CN201410786333 A CN 201410786333A CN 105753756 A CN105753756 A CN 105753756A
- Authority
- CN
- China
- Prior art keywords
- bulbus allii
- garlicin
- supercritical
- extraction
- allicin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
The invention relates to allicin-processing technology. The technology specifically comprises the following steps: (1) material preparation; (2) pulverization and drying; (3) grinding, in which, materials are ground into powder through a grinder and are sieved through an 80-100 mesh sieve; (4) soaking for deodorization; and (5) separation. Supercritical CO2 fluid extraction technology is also adopted, and allicin is purified through ethanol leaching combined with supercritical CO2 purification. Advantages of the two methods are kept, and weaknesses are overcome. Therefore, allicin is purified through continuous supercritical CO2 extraction. Through adoption of allicin, production ability of livestock and fishes is obviously improved, the incidence rate and the mortality are reduced, and the culture benefit is increased. The allicin can replace part of antibiotics, so that drug-resistance developed by microorganisms is reduced. The allicin produces beneficial effects on health of livestock and fish. The addition of allicin into feed is a method for overcoming the problem in antibiotics. The technology is simple and useful, and can meet requirements of people's life and sterilization.
Description
Technical field
The present invention relates to the process technology of a kind of garlicin, belong to food processing technology field.
Background technology
Garlicin is the volatility grease extracted from the spherical bulb of Bulbus Allii, it it is the mixture of diallyl trisulfide, diallyl disulfide and methallyl based bisulfide etc., pathogenic microorganism is had stronger suppression and killing action by trisulfide therein, and disulphide also has certain antibacterial and bactericidal action.
Summary of the invention
It is an object of the invention to provide the process technology of a kind of garlicin, in order to prepare satisfactory garlicin better, improve the living standard of people.
To achieve these goals, technical scheme is as follows.
The process technology of a kind of garlicin, specifically includes following steps:
(1) get the raw materials ready.Hank ripe, dry, free from insect pests, without the Bulbus Allii gone rotten, stalk, point lobe, stripping underwear, rinse with clear water, remove impurity and undesirable set of garlic tablet.
(2) broken, drying.With pulverizer, garlic tablet is processed into pasty state.Being stuck with paste by Bulbus Allii and put into baking oven, dry with slow fire, temperature controls at 60～65 DEG C, dries 6～8 hours, within every 2 hours, stirs 1 time, makes Bulbus Allii stick with paste and is heated evenly.
(3) pulverizing: use pulverizer grinds, crosses 80～100 mesh sieves.
(4) deodorization is soaked.It is 1:3 that Bulbus Allii powder puts into 30～40 DEG C of wine sealing immersion deodorization in 6 hours (Bulbus Allii powder and wine) ratios.
(5) separate.Adopt suction method, the solution on upper strata is taken out, is deodorised allicin stock solution.
Supercritical CO can also be adopted2Fluid extraction technology, adopts ethanol to leach and supercritical CO2Purify the Methods For Purification garlicin that combines, maintain both original strong points and avoided their weakness, it is possible to achieve the supercritical CO of garlicin2Continuous extraction purification operations.Technology is as follows:
(1) ethanol extraction Bulbus Allii liquid.Bulbus Allii head peeling, section, soak with ethanol, isolate ethanol Bulbus Allii liquid, as the raw material of SCF-CO 2.Ethanol Bulbus Allii liquid is containing 1.2～2.2mg garlicin/ml.
(2) supercritical CO2Purify garlicin.Ethanol Bulbus Allii liquid is added extraction kettle by liquid pump, from the CO of steel cylinder2It is pumped to extraction kettle by high pressure measurement and extracts garlicin, then sequentially through one-level pressure relief valve, flash vaporization kettle, second depressurized valve, reclaim CO2, extract after terminating, from extraction kettle and flash vaporization kettle, take out raffinate and garlicin respectively.Adopt alcohol steep and supercritical CO2The technology that extraction phase combines extracts garlicin, and extraction ratio can reach more than 92%, and garlicin purity reaches 84%, suitable with fresh Bulbus Allii juice, therefore, adopts supercritical CO2Extraction process can make extract keep the original fresh flavor of Bulbus Allii and medicinal component.
This beneficial effect of the invention is in that: garlicin can significantly improve production performance, reduces sickness rate, reduces mortality rate, increases culture benefit；Can part substitute antibiotics, thus reducing the Drug resistance that microorganism produces, the health of herding Fish is produced wholesome effect, adding garlicin in feedstuff can as the approach solving antibiotic problem.The technology of the present invention uses simple and practical, can meet life and the sterilization demand of people.
Detailed description of the invention
Below in conjunction with embodiment, the specific embodiment of the present invention is described, in order to be better understood from the present invention.
Embodiment
The process technology of a kind of garlicin, specifically includes following steps:
(1) get the raw materials ready.Hank ripe, dry, free from insect pests, without the Bulbus Allii gone rotten, stalk, point lobe, stripping underwear, rinse with clear water, remove impurity and undesirable set of garlic tablet.
(2) broken, drying.With pulverizer, garlic tablet is processed into pasty state.Being stuck with paste by Bulbus Allii and put into baking oven, dry with slow fire, temperature controls at 60～65 DEG C, dries 6～8 hours, within every 2 hours, stirs 1 time, makes Bulbus Allii stick with paste and is heated evenly.
(3) pulverizing: use pulverizer grinds, crosses 80～100 mesh sieves.
(4) deodorization is soaked.It is 1:3 that Bulbus Allii powder puts into 30～40 DEG C of wine sealing immersion deodorization in 6 hours (Bulbus Allii powder and wine) ratios.
(5) separate.Adopt suction method, the solution on upper strata is taken out, is deodorised allicin stock solution.
Supercritical CO can also be adopted2Fluid extraction technology, adopts ethanol to leach and supercritical CO2Purify the Methods For Purification garlicin that combines, maintain both original strong points and avoided their weakness, it is possible to achieve the supercritical CO of garlicin2Continuous extraction purification operations.Technology is as follows:
(1) ethanol extraction Bulbus Allii liquid.Bulbus Allii head peeling, section, soak with ethanol, isolate ethanol Bulbus Allii liquid, as the raw material of SCF-CO 2.Ethanol Bulbus Allii liquid is containing 1.2～2.2mg garlicin/ml.
(2) supercritical CO2Purify garlicin.Ethanol Bulbus Allii liquid is added extraction kettle by liquid pump, from the CO of steel cylinder2It is pumped to extraction kettle by high pressure measurement and extracts garlicin, then sequentially through one-level pressure relief valve, flash vaporization kettle, second depressurized valve, reclaim CO2, extract after terminating, from extraction kettle and flash vaporization kettle, take out raffinate and garlicin respectively.Adopt alcohol steep and supercritical CO2The technology that extraction phase combines extracts garlicin, and extraction ratio can reach more than 92%, and garlicin purity reaches 84%, suitable with fresh Bulbus Allii juice, therefore, adopts supercritical CO2Extraction process can make extract keep the original fresh flavor of Bulbus Allii and medicinal component.
The above is the preferred embodiment of the present invention; it should be pointed out that, for those skilled in the art, under the premise without departing from the principles of the invention; can also making some improvements and modifications, these improvements and modifications are also considered as protection scope of the present invention.
Claims (2)
1. a process technology for garlicin, specifically includes following steps:
(1) get the raw materials ready: ripe, dry, the free from insect pests of hanking, without the Bulbus Allii gone rotten, stalk, point lobe, stripping underwear, rinse with clear water, remove impurity and undesirable set of garlic tablet；
(2) broken, drying: garlic tablet is processed into pasty state with pulverizer；Being stuck with paste by Bulbus Allii and put into baking oven, dry with slow fire, temperature controls at 60～65 DEG C, dries 6～8 hours, within every 2 hours, stirs 1 time, makes Bulbus Allii stick with paste and is heated evenly；
(3) pulverizing: use pulverizer grinds, crosses 80～100 mesh sieves；
(4) deodorization is soaked: it is 1:3 that Bulbus Allii powder puts into 30～40 DEG C of wine sealing immersion deodorization in 6 hours (Bulbus Allii powder and wine) ratios；
(5) separate: adopt suction method, the solution on upper strata is taken out, is deodorised allicin stock solution.
2. the process technology of a kind of garlicin according to claim 1, it is characterised in that: specifically include following steps: adopt supercritical CO2Fluid extraction technology, adopts ethanol to leach and supercritical CO2Purify the Methods For Purification garlicin that combines, maintain both original strong points and avoided their weakness, it is achieved the supercritical CO of garlicin2Continuous extraction purification operations；Technology is as follows:
(1) ethanol extraction Bulbus Allii liquid: Bulbus Allii head peeling, section, soak with ethanol, isolates ethanol Bulbus Allii liquid, as the raw material of SCF-CO 2；Ethanol Bulbus Allii liquid is containing 1.2～2.2mg garlicin/ml；
(2) supercritical CO2Purify garlicin: ethanol Bulbus Allii liquid is added extraction kettle by liquid pump, from the CO of steel cylinder2It is pumped to extraction kettle by high pressure measurement and extracts garlicin, then sequentially through one-level pressure relief valve, flash vaporization kettle, second depressurized valve, reclaim CO2, extract after terminating, from extraction kettle and flash vaporization kettle, take out raffinate and garlicin respectively；Adopt alcohol steep and supercritical CO2The technology that extraction phase combines extracts garlicin, and extraction ratio can reach more than 92%, and garlicin purity reaches 84%, suitable with fresh Bulbus Allii juice, therefore, adopts supercritical CO2Extraction process can make extract keep the original fresh flavor of Bulbus Allii and medicinal component.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410786333.1A CN105753756A (en) | 2014-12-18 | 2014-12-18 | Allicin-processing technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410786333.1A CN105753756A (en) | 2014-12-18 | 2014-12-18 | Allicin-processing technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105753756A true CN105753756A (en) | 2016-07-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410786333.1A Pending CN105753756A (en) | 2014-12-18 | 2014-12-18 | Allicin-processing technology |
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| CN (1) | CN105753756A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107141075A (en) * | 2017-05-19 | 2017-09-08 | 郑州惠农有害生物防治有限公司 | A kind of tobacco leaf falls yellow Synergistic compound mixture and its application method |
| CN115152764A (en) * | 2022-06-24 | 2022-10-11 | 江苏省农业科学院 | Application of allicin in preventing and treating pythium root rot of mung beans |
-
2014
- 2014-12-18 CN CN201410786333.1A patent/CN105753756A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107141075A (en) * | 2017-05-19 | 2017-09-08 | 郑州惠农有害生物防治有限公司 | A kind of tobacco leaf falls yellow Synergistic compound mixture and its application method |
| CN115152764A (en) * | 2022-06-24 | 2022-10-11 | 江苏省农业科学院 | Application of allicin in preventing and treating pythium root rot of mung beans |
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Application publication date: 20160713 |