CN105726352A - Konjac glucomannan infant powder and preparation method thereof - Google Patents
Konjac glucomannan infant powder and preparation method thereof Download PDFInfo
- Publication number
- CN105726352A CN105726352A CN201610063478.8A CN201610063478A CN105726352A CN 105726352 A CN105726352 A CN 105726352A CN 201610063478 A CN201610063478 A CN 201610063478A CN 105726352 A CN105726352 A CN 105726352A
- Authority
- CN
- China
- Prior art keywords
- powder
- rhizoma amorphophalli
- amorphophalli glucomannan
- prepare
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 105
- LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 title claims abstract description 47
- 229920002581 Glucomannan Polymers 0.000 title claims abstract description 47
- 229940046240 glucomannan Drugs 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 229920002752 Konjac Polymers 0.000 title claims abstract description 14
- 235000001206 Amorphophallus rivieri Nutrition 0.000 title abstract 8
- 235000010485 konjac Nutrition 0.000 title abstract 8
- 239000000252 konjac Substances 0.000 title abstract 8
- 241001312219 Amorphophallus konjac Species 0.000 title 1
- 241000205585 Aquilegia canadensis Species 0.000 claims abstract description 23
- 235000006040 Prunus persica var persica Nutrition 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 33
- 238000001291 vacuum drying Methods 0.000 claims description 21
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000000706 filtrate Substances 0.000 claims description 18
- 238000000746 purification Methods 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- 239000008367 deionised water Substances 0.000 claims description 6
- 229910021641 deionized water Inorganic materials 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 238000001556 precipitation Methods 0.000 claims description 6
- 238000002390 rotary evaporation Methods 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 229940076988 freshmint Drugs 0.000 claims description 5
- 240000006413 Prunus persica var. persica Species 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 241001448624 Miliaria Species 0.000 abstract description 11
- 230000000694 effects Effects 0.000 abstract description 9
- 244000144730 Amygdalus persica Species 0.000 abstract description 7
- 239000002994 raw material Substances 0.000 abstract description 5
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 206010061218 Inflammation Diseases 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 3
- 230000006378 damage Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 230000004054 inflammatory process Effects 0.000 abstract description 3
- 239000003053 toxin Substances 0.000 abstract description 3
- 241000196324 Embryophyta Species 0.000 abstract description 2
- 208000003251 Pruritus Diseases 0.000 abstract description 2
- 210000004243 sweat Anatomy 0.000 abstract description 2
- 231100000331 toxic Toxicity 0.000 abstract description 2
- 230000002588 toxic effect Effects 0.000 abstract description 2
- 231100000765 toxin Toxicity 0.000 abstract description 2
- 244000247812 Amorphophallus rivieri Species 0.000 abstract 7
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 2
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 2
- 241000894006 Bacteria Species 0.000 abstract 1
- 238000011109 contamination Methods 0.000 abstract 1
- 230000003467 diminishing effect Effects 0.000 abstract 1
- 230000007803 itching Effects 0.000 abstract 1
- 208000017520 skin disease Diseases 0.000 abstract 1
- 244000293323 Cosmos caudatus Species 0.000 description 6
- 235000005956 Cosmos caudatus Nutrition 0.000 description 6
- 230000036541 health Effects 0.000 description 5
- 210000003491 skin Anatomy 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 229920001661 Chitosan Polymers 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000003115 biocidal effect Effects 0.000 description 3
- 201000004624 Dermatitis Diseases 0.000 description 2
- 241000628997 Flos Species 0.000 description 2
- 102000016943 Muramidase Human genes 0.000 description 2
- 108010014251 Muramidase Proteins 0.000 description 2
- 108010062010 N-Acetylmuramoyl-L-alanine Amidase Proteins 0.000 description 2
- 208000027418 Wounds and injury Diseases 0.000 description 2
- 230000001139 anti-pruritic effect Effects 0.000 description 2
- 239000003908 antipruritic agent Substances 0.000 description 2
- 208000010668 atopic eczema Diseases 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000002596 correlated effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 208000014674 injury Diseases 0.000 description 2
- 235000010335 lysozyme Nutrition 0.000 description 2
- 239000004325 lysozyme Substances 0.000 description 2
- 229960000274 lysozyme Drugs 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 206010007247 Carbuncle Diseases 0.000 description 1
- NUCLJNSWZCHRKL-UHFFFAOYSA-N Diureido-essigsaeure Natural products NC(=O)NC(C(O)=O)NC(N)=O NUCLJNSWZCHRKL-UHFFFAOYSA-N 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 240000003183 Manihot esculenta Species 0.000 description 1
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- 206010033128 Ovarian cancer Diseases 0.000 description 1
- 206010061535 Ovarian neoplasm Diseases 0.000 description 1
- 208000004210 Pressure Ulcer Diseases 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000000648 calcium alginate Substances 0.000 description 1
- 235000010410 calcium alginate Nutrition 0.000 description 1
- 229960002681 calcium alginate Drugs 0.000 description 1
- OKHHGHGGPDJQHR-YMOPUZKJSA-L calcium;(2s,3s,4s,5s,6r)-6-[(2r,3s,4r,5s,6r)-2-carboxy-6-[(2r,3s,4r,5s,6r)-2-carboxylato-4,5,6-trihydroxyoxan-3-yl]oxy-4,5-dihydroxyoxan-3-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylate Chemical compound [Ca+2].O[C@@H]1[C@H](O)[C@H](O)O[C@@H](C([O-])=O)[C@H]1O[C@H]1[C@@H](O)[C@@H](O)[C@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@H](O2)C([O-])=O)O)[C@H](C(O)=O)O1 OKHHGHGGPDJQHR-YMOPUZKJSA-L 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 230000003203 everyday effect Effects 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 206010025482 malaise Diseases 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 230000007180 physiological regulation Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 230000005808 skin problem Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000000106 sweat gland Anatomy 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Jellies, Jams, And Syrups (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to konjac glucomannan infant powder and a preparation method thereof. The preparation method of the konjac glucomannan infant powder comprises the following steps: preparing purified powder of konjac glucomannan; preparing mint powder; preparing honeysuckle powder; preparing peach leaf powder; and mixing to form the powder. According to the konjac glucomannan infant powder provided by the invention, the konjac glucomannan serves as the main component which is added with other three kinds of natural medicinal plant powder; the mint has a special effect in controlling miliaria, the honeysuckle has an antibacterial function and can be used for treating heat-toxin sores, miliaria and the like, and the peach leaves are an ancient folk prescription for treating miliaria and can quickly dissipate miliaria and realize the functions of removing toxin, diminishing inflammation and relieving itching and pain. The konjac glucomannan has a good antibacterial property and strong water absorbability. The konjac glucomannan infant powder provided by the invention can absorb sweat and other secreta so as to damage the growth conditions of miliaria and bacteria and reduce the probability of skin diseases; and the product also has the advantages of pure nature, no toxic or side effects, little contamination to clothes in use, simple production technology and cheap raw materials.
Description
Technical field
The present invention relates to a kind of article of everyday use and preparation method thereof, be specifically related to a kind of Rhizoma amorphophalli glucomannan baby powder and preparation method thereof.
Background technology
Infant is due to every function of health undeveloped mature, physiological regulation function is poor, frivolous and tender and lovely plus keratodermatitis, so, skin is weak for environmental stimuli resistivity, particularly to summer, temperature height, high humidity, sweat gland secretion are too much, epidermis is continued to impregnate by perspiration, perspiration can not unobstructed excretion and accumulate in sweat duct, slight dermal inflammation is caused to react, result produces the skin problem such as infant eczema, miliaria, and prevention infant eczema etc. is highly profitable by reasonable scientifical use baby skin protection product, and talcum powder is the necessary article of infant nursing.The baby powder of commercial type is mainly with Pulvis Talci, Margarita powder, Pollen Pini etc. for raw material, through expert testimony, there is many side effect and be unfavorable for the healthy of infant in Pulvis Talci, increase the sickness rate of cancer, and Margarita powder, Pollen Pini are with high costs, increase the economic pressures of consumer.
Number of patent application be 201310633433.6 patent of invention " talcum powder " (applying date: 2013.11.29) provide and a kind of use after shower, perspiration can be absorbed, smooth skin, refrigerant fragrance, and can disinfection, skin is made to have comfort, and baby uses will not the talcum powder of allergy, but this talcum powder is mainly using chemical substances such as Pulvis Talci, magnesium carbonate, dihydroxy allantoic acid ammoniums as raw material, and Pulvis Talci is unfavorable for that infantile health is grown up, life-time service can increase the risk that girl has ovarian cancer.
Number of patent application be 201110152766.8 patent of invention " a kind of Pearl body-cooling powder " (applying date: 2011.06.08) describe a kind of utilize Margarita powder, modified corn starch to replace Pulvis Talci makes that Pulvis Talci can be avoided human injury, and the refreshing good Pearl body-cooling powder of body effect, although the talcum powder in this invention avoids the injury to human body, but raw material Margarita is rare, Margarita powder is expensive, significantly increases the cost of manufacture of talcum powder and the economic pressures of consumer.
Number of patent application be 201510065086.0 the patent of invention talcum powder and preparation method thereof of moisture absorption sterilization " a kind of can " (applying date: 2015.02.06) utilize the lysozyme extracted from egg, tapioca is selected to do diluent, it is aided with chitosan, calcium alginate, chitosan/carboxymethyl cellulose resin, aerosils etc. make talcum powder, itch dispelling although this talcum powder has traditional talcum powder, antipruritic, pre-counteracting bedsores, effect of antiinflammatory aspect, and moisture absorption bactericidal effect is more notable, but the lysozyme used in this invention, chitosan extracts relative difficulty, and the dispensing that this invention uses is more, production process bothers.
Along with improving constantly of living standard, growing up healthy and sound of infant becomes the focus point of a new generation father and mother, the requirement of infant skin care health product is also improved by people therewith, talcum powder is exactly the one of many health product, the baby powder made with Pulvis Talci, Margarita powder etc. has not met the requirement in epoch, environmental protection, economy baby powder ready to appear.
Summary of the invention
It is an object of the invention to provide a kind of Rhizoma amorphophalli glucomannan baby powder and preparation method thereof.
The present invention, with Rhizoma amorphophalli glucomannan for main component, utilizes its antibiotic property, strong absorptive and is aided with Herba Menthae powder, Flos Lonicerae powder and Folium Persicae powder and makes nontoxic, green health, not pollution clothes, make Rhizoma amorphophalli glucomannan baby powder simple, cheap, that moisture pick-up properties is good.
The preparation method of a kind of Rhizoma amorphophalli glucomannan baby powder of the present invention, it is characterised in that preparation process is as follows:
(1) Rhizoma amorphophalli glucomannan purification powder is prepared: by mass parts, in the deionized water of 2000~5000 parts, 65~85 DEG C, room temperature adds 5~15 parts of konjaku powders while stirring, stands 1~3h after stirring 25~35min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into original volume half, with volume ratio be 85~95% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 25~35 DEG C dry 4~6h, then be placed in 25~35 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder;
(2) prepare Herba Menthae powder: take fresh mint leaf, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, obtain Herba Menthae powder;
(3) prepare Honeysuckle Flower: take new fresh honeysuckle, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Honeysuckle Flower;
(4) prepare Folium Persicae powder: take fresh peach tree leaves, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Folium Persicae powder;
(5) it is mixed to form talcum powder: take the prepared Rhizoma amorphophalli glucomannan purification powder 400-500 part of step (1) in dry powder blender, add step (2) prepare Herba Menthae powder 30-50 part, step (3) prepare Honeysuckle Flower 30-50 part and step (4) in prepare Folium Persicae powder 30-50 part, mix homogeneously, prepares talcum powder.
The Rhizoma amorphophalli glucomannan baby powder of the present invention, with Rhizoma amorphophalli glucomannan for main component, adding other three kinds of natural medicinal plant powder, Herba Menthae has specially good effect in preventing and treating miliaria, and Flos Lonicerae has antibacterial action, hot carbuncle toxin, miliaria etc. can be treated, peach tree blade is the ancient folk prescription for the treatment of miliaria, because containing tannin component in leaf of Fructus Persicae, it is possible to make miliaria dissipate rapidly, and play detoxicating, relieving inflammation, the effect of antipruritic pain relieving.And Rhizoma amorphophalli glucomannan has good antibiotic property and strong absorptive.Rhizoma amorphophalli glucomannan baby powder can absorb perspiration and other secretions, destroy the condition of miliaria and bacterial growth, reduce dermopathic incidence rate, and this product also has Pure natural nontoxic side effect, use in the advantage production technologies such as the pollution of medicated clothing is little is simple, the advantage of low in raw material price.The Rhizoma amorphophalli glucomannan baby powder of the present invention is as shown in table 1 with existing talcum powder correlated performance test comparison result on the market.
The Rhizoma amorphophalli glucomannan baby powder of table 1 present invention and existing talcum powder correlated performance test comparison result on the market
Through above-mentioned test comparison, the present invention is in toxic and side effects, and water absorption, antibiotic property, in the index such as cost performance, other talcum powder are more excellent all more on the market, can become a kind of talcum powder that infant uses.
Detailed description of the invention
In order to fully disclose Rhizoma amorphophalli glucomannan baby powder of the present invention and preparation method thereof, below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1, a kind of Rhizoma amorphophalli glucomannan baby powder preparation method, comprise the following steps:
(1) prepare Rhizoma amorphophalli glucomannan purification powder: by mass parts, in the deionized water of 4000 parts, 75 DEG C, room temperature adds 10 parts of konjaku powders while stirring, stand 2h after stirring 30min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into original volume half, with volume ratio be 90% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 30 DEG C dry 5h, then be placed in 30 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder;
(2) prepare Herba Menthae powder: take fresh mint leaf, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, obtain Herba Menthae powder;
(3) prepare Honeysuckle Flower: take new fresh honeysuckle, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Honeysuckle Flower;
(4) prepare Folium Persicae powder: take fresh peach tree leaves, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Folium Persicae powder;
(5) it is mixed to form talcum powder: take 450 parts prepared of Rhizoma amorphophalli glucomannan purification powder of step (1) in dry powder blender, add step (2) prepare 40 parts of Herba Menthae powder, step (3) prepare Honeysuckle Flower 40 parts and step (4) in prepare 40 parts of Folium Persicae powder, mix homogeneously, prepares talcum powder.
Embodiment 2, a kind of Rhizoma amorphophalli glucomannan baby powder preparation method, comprise the following steps:
(1) prepare Rhizoma amorphophalli glucomannan purification powder: in 2000g, the deionized water of 75 DEG C, room temperature adds 10g konjaku powder while stirring, stand 3h after stirring 25min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into the half of original volume, with volume ratio be 95% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 30 DEG C dry 6h, then be placed in 35 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder;
(2) prepare Herba Menthae powder: take fresh mint leaf, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, obtain Herba Menthae powder;
(3) prepare Honeysuckle Flower: take new fresh honeysuckle, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Honeysuckle Flower;
(4) prepare Folium Persicae powder: take fresh peach tree leaves, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Folium Persicae powder;
(5) it is mixed to form talcum powder: take 400 parts prepared of Rhizoma amorphophalli glucomannan purification powder of step (1) in dry powder blender, add step (2) prepare 40 parts of Herba Menthae powder, step (3) prepare Honeysuckle Flower 30 parts and step (4) in prepare 40 parts of Folium Persicae powder, mix homogeneously, prepares talcum powder.
Embodiment 3, a kind of Rhizoma amorphophalli glucomannan baby powder preparation method, comprise the following steps:
(1) prepare Rhizoma amorphophalli glucomannan purification powder: in 4000g, the deionized water of 85 DEG C, room temperature adds 15g konjaku powder while stirring, stand 2h after stirring 35min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into the half of original volume, with volume ratio be 95% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 35 DEG C dry 5h, then be placed in 30 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder;
(2) prepare Herba Menthae powder: take fresh mint leaf, dry, pulverize, cross 100 mesh sieves be placed on 25 DEG C of vacuum drying ovens be dried to quality keep constant, obtain Herba Menthae powder;
(3) prepare Honeysuckle Flower: take new fresh honeysuckle, dry, pulverize, cross 100 mesh sieves be placed on 30 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Honeysuckle Flower;
(4) prepare Folium Persicae powder: take fresh peach tree leaves, dry, pulverize, cross 100 mesh sieves be placed on 35 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Folium Persicae powder;
(5) it is mixed to form talcum powder: take 500 parts prepared of Rhizoma amorphophalli glucomannan purification powder of step (1) in dry powder blender, add step (2) prepare 50 parts of Herba Menthae powder, step (3) prepare Honeysuckle Flower 50 parts and step (4) in prepare 50 parts of Folium Persicae powder, mix homogeneously, prepares talcum powder.
The foregoing is only presently preferred embodiments of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to the covering scope of the present invention.
Claims (4)
1. the preparation method of a Rhizoma amorphophalli glucomannan baby powder, it is characterised in that preparation process is as follows:
(1) Rhizoma amorphophalli glucomannan purification powder is prepared: by mass parts, in the deionized water of 2000~5000 parts, 65~85 DEG C, room temperature adds 5~15 parts of konjaku powders while stirring, stands 1~3h after stirring 25~35min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into the half of original volume, with volume ratio be 85~95% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 25~35 DEG C dry 4~6h, then be placed in 25~35 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder;
(2) prepare Herba Menthae powder: take fresh mint leaf, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, obtain Herba Menthae powder;
(3) prepare Honeysuckle Flower: take new fresh honeysuckle, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Honeysuckle Flower;
(4) prepare Folium Persicae powder: take fresh peach tree leaves, dry, pulverize, cross 100 mesh sieves be placed on 25~35 DEG C of vacuum drying ovens be dried to quality keep constant, prepare Folium Persicae powder;
(5) it is mixed to form talcum powder: take the prepared Rhizoma amorphophalli glucomannan purification powder 400-500 part of step (1) in dry powder blender, add step (2) prepare Herba Menthae powder 30-50 part, step (3) prepare Honeysuckle Flower 30-50 part and step (4) in prepare Folium Persicae powder 30-50 part, mix homogeneously, prepares Rhizoma amorphophalli glucomannan baby powder.
2. the preparation method of a kind of Rhizoma amorphophalli glucomannan baby powder according to claim 1, it is characterized in that described preparing Rhizoma amorphophalli glucomannan purification powder: by mass parts, in the deionized water of 4000 parts, 75 DEG C, room temperature adds 10 parts of konjaku powders while stirring, 2h is stood after stirring 30min with 400r/min, remove insoluble impurities through sucking filtration, retain filtrate;Rotary evaporation filtrate is concentrated into original volume half, with volume ratio be 90% ethanol for precipitant, pour in the filtrate after concentration, pour into while stir, collect precipitation and with absolute ethanol washing, then put the precipitate in the air dry oven of 30 DEG C dry 5h, then be placed in 30 DEG C of vacuum drying ovens and be dried to quality and keep constant, obtain Rhizoma amorphophalli glucomannan purification powder.
3. the preparation method of a kind of Rhizoma amorphophalli glucomannan baby powder according to claim 1, talcum powder it is mixed to form: take 450 parts of Rhizoma amorphophalli glucomannan purification powder in dry powder blender described in it is characterized in that, add 40 parts of Herba Menthae powder, Honeysuckle Flower 40 parts and 40 parts of Folium Persicae powder, mix homogeneously, prepares talcum powder.
4. the Rhizoma amorphophalli glucomannan baby powder that prepared by the either method described in claim 1-3.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610063478.8A CN105726352B (en) | 2016-01-29 | 2016-01-29 | A kind of konjaku glucomannan baby powder and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610063478.8A CN105726352B (en) | 2016-01-29 | 2016-01-29 | A kind of konjaku glucomannan baby powder and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105726352A true CN105726352A (en) | 2016-07-06 |
CN105726352B CN105726352B (en) | 2018-07-13 |
Family
ID=56248120
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610063478.8A Active CN105726352B (en) | 2016-01-29 | 2016-01-29 | A kind of konjaku glucomannan baby powder and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105726352B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106344430A (en) * | 2016-11-15 | 2017-01-25 | 福建农林大学 | Konjac glucomannan shower gel and preparation method thereof |
CN107213108A (en) * | 2017-07-19 | 2017-09-29 | 郑生华 | A kind of plant for baby is releived liquid talcum powder and preparation method thereof |
CN109288762A (en) * | 2018-11-28 | 2019-02-01 | 广州贝玛生物科技有限公司 | A kind of baby's peach leaf is felt well body dew and preparation method thereof |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2002284926A (en) * | 2001-03-26 | 2002-10-03 | Noevir Co Ltd | Microgel, method for preparing the same, thickening agent and thickening composition |
CN104887607A (en) * | 2015-06-11 | 2015-09-09 | 福建农林大学 | Konjac glucomannan miliaria paste and preparation method thereof |
CN105054565B (en) * | 2015-07-03 | 2018-05-08 | 福建农林大学 | Konjaku glucomannan double-edged eyelid patch and preparation method thereof |
-
2016
- 2016-01-29 CN CN201610063478.8A patent/CN105726352B/en active Active
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106344430A (en) * | 2016-11-15 | 2017-01-25 | 福建农林大学 | Konjac glucomannan shower gel and preparation method thereof |
CN107213108A (en) * | 2017-07-19 | 2017-09-29 | 郑生华 | A kind of plant for baby is releived liquid talcum powder and preparation method thereof |
CN109288762A (en) * | 2018-11-28 | 2019-02-01 | 广州贝玛生物科技有限公司 | A kind of baby's peach leaf is felt well body dew and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
CN105726352B (en) | 2018-07-13 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104841008B (en) | A kind of aerogel dressing and preparation method thereof | |
CN105833336A (en) | Panty liner with antibacterial and healthcare functions for women | |
CN105726352A (en) | Konjac glucomannan infant powder and preparation method thereof | |
CN103989612B (en) | A kind of prickly-heat powder | |
CN104706564A (en) | Acne removing mask and preparation method thereof | |
CN107213108A (en) | A kind of plant for baby is releived liquid talcum powder and preparation method thereof | |
CN104367876A (en) | Oral care solution and preparation method thereof | |
CN106266189A (en) | Compound recipe Radix Arnebiae (Radix Lithospermi) mosquito-expelling and antipruritic cream and preparation method thereof | |
CN103599029A (en) | Antisepsis and anti-inflammation composition, talcum powder and preparation method thereof | |
CN103655390A (en) | Talcum powder containing herbal natural components and preparation process thereof | |
CN104026676A (en) | Plantain herb soup with function of clearing away heat and toxic materials and production method thereof | |
CN114652519A (en) | Nursing sanitary towel of plant polyphenol composite antibacterial system and preparation process | |
CN108432922B (en) | Honeysuckle and chrysanthemum tea for clearing pestilence and removing epidemic disease | |
CN102716060B (en) | Pine needle powder-superfine microcrystalline cellulose toilet powder and manufacturing method thereof | |
CN1533791A (en) | Chinese medicine scented tea | |
CN103798796A (en) | Blueberry wine with function of moistening throats to stop pains and production method thereof | |
CN107875285B (en) | Chinese medicinal preparation and its preparation method | |
CN106860062B (en) | One grows tea antiperspirant and preparation method thereof | |
CN114568557B (en) | Ginseng polysaccharide sweet golden flower black tea and preparation method thereof | |
CN103599205B (en) | Traditional Chinese medicine liquid of control wound infection and preparation method thereof | |
CN109303718A (en) | A kind of pure Chinese medicine compound wet tissue and preparation method thereof for preventing and treating the red stern of baby | |
CN105638993A (en) | Halitosis-removal tea bag containing radix notoginseng and preparation method thereof | |
CN105638994A (en) | Halitosis-removal tea bag containing tuckahoe and preparation method thereof | |
CN103505547A (en) | Traditional Chinese medicine composition for treating umbilical hernia | |
CN105079337A (en) | Care solution for preventing bed sore and preparation method therefor |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240621 Address after: Floor 2-3, Building 1, No. 3 Zhenggang Road, Dongqiao Economic Development Zone, Ningde City, Fujian Province, 352100 Patentee after: FUJIAN CHENRUN BIOTECH Co.,Ltd. Country or region after: China Address before: No. 15, Cangshan District, Fujian, Fuzhou, Fujian Patentee before: FUJIAN AGRICULTURE AND FORESTRY University Country or region before: China |