CN105726344A - Preparation method of cosmetic sericite having easy dispersibility - Google Patents
Preparation method of cosmetic sericite having easy dispersibility Download PDFInfo
- Publication number
- CN105726344A CN105726344A CN201610072002.0A CN201610072002A CN105726344A CN 105726344 A CN105726344 A CN 105726344A CN 201610072002 A CN201610072002 A CN 201610072002A CN 105726344 A CN105726344 A CN 105726344A
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- sericite
- cosmetic
- preparation
- ore raw
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
Abstract
The invention discloses a preparation method of a cosmetic sericite having easy dispersibility.The preparation method includes the following steps that S1, rolling compaction is performed: sericite ore raw materials are acquired, high-quality sericite ore raw materials are selected, coarse breaking is performed, the broken sericite ore raw materials are subjected to rolling compaction through an edge runner mill, and rolling compaction is repeated for 2-6 times to obtain particles A; S2, fine grinding is performed, the particles A are put into a grinding machine for full fine grinding, grinding continues for 1-3 hours to obtain a grinded material B; S3, ultrasonic treatment is performed, the grinded material B is put into an ultrasonic oscillator for ultrasonic treatment for 1-2 hours and then is put into a reaction kettle, and drying and disinfection are performed for 2-4 hours; S4, modification is performed: a surface treating agent is added to the reaction kettle in the step S3, stirring is performed at the temperature of 60-80 DEG C for 2-3 hours to obtain a modified material C; S5, dispersion is performed: heat preservation is conducted on the modified material C at the temperature of 100-120 DEG C for 1-3 hours.The preparation method is simple, and the prepared sericite has better dispersibility and more glossiness and is suitable for application in cosmetics.
Description
Technical field
The present invention relates to the preparation method technical field with the sericite used for cosmetic of easily disperse, particularly relate to the preparation method of a kind of sericite used for cosmetic with easily disperse.
Background technology
Sericite is a kind of natural particulate white mica, and outward appearance is translucent, is rich in the silky luster of texture, and high radius-thickness ratio structure and the excellent uv-shielding capacity, especially finely squamose laminate structure with uniqueness have soft smooth characteristic.China's sericite rich in mineral resources, reserves are big, distribution is wide, and a lot of provinces are with the presence of big sericite mica ore.Common sericite in powder is hydrophilic inorganic filler, has been widely used in the industrial departments such as pottery, coating, rubber.
The preferential content of beary metal of cosmetics-stage sericite is far below the high radius-thickness ratio raw material of national standard, use the preparation technology centered by dispersibility control method, eliminate traditional handicraft because of exist wafer fracture formation burr edge and affect the flaw of skinfeel, the sensation that skin clearly smooths, exquisite quality, transparent jade-like stone are bright can be given, the particular/special requirement of senior cosmetics can be met, be widely used in various cosmetic field as extender pigment.
Existing cosmetics-stage sericite, when making cosmetics, we have proposed the preparation method of a kind of sericite used for cosmetic with easily disperse on the dispersibility of product not for this.
Summary of the invention
The technical problem existed based on background technology, the present invention proposes the preparation method of a kind of sericite used for cosmetic with easily disperse.
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 2-6 time, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 1-3h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1-2h, then abrasive material B is put in reactor, be dried sterilization, continue 2-4h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 60-80 DEG C, stir 2-3h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 100-120 DEG C 1-3h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
Preferably, described surface conditioning agent is the mixture of modifying agent and isopropanol, and the weight ratio of described modifying agent and isopropanol is 1-3:2-5.
Preferably, in described S1, gathering sericite mica ore raw material, choose the sericite mica ore raw material of high-quality, and slightly break, the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 4 times, obtains particulate matter A.
Preferably, in described S3, abrasive material B is put in ultrasonator, carry out supersound process 1.5h, then abrasive material B is put in reactor, be dried sterilization, continue 3h.
Preferably, in described S5, modifier C is incubated at a temperature of 110 DEG C 2h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
In the present invention, sericite mica ore raw material is relatively easy to obtain, in preparation process, sericite mica ore raw material is slightly broken, roll through edge runner mill again, sericite is relatively easy in post-production, is ground by grinder, the supersound process after being conducive to, more efficient, finally by being added thereto to surface conditioning agent so that it is modified, it is thus achieved that there is the sericite used for cosmetic of easily disperse, the preparation method of the present invention is simple, the sericite prepared more has dispersibility, more glossy, is suitably applied cosmetics aspect.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is explained orally further.
Embodiment one
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 2 times, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 1h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1h, then abrasive material B is put in reactor, be dried sterilization, continue 2h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 60 DEG C, stir 2h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 100 DEG C 1h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
Embodiment two
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 3 times, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 1.5h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1.25h, then abrasive material B is put in reactor, be dried sterilization, continue 2.5h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 65 DEG C, stir 2.25h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 105 DEG C 1.5h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
Embodiment three
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 4 times, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 2h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1.5h, then abrasive material B is put in reactor, be dried sterilization, continue 3h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 70 DEG C, stir 2.5h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 110 DEG C 2h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
Embodiment four
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 5 times, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 2.5h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1.75h, then abrasive material B is put in reactor, be dried sterilization, continue 3.5h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 75 DEG C, stir 2.75h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 115 DEG C 2.5h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
Embodiment five
The preparation method of a kind of sericite used for cosmetic with easily disperse that the present invention proposes, comprises the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 6 times, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 3h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 2h, then abrasive material B is put in reactor, be dried sterilization, continue 4h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 80 DEG C, stir 3h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 120 DEG C 3h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
The above; it is only the present invention preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; any those familiar with the art is in the technical scope that the invention discloses; according to technical scheme and inventive concept equivalent or change in addition thereof, all should contain within protection scope of the present invention.
Claims (5)
1. the preparation method of a sericite used for cosmetic with easily disperse, it is characterised in that comprise the following steps:
S1, rolls: gathers sericite mica ore raw material, chooses the sericite mica ore raw material of high-quality, and slightly break, and the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 2-6 time, obtains particulate matter A；
S2, levigate: particulate matter A is put into grinder, the most levigate, persistently grind 1-3h, obtain abrasive material B；
S3, supersound process: abrasive material B is put in ultrasonator, carry out supersound process 1-2h, then abrasive material B is put in reactor, be dried sterilization, continue 2-4h；
S4, modified: the reactor in S3 adds surface conditioning agent, at a temperature of 60-80 DEG C, stir 2-3h, obtain modifier C；
S5, breaks up: modifier C is incubated at a temperature of 100-120 DEG C 1-3h, breaks up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
The preparation method of a kind of sericite used for cosmetic with easily disperse the most according to claim 1, it is characterised in that described surface conditioning agent is the mixture of modifying agent and isopropanol, and the weight ratio of described modifying agent and isopropanol is 1-3:2-5.
The preparation method of a kind of sericite used for cosmetic with easily disperse the most according to claim 1, it is characterized in that, in described S1, gather sericite mica ore raw material, choosing the sericite mica ore raw material of high-quality, and slightly break, the sericite mica ore raw material after slightly breaking is rolled by edge runner mill, after repeating to roll 4 times, obtain particulate matter A.
The preparation method of a kind of sericite used for cosmetic with easily disperse the most according to claim 1, it is characterised in that in described S3, abrasive material B is put in ultrasonator, carries out supersound process 1.5h, then abrasive material B is put in reactor, it is dried sterilization, continues 3h.
The preparation method of a kind of sericite used for cosmetic with easily disperse the most according to claim 1, it is characterized in that, in described S5, modifier C is incubated at a temperature of 110 DEG C 2h, break up after cooling, i.e. can get a kind of sericite used for cosmetic with easily disperse.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610072002.0A CN105726344A (en) | 2016-02-02 | 2016-02-02 | Preparation method of cosmetic sericite having easy dispersibility |
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| CN201610072002.0A CN105726344A (en) | 2016-02-02 | 2016-02-02 | Preparation method of cosmetic sericite having easy dispersibility |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243783A (en) * | 2016-07-11 | 2016-12-21 | 滁州格锐矿业有限责任公司 | A kind of white pearlescent pigment preparation method based on sericite |
| CN107188193A (en) * | 2017-07-24 | 2017-09-22 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1542049A (en) * | 2003-11-05 | 2004-11-03 | 中国地质大学（武汉） | High water absorbing and retaining composite containing sericite and method for preparing the same |
| CN104004404A (en) * | 2014-06-11 | 2014-08-27 | 安徽恒昊科技有限公司 | Sericite/nano-silicon dioxide composite material and preparation method thereof |
| CN104606072A (en) * | 2014-12-31 | 2015-05-13 | 安徽恒昊科技有限公司 | Preparation method of silicone-treated sericite powder |
| CN104761932A (en) * | 2015-04-17 | 2015-07-08 | 武汉理工大学 | Easy-to-disperse sericite for cosmetics and preparation method thereof |
| CN104909380A (en) * | 2015-05-26 | 2015-09-16 | 武汉理工大学 | Method used for preparing sericite powder used for cosmetics |
-
2016
- 2016-02-02 CN CN201610072002.0A patent/CN105726344A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1542049A (en) * | 2003-11-05 | 2004-11-03 | 中国地质大学（武汉） | High water absorbing and retaining composite containing sericite and method for preparing the same |
| CN104004404A (en) * | 2014-06-11 | 2014-08-27 | 安徽恒昊科技有限公司 | Sericite/nano-silicon dioxide composite material and preparation method thereof |
| CN104606072A (en) * | 2014-12-31 | 2015-05-13 | 安徽恒昊科技有限公司 | Preparation method of silicone-treated sericite powder |
| CN104761932A (en) * | 2015-04-17 | 2015-07-08 | 武汉理工大学 | Easy-to-disperse sericite for cosmetics and preparation method thereof |
| CN104909380A (en) * | 2015-05-26 | 2015-09-16 | 武汉理工大学 | Method used for preparing sericite powder used for cosmetics |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243783A (en) * | 2016-07-11 | 2016-12-21 | 滁州格锐矿业有限责任公司 | A kind of white pearlescent pigment preparation method based on sericite |
| CN107188193A (en) * | 2017-07-24 | 2017-09-22 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
| CN107188193B (en) * | 2017-07-24 | 2019-05-03 | 安徽恒昊科技有限公司 | A kind of preparation method of high-purity mica powder of wet process used for cosmetic |
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Application publication date: 20160706 |
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