CN105726367B - A kind of foundation cream and preparation method thereof of the mud of coloured silk containing natural minerals - Google Patents
A kind of foundation cream and preparation method thereof of the mud of coloured silk containing natural minerals Download PDFInfo
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- CN105726367B CN105726367B CN201610229228.7A CN201610229228A CN105726367B CN 105726367 B CN105726367 B CN 105726367B CN 201610229228 A CN201610229228 A CN 201610229228A CN 105726367 B CN105726367 B CN 105726367B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/23—Sulfur; Selenium; Tellurium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
Abstract
The present invention provides a kind of foundation cream and preparation method thereof of mud of coloured silk containing natural minerals, and the foundation cream includes each component of following mass percent: natural minerals coloured silk mud 1~10%, emollient 5%~17%, film forming agent 0.5~2%, suspending agent 1~5%, emulsifier 1.5~7%, moisturizer 3%~15%；The suspending agent is ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite, and the emulsifier is that both PEG-9 Polydimethylsiloxyethyl Dimethicone and PEG-10 Polydimethylsiloxane are composed.Foundation cream provided by the invention containing natural minerals coloured silk mud, good stability, wherein the natural minerals coloured silk mud added can substitute the traditional stains substance of the titanium dioxide and iron oxides that add in traditional foundation cream completely.
Description
Technical field
The invention belongs to cosmetic technical field, in particular to a kind of foundation cream containing natural minerals coloured silk mud and its preparation side
Method.
Background technique
Commercially available foundation cream class product is general to reach screening by the pigment of addition titanium dioxide (titanium dioxide) and iron oxides
The flaw, whitening, the effect for adjusting the colour of skin, mineral composition due to titanium dioxide and the pigment of iron oxides without containing needed by human body and
Microelement, they cannot carry out any skin-care effect to skin tape.Moreover, the product of foundation cream class, the colour of skin is adjusted in formula
For the density of raw material (titanium dioxide, iron oxides etc.) often compared with other raw materials, density contrast is very big, so the requirement to formula
Can it is relatively high, how this substance to be steadily suspended in formula system, a foundation formulas steady in a long-term is made, this
The art technological difficulties always.
Summary of the invention
The present invention is to make up the deficiencies in the prior art, provides a kind of foundation cream containing natural minerals coloured silk mud, which stablizes
Property is good, wherein the natural minerals coloured silk mud added can substitute the tradition of the titanium dioxide and iron oxides that add in traditional foundation cream completely
Coloring material.
The present invention be reach its purpose, the technical solution adopted is as follows:
A kind of foundation cream of the mud of coloured silk containing natural minerals, the foundation cream includes each component of following mass percent: natural minerals
Color mud 1~10%, emollient 5%~17%, film forming agent 0.5~2%, suspending agent 1~5%, emulsifier 1.5~7%, moisturizer
3%~15%；The suspending agent is ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite, and the emulsifier is
Both PEG-9 Polydimethylsiloxyethyl Dimethicone and PEG-10 Polydimethylsiloxane are composed.
Further, its partial size of the natural minerals coloured silk mud is 10~20 microns, and density is 2.13~2.3g/cm3.This hair
(density: 2.130~2.300) than iron oxides, (density is about 5.24g/cm to the density of bright natural minerals coloured silk mud3) lower, with
Relatively, it is more easily more suspending stabilized than iron oxides for the density of foundation product, is matched using the preferred natural minerals coloured silk mud
The foundation product of system more is stablized.
Further, the natural minerals coloured silk mud is prepared according to the method included the following steps:
1) it air-dries: by the ring that the clay acquired from Amazon River estuary is placed on 45-50 DEG C of temperature, humidity is 15-25%
It is air-dried under border；The color that the color of natural minerals coloured silk mud is carried from the clay of acquisition itself.
2) physics refines: the clay after step 1) is air-dried is ground into the coarse powder that partial size is -1500 mesh of 1000 mesh.
3) air-flow crushing: coarse powder being put into and carries out air-flow crushing in airslide disintegrating mill, obtain partial size be 10-20 micron surpass
Fine powder；
4) superfines ozone sterilization: is used into ozone sterilization while stirring.
It is further preferred that the clay acquisition is from the unpolluted stratum of Amazon River estuary, it is further specific
, intersection of the clay from Amazon River estuary and the Atlantic Ocean.
As a kind of specific embodiment, it is the natural of red, purple or black that the natural minerals coloured silk mud, which is selected from color,
At least one of mineral coloured silk mud.It can also be the natural minerals coloured silk mud of other colors, such as white, primary color, vanilla color, shallow
Green, rosiness, light red, dark red, brown, purple, black, golden yellow, yellow etc..These colors are natural from preparation
Clay itself institute band color used when mineral coloured silk mud, such as clay collected is red, then corresponding natural minerals coloured silk mud is
It is red.
It is further preferred that the emulsifier is that the following group of shared mass percent is grouped as in foundation cream: PEG-9 is poly-
Dimethyl silica ethyl dimethyl silicone polymer 1.0%~4.0%, PEG-10 Polydimethylsiloxane 0.5%~3.0%.It is logical
Preferred suspending agent and emulsifier combination are crossed, can further improve the stability of formula system.
As a preferred embodiment, the emollient includes each component that shared mass percent is following in foundation cream: different
Tridecanol isononoate 2.0%~5.0%, phenyl trimethicone 1.0%~2.0%, isononyl isononanoate 2.0%~
10.0%；The film forming agent be ring five dimethyl silicone polymer (and) acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer；Institute
Stating moisturizer includes each component that shared mass percent is following in foundation cream: trehalose 1.0%~8.0%, butanediol 2.0%
~7.0%.
As a preferred embodiment, the foundation cream further include skin sense regulator 1.0%~3.0%, emollients 1.0%~
5.0%, the water of antifreeze 0.5%~1.0%, functional additive 1.0%~4.0%, preservative 0.1~1.0% and surplus.
Further, the skin sense regulator is polyamide fibre -6, and the emollients are phenyl trimethicone, described anti-
Jelly agent is magnesium sulfate, and the functional additive is avenabeta glucosan.
Second aspect of the present invention provides a kind of preparation method of the foundation cream of mud of coloured silk containing natural minerals described above, including such as
Lower step:
1) each component is weighed by formula, the formula includes each component of following mass percent: natural minerals coloured silk mud 1%
~10%, different tridecanol isononoate 2.0%~5.0%, phenyl trimethicone 1.0%~2.0%, titanium dioxide
0%~6.0%, iron oxide color paste 0%~0.8%, polyamide fibre -6 1.0%~3.0%, ring five dimethyl silicone polymer (and) third
Olefin(e) acid (ester) class/polydimethylsiloxanecopolymer copolymer 0.5%~2.0%, isononyl isononanoate 2.0%~10.0%, ring five are poly-
Dimethyl siloxane/distearyl dimethylammonium hectorite 1.0%~5.0%, PEG-9 polydimethylsiloxanes ethyl poly dimethyl silicon
Oxygen alkane 1.0%~4.0%, PEG-10 Polydimethylsiloxane 0.5%~3.0%, phenyl trimethicone 1.0%~
5.0%, trehalose 1.0%~8.0%, butanediol 2.0%~7.0%, magnesium sulfate 0.5%~1.0%, avenabeta glucosan
1.0%~4.0%, Phenoxyethanol (and) Sensiva SC50 0.1-1%, surplus is deionized water；
2) by natural minerals coloured silk mud, different tridecanol isononoate, phenyl trimethicone, polyamide fibre -6, ring five poly- two
Methylsiloxane (and) acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer be uniformly mixed, it is spare after three-roller is ground, make
For component A；
3) by isononyl isononanoate, ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite, the poly- diformazan of PEG-9
Base silica ethyl dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, phenyl trimethicone are added in oily phase pot,
As B component；The component A in step 2) is added in B component again, is uniformly mixed to obtain AB mixed component；
4) trehalose, butanediol, magnesium sulfate, water are uniformly mixed, are added in water phase pot, be heated to 75-85 DEG C, heat preservation 5
~30 minutes, 55~45 DEG C are cooled to, as component C；
5) component C is pumped into the AB mixed component in step 3), stirring, homogeneous；Stirring is cooled to 45 DEG C hereinafter, being added
Avenabeta glucosan, Phenoxyethanol (and) Sensiva SC50, homogeneous stirs evenly.
Technical solution provided by the invention has the following beneficial effects:
Its stability of foundation formulas is always the technological difficulties of the art, especially after addition mineral composition, surely
Qualitative is even more the problem that those skilled in the art are faced.The present invention by natural containing abundant minerals and microelement
Mineral coloured silk mud is added in foundation formulas, can not only assign the more skin-care effects of foundation product, the application range of widening foundation cream,
Improve the concealing power of foundation cream；And special formulation system through the invention, by the combined application of suspending agent and emulsifier etc.,
Obtained foundation cream its stability containing natural minerals coloured silk mud is fine, and the present invention prepares foundation cream production using natural minerals coloured silk mud
Product can substitute the colorant materials of traditional titanium dioxide and iron oxides completely.
The natural minerals coloured silk mud of addition of the invention is made by special technique, and for partial size at 10-20 microns, skin sense is soft
With；The color that clay itself carries, more naturally, and stability is high, is not influenced by high temperature and pH value；Surface is spherical,
Glabrous skin improves sense of touch, foundation cream is made when in use, skin sense is softer, adjusts the better effect of the colour of skin；Powder of the invention
This natural minerals coloured silk mud added in bottom can good absorption skin surface grease, it is possible to reduce it is glossy on the face, pH value and
Skin approaches and the affinity of skin is high, while also having good concealing power, can help to cover color spot and the adjustment colour of skin.
Natural minerals coloured silk mud is added in foundation product, due to the various metals member contained in natural minerals coloured silk mud
Element can assign the appearance for inhaling human eye ball so as to show multicoloured natural color with the bottom adornment product that it is prepared.
Due to the diversity of its color of natural minerals coloured silk mud, the application range of conventional oxidation iron class pigment has been expanded significantly, can have been produced
The bottom adornment product of more masstone out.Several mineral materials and microelement contained in natural minerals coloured silk mud are common oxidations
Iron and titanium dioxide are incomparable, can further promote the skin-care effect of foundation cream.
Foundation product prepared by the present invention, it is in terms of stability, safety, skin sense, patch skin and effect and traditional
Foundation product is compared, and has obviously advantage.
Specific embodiment
Technical scheme is described further combined with specific embodiments below:
Embodiment 1-3 is foundation cream embodiment of the present invention
The foundation product of Examples 1 to 3 is prepared in accordance with the following steps:
The production method of foundation cream of the invention, its step are as follows:
1) each component of embodiment 1-3 is weighed according to formula table shown in the following table 1, it is spare；
2) component A is uniformly mixed, then cross three-roller grind 2 times it is spare；
3) B component is sequentially added into oily phase pot, then B component is added in ground component A, be uniformly mixed, obtain AB mixing
Component；
4) component C is uniformly mixed, opens stirring, be added in water phase pot, be heated to 80 DEG C, kept the temperature 20 minutes, be cooled to
50℃；
5) it vacuumizes, under middling speed (600~700rpm) stirring, component C is uniformly pumped into AB mixed component, C
After the completion of component is added, continue 15~20min of stirring, and homogeneous；When stirring is cooled to 45 DEG C or less, D component is added, homogeneous is simultaneously
It stirs evenly；
6) 40 DEG C are cooled to, it is qualified to examine, and discharges filling.
Natural minerals coloured silk mud in Examples 1 to 3 is made in accordance with the following steps:
1) it air-dries: the clay acquired from the unpolluted stratum of Amazon River estuary is placed on 45-50 DEG C of temperature, wet
Degree is forced air drying in the environment of 20%, and the time controlled at 20-24 hours.
2) physics refines: the clay after air-drying being stirred with pulverizer and is crushed, obtaining partial size is about -1500 purpose of 1000 mesh
Coarse powder.
3) air-flow crushing: coarse powder is put into and carries out high pressure (5 atmospheric pressure) in airslide disintegrating mill air-flow crushing 2-3 times, is obtained
The superfines for being about 10-20 microns to partial size.
4) ozone sterilization: the superfines of 30KG is put into 200L sealing agitated kettle, the ozone of high concentration, side are passed through
Side sterilization is stirred, 1 hour is persistently stirred；Obtain natural minerals coloured silk mud.
5) sealed package: the natural minerals coloured silk mud after disinfection being fitted into the polybag of sealing, and sealing is labelled.
1 formula table of table
Reference examples
The foundation cream of reference examples is according to formula weighs each component accordingly shown in table 1, remaining preparation step and embodiment 1-3 base
This is identical, repeats no more.
Product evaluation and detection
One, oil-control skin care is evaluated
Test sample: embodiment 1 (color mud foundation cream), reference examples (traditional foundation cream)
Test purpose: being used continuously skin-protection product by adult female volunteer under normal circumstances, assesses skin care production
The effect of product are in terms of oil-control and skin care.
Volunteer's age: 22~44 years old
Gender: women
Volunteer's number: 50 people
Volunteer's face skin quality: blee is obscure, matt
Whitening effect: cheek (left and right face)
Product frequency of use: uniformly smearing after face cleaning, and 1 time a day, left face is 1 sample of embodiment, and right face is reference examples sample
Product.Using after product four weeks and using after product eight weeks.
Test item: oil-control skin effect
Appraisal procedure: by the way of questionnaire survey, 4 weeks and 8 weeks understanding subjects use product after using product
Evaluation in terms of oil-control skin care afterwards.Judging quota is broadly divided into: oil-control skin effect.As a result be divided into: effect is unobvious, effect one
As, it is obvious, clearly.
1), after using product four weeks
Conclusion: using color mud foundation cream of the invention, and 28 days oil-control skin effects count display, about 70% aspiration
Person feels the oil-control skin effect for having obvious.
2), using after product eight weeks
Conclusion: using color mud foundation cream of the invention, and 56 days oil-control skin effects count display, about 92% aspiration
Person feels the oil-control skin effect for having obvious.
Two, product safety assessment (subsensitivety test result)
Evaluation method:
1) tested material: embodiment 1-3 (color mud foundation cream)
2) negative control: reference examples (traditional foundation cream)
2) subject: totally 30 people, male 8 people, 22 people of female, the age 20~35 years old, sensibility skin crowd.
3) spot test method: selecting qualified spot tester, with enclosed patch test method, by tested material about 0.02ml~
0.025ml is applied in spot tester, and external application special adhesive tape is pasted on subject's forearm song side, removes tested material after 24 hours, in going
Except 30min after tested material spot tester, dermoreaction is observed after impression disappearance, by " cosmetics health specification " (version in 2007)
Dermoreaction grade scale records its result.
4) evaluation of result: according to the form below (skin adverse reaction grading standard) records reaction result.
Skin adverse reaction grading standard
5) test result:
Cosmetic skin patch test results
Human skin patch test result is shown:
A, in embodiment 1, embodiment 2, embodiment 3, all negative (grading system: 0 of 30 subjects skins
Grade).According to " cosmetics health specification " (version in 2007) human skin patch judgment criteria, sample to human body without skin not
Good reaction.
B, compared with reference examples, color mud foundation cream shows higher safety for embodiment 1, embodiment 2, embodiment 3, even if
Using the crowd in sensitive skin, also no any abnormal response of appearance.
Three, product stability is assessed
1.1 temperature stability test
1.1.1 48 DEG C of stability tests:
◆ test sample: 2
◆ the testing time: 4 weeks
◆ test method: product (content) is fitted into the PET bottle of 30ML, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 48 DEG C of biochemical cultivation case, exist respectively
The variation of the appearance, smell, pH, viscosity of (restore to room temperature) observation product at 24 hours, 1 week, 2 weeks, 4 weeks, and by day part
Variation, be recorded into report.
1.1.2 40 DEG C of stability tests:
◆ test sample: 2
◆ the testing time: 12 weeks
◆ test method: product (content) is fitted into the PET bottle of 30ML, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, be placed in the heat-resistant stability of test product in 40 DEG C of biochemical cultivation case, exist respectively
(restore to room temperature) variation of the appearance, smell, pH, viscosity of observation product at 24 hours, 1 week, 2 weeks, 4 weeks, 8 weeks and 12 weeks,
And by the variation of day part, it is recorded into report.
1.1.3 room temperature (Ambient) stability test:
◆ test sample: 2
◆ the testing time: 12 weeks
◆ test method: product (content) is fitted into the PET bottle of 30ML, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, be placed in sample cabinet, respectively 24 hours (surveying pH value, viscosimetric), 1 week, 2 weeks, 4
The variation of the appearance, smell, pH, viscosity of observation product when week, 8 weeks and 12 weeks (surveying pH value), and by the variation of day part, it records
Enter in report.
1.1.4-18 DEG C of stability tests:
◆ test sample: 2
◆ the testing time: 12 weeks
◆ test method: product (content) is fitted into the PET bottle of 30ML, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, the cold-resistant stability of test product in -18 DEG C of refrigerators is placed in, respectively 24 hours, 1
Week, 2 weeks, 4 weeks, 8 weeks and at 12 weeks (recovery to room temperature) observe the variation of the appearance, smell, pH, viscosity of product, and will be each when
The variation of section, is recorded into report.
1.1.5 48 DEG C and -18 DEG C of cyclical stability tests
◆ test sample: 2
◆ the testing time: continuous loop test three times is (after first placing 24 hours in 48 DEG C of biochemical cultivation cases, at room temperature
It places 24 hours, is then placed within -18 DEG C of refrigerators 24 hours, then restore to room temperature to recycle for one again and observe result).
◆ test method: product (content) is fitted into the PET bottle of 30ML, labelled, indicates name of product, formula
Number, the information such as test condition, testDate, be placed in 48 DEG C of biochemical cultivation case 24 hours, restore to being placed at room temperature for 24 hours,
It is subsequently placed in -18 DEG C of refrigerators 24 hours, then restores again to room temperature.Observe product when resisting cold heat-resisting alternate cycles product it is outer
The variation of sight, smell, PH, viscosity etc., and be recorded into report.
Stability result: by 12 weeks stability tests, embodiment 1, embodiment 2, the performance for stability of embodiment 3 were good
It is good, comply fully with relevant laws and regulations requirement.There is the phenomenon that water oil layer in heat-resisting test in the 2nd week in the foundation cream of reference examples,
The stability of product is not good enough.
Natural minerals coloured silk mud in the embodiment of the present invention can also use commercialized natural minerals coloured silk mud, such as fromThe color mud product of corresponding color.
The above described is only a preferred embodiment of the present invention, limitation in any form not is done to the present invention, therefore
All contents without departing from technical solution of the present invention, it is made to the above embodiment according to the technical essence of the invention any simply to repair
Change, equivalent variations and modification, all of which are still within the scope of the technical scheme of the invention.
Claims (9)
1. a kind of foundation cream of the mud of coloured silk containing natural minerals, which is characterized in that the foundation cream includes each component of following mass percent:
Natural minerals coloured silk mud 1~10%, emollient 5%~17%, film forming agent 0.5~2%, suspending agent 1~5%, emulsifier 1.5~
7%, moisturizer 3%~15%；The suspending agent is ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite, described
Emulsifier be both PEG-9 Polydimethylsiloxyethyl Dimethicone and PEG-10 Polydimethylsiloxane combine and
At；
The natural minerals coloured silk mud is prepared according to the method included the following steps:
1) it air-dries: 45-50 DEG C of temperature, humidity will be placed on from the clay that Amazon River estuary acquires as in the environment of 15-25%
It air-dries；
2) physics refines: the clay after step 1) is air-dried is ground into the coarse powder that partial size is -1500 mesh of 1000 mesh；
3) air-flow crushing: coarse powder being put into and carries out air-flow crushing in airslide disintegrating mill, obtains the superfine powder that partial size is 10-20 microns
End；
4) superfines ozone sterilization: is used into ozone sterilization while stirring.
2. foundation cream according to claim 1, which is characterized in that its partial size of the natural minerals coloured silk mud is 10~20 microns,
Density is 2.13~2.3g/cm3。
3. foundation cream according to claim 1, which is characterized in that the clay is acquired from unpolluted stratum.
4. foundation cream according to claim 1, which is characterized in that it is red, purple that the natural minerals coloured silk mud, which is selected from color,
Or at least one of natural minerals coloured silk mud of black.
5. foundation cream according to claim 1, which is characterized in that the emulsifier is that shared mass percent is such as in foundation cream
Under group be grouped as: PEG-9 Polydimethylsiloxyethyl Dimethicone 1.0%~4.0%, PEG-10 poly dimethyl silicon
Oxygen alkane 0.5%~3.0%.
6. foundation cream according to claim 1, which is characterized in that the emollient is included in shared mass percent in foundation cream
Following each component: different tridecanol isononoate 2.0%~5.0%, phenyl trimethicone 1.0%~2.0%, different nonyl
The different nonyl ester 2.0%~10.0% of acid；The film forming agent is ring five dimethyl silicone polymer and acrylic acid (ester) class/poly dimethyl silicon
Siloxane copolymers；The moisturizer includes each component that shared mass percent is following in foundation cream: trehalose 1.0%~
8.0%, butanediol 2.0%~7.0%.
7. foundation cream according to claim 1, which is characterized in that the foundation cream further include skin sense regulator 1.0%~
3.0%, emollients 1.0%~5.0%, antifreeze 0.5%~1.0%, functional additive 1.0%~4.0%, preservative 0.1
~1.0% and surplus water.
8. foundation cream according to claim 7, which is characterized in that the skin sense regulator is polyamide fibre -6, and the emollients are
Phenyl trimethicone, the antifreeze are magnesium sulfate, and the functional additive is avenabeta glucosan.
9. a kind of preparation method of the foundation cream of the mud of coloured silk containing natural minerals, which comprises the steps of:
1) each component is weighed by formula, the formula includes each component of following mass percent: natural minerals coloured silk mud 1%~
10%, different tridecanol isononoate 2.0%~5.0%, phenyl trimethicone 1.0%~2.0%, polyamide fibre -6 1.0%
~3.0%, ring five dimethyl silicone polymer and acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer 0.5%~2.0%, different
The different nonyl ester 2.0%~10.0% of n-nonanoic acid, ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite 1.0%~5.0%,
PEG-9 Polydimethylsiloxyethyl Dimethicone 1.0%~4.0%, PEG-10 Polydimethylsiloxane 0.5%~
3.0%, phenyl trimethicone 1.0%~5.0%, trehalose 1.0%~8.0%, butanediol 2.0%~7.0%, sulphur
Sour magnesium 0.5%~1.0%, avenabeta glucosan 1.0%~4.0%, Phenoxyethanol and Sensiva SC50 0.1-1%, surplus
For deionized water；
2) by natural minerals coloured silk mud, different tridecanol isononoate, phenyl trimethicone, polyamide fibre -6, five poly dimethyl of ring
Siloxanes and acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer are uniformly mixed, spare after three-roller is ground, as A group
Point；
3) by isononyl isononanoate, ring five dimethyl silicone polymer/distearyl dimethylammonium hectorite, PEG-9 poly dimethyl silicon
Oxygen ethyl dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, phenyl trimethicone are added in oily phase pot, as
B component；The component A in step 2) is added in B component again, is uniformly mixed to obtain AB mixed component；
4) trehalose, butanediol, magnesium sulfate, water are uniformly mixed, are added in water phase pot, be heated to 75-85 DEG C, heat preservation 5~30
Minute, 55~45 DEG C are cooled to, as component C；
5) component C is pumped into the AB mixed component in step 3), stirring, homogeneous；Stirring is cooled to 45 DEG C hereinafter, oat is added
Beta glucan, Phenoxyethanol and Sensiva SC50, homogeneous stir evenly；
The natural minerals coloured silk mud is prepared according to the method included the following steps:
1) it air-dries: 45-50 DEG C of temperature, humidity will be placed on from the clay that Amazon River estuary acquires as in the environment of 15-25%
It air-dries；
2) physics refines: the clay after step 1) is air-dried is ground into the coarse powder that partial size is -1500 mesh of 1000 mesh；
3) air-flow crushing: coarse powder being put into and carries out air-flow crushing in airslide disintegrating mill, obtains the superfine powder that partial size is 10-20 microns
End；
4) superfines ozone sterilization: is used into ozone sterilization while stirring.
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| CN107149563B (en) * | 2017-05-02 | 2020-02-18 | 上海蔻沣生物科技有限公司 | Foundation premix changing color from light to dark, foundation composition and preparation method thereof |
| CN107693405A (en) * | 2017-11-08 | 2018-02-16 | 诺斯贝尔化妆品股份有限公司 | A kind of net face mud of colour rich in mineral element |
| CN111253805A (en) * | 2020-01-08 | 2020-06-09 | 江西联锴科技有限公司 | Water-based nano ferric oxide color paste and preparation method thereof |
| CN113750001B (en) * | 2021-03-24 | 2022-07-01 | 北京东方淼森生物科技有限公司 | Mirabilis jalapa seed powder and preparation method and application thereof |
| CN114504511B (en) * | 2022-01-05 | 2024-02-23 | 上海百雀羚生物科技有限公司 | Powdery cosmetic composition |
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| CN104042511A (en) * | 2014-06-23 | 2014-09-17 | 诺斯贝尔(中山)无纺日化有限公司 | Muddy facial mask containing natural volcanic mineral mud powder |
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| CN104042511A (en) * | 2014-06-23 | 2014-09-17 | 诺斯贝尔(中山)无纺日化有限公司 | Muddy facial mask containing natural volcanic mineral mud powder |
| CN104042460A (en) * | 2014-07-10 | 2014-09-17 | 许伟琦 | Mineral mud mask prepared by use of xihua red clay and preparation method thereof |
| CN104146887A (en) * | 2014-08-26 | 2014-11-19 | 广州神采化妆品有限公司 | BB cream having long-acting moisturizing function and preparation method thereof |
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