CN105713708A - Anti-rust lubricating canola oil for door lock and preparation method thereof - Google Patents
Anti-rust lubricating canola oil for door lock and preparation method thereof Download PDFInfo
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- CN105713708A CN105713708A CN201610076662.6A CN201610076662A CN105713708A CN 105713708 A CN105713708 A CN 105713708A CN 201610076662 A CN201610076662 A CN 201610076662A CN 105713708 A CN105713708 A CN 105713708A
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- canola oil
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- 235000019519 canola oil Nutrition 0.000 title claims abstract description 20
- 239000000828 canola oil Substances 0.000 title claims abstract description 20
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims description 7
- 230000001050 lubricating effect Effects 0.000 title abstract 3
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 14
- 239000002199 base oil Substances 0.000 claims abstract description 10
- 230000007935 neutral effect Effects 0.000 claims abstract description 9
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical compound CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000007765 cera alba Substances 0.000 claims abstract description 8
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 7
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000000344 soap Substances 0.000 claims abstract description 7
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 claims abstract description 6
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 6
- 239000000176 sodium gluconate Substances 0.000 claims abstract description 6
- 229940005574 sodium gluconate Drugs 0.000 claims abstract description 6
- 235000012207 sodium gluconate Nutrition 0.000 claims abstract description 6
- QDCPNGVVOWVKJG-VAWYXSNFSA-N 2-[(e)-dodec-1-enyl]butanedioic acid Chemical compound CCCCCCCCCC\C=C\C(C(O)=O)CC(O)=O QDCPNGVVOWVKJG-VAWYXSNFSA-N 0.000 claims abstract description 5
- DBVJJBKOTRCVKF-UHFFFAOYSA-N Etidronic acid Chemical compound OP(=O)(O)C(O)(C)P(O)(O)=O DBVJJBKOTRCVKF-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 3
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims description 30
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 239000000839 emulsion Substances 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 12
- 238000005461 lubrication Methods 0.000 claims description 9
- RAADJDWNEAXLBL-UHFFFAOYSA-N 1,2-di(nonyl)naphthalene Chemical compound C1=CC=CC2=C(CCCCCCCCC)C(CCCCCCCCC)=CC=C21 RAADJDWNEAXLBL-UHFFFAOYSA-N 0.000 claims description 7
- 229910052788 barium Inorganic materials 0.000 claims description 7
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 claims description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000002131 composite material Substances 0.000 claims description 6
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000007127 saponification reaction Methods 0.000 claims description 6
- 235000011572 Pyrus ussuriensis Nutrition 0.000 claims description 5
- 244000173166 Pyrus ussuriensis Species 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 5
- NHXVNEDMKGDNPR-UHFFFAOYSA-N zinc;pentane-2,4-dione Chemical compound [Zn+2].CC(=O)[CH-]C(C)=O.CC(=O)[CH-]C(C)=O NHXVNEDMKGDNPR-UHFFFAOYSA-N 0.000 claims description 5
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 3
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 229960004756 ethanol Drugs 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical class CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 3
- 239000001117 sulphuric acid Substances 0.000 claims description 3
- 235000011149 sulphuric acid Nutrition 0.000 claims description 3
- 229920001169 thermoplastic Polymers 0.000 claims description 3
- 239000004416 thermosoftening plastic Substances 0.000 claims description 3
- JJJOZVFVARQUJV-UHFFFAOYSA-N 2-ethylhexylphosphonic acid Chemical compound CCCCC(CC)CP(O)(O)=O JJJOZVFVARQUJV-UHFFFAOYSA-N 0.000 claims description 2
- 150000002148 esters Chemical class 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000010687 lubricating oil Substances 0.000 abstract description 8
- KEQFTVQCIQJIQW-UHFFFAOYSA-N N-Phenyl-2-naphthylamine Chemical compound C=1C=C2C=CC=CC2=CC=1NC1=CC=CC=C1 KEQFTVQCIQJIQW-UHFFFAOYSA-N 0.000 abstract description 4
- 239000003921 oil Substances 0.000 abstract description 4
- 235000019198 oils Nutrition 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 abstract description 2
- 230000007797 corrosion Effects 0.000 abstract description 2
- 238000005260 corrosion Methods 0.000 abstract description 2
- 230000003670 easy-to-clean Effects 0.000 abstract description 2
- 239000001587 sorbitan monostearate Substances 0.000 abstract description 2
- 229940035048 sorbitan monostearate Drugs 0.000 abstract description 2
- 235000011076 sorbitan monostearate Nutrition 0.000 abstract description 2
- 159000000009 barium salts Chemical class 0.000 abstract 2
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 abstract 2
- 239000012964 benzotriazole Substances 0.000 abstract 2
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 abstract 1
- 230000002035 prolonged effect Effects 0.000 abstract 1
- 239000003053 toxin Substances 0.000 abstract 1
- 231100000765 toxin Toxicity 0.000 abstract 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000000047 product Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000019508 mustard seed Nutrition 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M101/00—Lubricating compositions characterised by the base-material being a mineral or fatty oil
- C10M101/04—Fatty oil fractions
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/26—Carboxylic acids; Salts thereof
- C10M129/28—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M129/30—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 7 or less carbon atoms
- C10M129/36—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 7 or less carbon atoms containing hydroxy groups
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- C10M129/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen
- C10M129/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing oxygen having a carbon chain of less than 30 atoms
- C10M129/26—Carboxylic acids; Salts thereof
- C10M129/28—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M129/38—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 8 or more carbon atoms
- C10M129/42—Carboxylic acids; Salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having 8 or more carbon atoms polycarboxylic
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- C10M133/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen
- C10M133/02—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing nitrogen having a carbon chain of less than 30 atoms
- C10M133/38—Heterocyclic nitrogen compounds
- C10M133/44—Five-membered ring containing nitrogen and carbon only
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- C10M135/08—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing sulfur, selenium or tellurium containing a sulfur-to-oxygen bond
- C10M135/10—Sulfonic acids or derivatives thereof
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- C10M139/00—Lubricating compositions characterised by the additive being an organic non-macromolecular compound containing atoms of elements not provided for in groups C10M127/00 - C10M137/00
- C10M139/02—Esters of silicon acids
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- C10M159/02—Natural products
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- C10M2207/08—Aldehydes; Ketones
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
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- C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
- C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/16—Naphthenic acids
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
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- C10M2207/283—Esters of polyhydroxy compounds
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- C10M2207/401—Fatty vegetable or animal oils used as base material
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- C10M2215/065—Phenyl-Naphthyl amines
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- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
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- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/02—Esters of silicic acids
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- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses anti-rust lubricating canola oil for a door lock.The canola oil is prepared from, by weight, 17-20 parts of canola oil, 100-110 parts of No.32 base oil, 0.1-0.4 part of naphthenic soap, 3-4 parts of Sorbitan monostearate, 0.7-1 part of polydimethylsiloxane, 5-7 parts of tetraethoxysilane, 1-2 parts of cera alba, 0.01-0.02 part of phenyl-2-naphthylamine, 6-9 parts of neutral dinonyl-naphthalenesulfonic aci barium salt, 4-5 parts of dodecenylsuccinic acid, 0.1-0.2 part of menthyl acetate, 0.6-2 parts of benzotriazole, 1-2 parts of sodium gluconate, 0.1-0.3 part of ainc acetylacetonate and 1-2 parts of 1-hydroxyethylidene-1,1-diphosphonic acid.The canola oil is added into lubricating oil so that the lubricating effect can be improved, sodium gluconate and benzotriazole are added so that corrosion resistance can be good, the storage life of refined oil is prolonged, and dodecenylsuccinic acid and neutral dinonyl-naphthalenesulfonic aci barium salt are added so that the anti-rust effect of the lubricating oil can be improved.The lubricating oil is safe, free of toxin, easy to clean and good in comprehensive performance.
Description
Technical field
The invention mainly relates to antirust solution field, particularly relate to a kind of door lock anti-rust and lubrication Canola oil and system thereof
Preparation Method.
Background technology
The easy corrosion of lock-up time length, bite is caused to cause key to rotate difficulty after inserting difficulty or inserting,
The most just can drip appropriate lubricating oil in door lock keyhole, and traditional door lock lubricating oil greasy is strong,
Viscosity is higher, it is more difficult to clean, and have possibly together with virulent volatile material, the health of human body is also made
Become a certain degree of infringement.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of door lock anti-rust and lubrication mustard seed
Oil and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of door lock anti-rust and lubrication Canola oil, it is made up of the raw material of following weight parts:
Canola oil 17-20, No. 32 base oil 100-110, naphthenic soap 0.1-0.4, the smooth single tristearin of Pyrusussuriensis
Acid esters 3-4, polydimethylsiloxane 0.7-1, tetraethyl orthosilicate 5-7, cera alba 1-2, N-phenyl-2-naphthalene
Amine 0.01-0.02, neutral dinonyl naphthalene sulfonate barium 6-9, dodecenylsuccinic acid 4-5, menthyl acetate
0.1-0.2, BTA 0.6-2, sodium gluconate 1-2, zinc acetylacetonate 0.1-0.3, hydroxy ethylidene
Di 2 ethylhexyl phosphonic acid 1-2.
The preparation method of a kind of door lock anti-rust and lubrication Canola oil, comprises the following steps:
(1) by above-mentioned cera alba thermoplastic, joining in the dehydrated alcohol of its weight 7-10 times, stirring is all
Even, add naphthenic soap, insulated and stirred 3-5 minute at 70-80 DEG C, obtain saponification alcohol liquid;
(2) take the 50-60% of above-mentioned No. 32 base oil weight, add neutral dinonyl naphthalene sulfonate barium, stirring
Uniformly, for antirust emulsion a;
(3) remaining No. 32 base oils are mixed with Canola oil, stir, add laurylene base fourth two
Acid, for antirust emulsion b;
(4) above-mentioned antirust emulsion a, antirust emulsion b are mixed, add Pyrusussuriensis under stirring condition smooth single stearic
Acid esters, 70-100 rev/min is stirred 10-15 minute, obtains composite antirust emulsion;
(5) above-mentioned BTA is joined in the dehydrated alcohol of its weight 5-7 times, stir, add
Entering 1-hydroxy ethylidene-1,1-diphosphonic acid, rise high-temperature and be 60-70 DEG C, dropping concentration is the sulphuric acid of 96-98%, regulates pH
For 1-3, stirring reaction 40-50 minute, obtain anticorrosion premixed liquid;
(6) by above-mentioned tetraethyl orthosilicate, menthyl acetate mixing, stir, join compound weight
6-10 times, concentration be 70-80% ethanol solution in, stir, be sequentially added into above-mentioned saponification alcohol liquid,
Zinc acetylacetonate, rises high-temperature and is 70-80 DEG C, and dropping concentration is the ammonia of 20-25%, and regulation pH is 10-13,
Insulation reaction 40-50 minute, obtains premix Ludox;
(7) by above-mentioned anticorrosion premixed liquid, premix Ludox mixing, stir, add above-mentioned composite antirust
Emulsion, 300-400 rev/min is stirred 10-15 minute, dehydration, adds and remains each raw material, 600-700 rev/min
Stir 20-30 minute, to obtain final product.
The invention have the advantage that
The lubricating oil of the present invention adds Canola oil, improves lubricant effect, adds sodium gluconate, benzene
And triazole, there are good anti-corrosive properties, be delayed the pot-life of product oil, add laurylene base fourth two
Dinonyl naphthalene sulfonate barium sour, neutral, improves the rust-proof effect of lubricating oil, uses tetraethyl orthosilicate to prepare silicon molten
Glue, is blended with cera alba etc., improves finished product oil viscosity, and the lubricating oil safety non-toxic of the present invention is easy to clean,
Good combination property.
Detailed description of the invention
Embodiment 1
A kind of door lock anti-rust and lubrication Canola oil, it is made up of the raw material of following weight parts:
20, No. 32 base oils 110 of Canola oil, naphthenic soap 0.4, sorbitan monostearate 4, poly-two
Methylsiloxane 0.7, tetraethyl orthosilicate 5-7, cera alba 1, N-phenyl-2-naphthylamine 0.02, neutral dinonyl
Naphthalene sulfonate barium 6, dodecenylsuccinic acid 5, menthyl acetate 0.2, BTA 0.6, sodium gluconate
1, zinc acetylacetonate 0.3,1-hydroxy ethylidene-1,1-diphosphonic acid 2.
The preparation method of a kind of door lock anti-rust and lubrication Canola oil, comprises the following steps:
(1) by above-mentioned cera alba thermoplastic, join in the dehydrated alcohol of its weight 10 times, stir,
Add naphthenic soap, insulated and stirred 3 minutes at 80 DEG C, obtain saponification alcohol liquid;
(2) take the 60% of above-mentioned No. 32 base oil weight, add neutral dinonyl naphthalene sulfonate barium, stir,
For antirust emulsion a;
(3) remaining No. 32 base oils are mixed with Canola oil, stir, add laurylene base fourth two
Acid, for antirust emulsion b;
(4) above-mentioned antirust emulsion a, antirust emulsion b are mixed, add Pyrusussuriensis under stirring condition smooth single stearic
Acid esters, 100 revs/min are stirred 15 minutes, obtain composite antirust emulsion;
(5) above-mentioned BTA is joined in the dehydrated alcohol of its weight 7 times, stir, add
1-hydroxy ethylidene-1,1-diphosphonic acid, rising high-temperature is 70 DEG C, and dropping concentration is the sulphuric acid of 98%, and regulation pH is 3, stirs
Mix reaction 50 minutes, obtain anticorrosion premixed liquid;
(6) by above-mentioned tetraethyl orthosilicate, menthyl acetate mixing, stir, join compound weight
10 times, concentration be 80% ethanol solution in, stir, be sequentially added into above-mentioned saponification alcohol liquid, levulinic
Ketone zinc, rising high-temperature is 80 DEG C, and dropping concentration is the ammonia of 25%, and regulation pH is 13, insulation reaction 50
Minute, obtain premix Ludox;
(7) by above-mentioned anticorrosion premixed liquid, premix Ludox mixing, stir, add above-mentioned composite antirust
Emulsion, 300 revs/min are stirred 10-15 minute, dehydration, add and remain each raw material, 700 revs/min of stirrings 30
Minute, to obtain final product.
Claims (2)
1. a door lock anti-rust and lubrication Canola oil, it is characterised in that it is by the raw material of following weight parts
Composition:
Canola oil 17-20, No. 32 base oil 100-110, naphthenic soap 0.1-0.4, the smooth single tristearin of Pyrusussuriensis
Acid esters 3-4, polydimethylsiloxane 0.7-1, tetraethyl orthosilicate 5-7, cera alba 1-2, N-phenyl-2-naphthalene
Amine 0.01-0.02, neutral dinonyl naphthalene sulfonate barium 6-9, dodecenylsuccinic acid 4-5, menthyl acetate
0.1-0.2, BTA 0.6-2, sodium gluconate 1-2, zinc acetylacetonate 0.1-0.3, hydroxy ethylidene
Di 2 ethylhexyl phosphonic acid 1-2.
2. a preparation method for door lock anti-rust and lubrication Canola oil as claimed in claim 1, its feature
It is, comprises the following steps:
(1) by above-mentioned cera alba thermoplastic, joining in the dehydrated alcohol of its weight 7-10 times, stirring is all
Even, add naphthenic soap, insulated and stirred 3-5 minute at 70-80 DEG C, obtain saponification alcohol liquid;
(2) take the 50-60% of above-mentioned No. 32 base oil weight, add neutral dinonyl naphthalene sulfonate barium, stirring
Uniformly, for antirust emulsion a;
(3) remaining No. 32 base oils are mixed with Canola oil, stir, add laurylene base fourth two
Acid, for antirust emulsion b;
(4) above-mentioned antirust emulsion a, antirust emulsion b are mixed, add Pyrusussuriensis under stirring condition smooth single stearic
Acid esters, 70-100 rev/min is stirred 10-15 minute, obtains composite antirust emulsion;
(5) above-mentioned BTA is joined in the dehydrated alcohol of its weight 5-7 times, stir, add
Entering 1-hydroxy ethylidene-1,1-diphosphonic acid, rise high-temperature and be 60-70 DEG C, dropping concentration is the sulphuric acid of 96-98%, regulates pH
For 1-3, stirring reaction 40-50 minute, obtain anticorrosion premixed liquid;
(6) by above-mentioned tetraethyl orthosilicate, menthyl acetate mixing, stir, join compound weight
6-10 times, concentration be 70-80% ethanol solution in, stir, be sequentially added into above-mentioned saponification alcohol liquid,
Zinc acetylacetonate, rises high-temperature and is 70-80 DEG C, and dropping concentration is the ammonia of 20-25%, and regulation pH is 10-13,
Insulation reaction 40-50 minute, obtains premix Ludox;
(7) by above-mentioned anticorrosion premixed liquid, premix Ludox mixing, stir, add above-mentioned composite antirust
Emulsion, 300-400 rev/min is stirred 10-15 minute, dehydration, adds and remains each raw material, 600-700 rev/min
Stir 20-30 minute, to obtain final product.
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Cited By (1)
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Application publication date: 20160629 |